JP2014523337A - インサイチュ注入を用いるプレート式反応器 - Google Patents
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Abstract
Description
アクロレインを生成するためのグリセリンの脱水のためのプロセス、または
アクリル酸を生成するための乳酸の脱水のためのプロセス、または
アクリル酸を生成するための3−ヒドロキシプロピオン酸の脱水のためのプロセス、または
メタクリル酸を生成するための3−ヒドロキシイソ酪酸の脱水のためのプロセス、または
メタクリル酸を生成するための、アルファヒドロキシイソ酪酸としても知られる2−ヒドロキシイソ酪酸の脱水のためのプロセス、または
ハイドロフルオロオレフィンの、またはハイドロフルオロカーボンの調製のためのプロセス、好ましくはフルオロプロペンの調製のためのプロセス、および非常に特に好ましくは2,3,3,3−テトラフルオロプロペンの調製のためのプロセス、である。
主に図1および図4を参照すると、本発明による反応器はチャンバを含み、これは有利なことに基本的に円形断面を備える円筒形であり、その内部には、その間に反応区画3を画定する熱交換プレート1のアセンブリが配置されている。
本発明は、反応区画3内に少なくとも1つ、好ましくは複数の、物質注入装置6を設ける。物質注入装置6は、熱交換プレート1、および熱交換プレート1の間の反応区画3を、通過する。
本発明は、再生可能起源のアクリル酸の生成、具体的にはアクロレインを生成するためのグリセリンの脱水の第一段階、続いてこうして得られたアクロレインの気相での酸化の段階を含む、グリセリンからのアクリル酸の生成のために、あるいは2−ヒドロキシプロピオン酸(乳酸)または3−ヒドロキシプロピオン酸およびこれらのエステルの脱水によるアクリル酸の生成において、有利に採用される。
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)の、
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための1,1,1,2,3−ペンタクロロプロパン(HCC−240db)の、
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための1,1,2,2,3−ペンタクロロプロパン(HCC−240aa)の、
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための2,3−ジクロロ−1,1,1−トリフルオロプロパン(HCFC−243db)の、
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための1,1,2,3‐テトラクロロ−1−プロペン(HCO−1230xa)の、
2,3,3,3−テトラフルオロ−1−プロペン(HFO−1234yf)を生成するための2,3,3,3−テトラクロロ−1−プロペン(HCO−1230xf)の、
2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)を生成するための1,1,1,2,3−ペンタクロロプロパン(HCC−240db)の、
2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)を生成するための1,1,2,2,3−ペンタクロロプロパン(HCC−240aa)の、
2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)を生成するための2,3−ジクロロ−1,1,1−トリフルオロプロパン(HCFC−243db)の、
2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)を生成するための1,1,2,3‐テトラクロロ−1−プロペン(HCO−1230xa)の、
2−クロロ−3,3,3−トリフルオロ−1−プロペン(HFCO−1233xf)を生成するための2,3,3,3−テトラクロロ−1−プロペン(HCO−1230xf)の、反応である。
Claims (14)
- その間に反応区画(3)を画定する複数の熱交換プレート(1)を含む化学反応器であって、反応器内で各熱交換プレート(1)は、その間に少なくとも1つの熱交換空間(4)を画定する2つの壁(2a、2b)を含み、それぞれの壁(2a、2b)は接合領域(5)によって互いに固定されており、反応器はまた反応区画(3)内への物質の注入のための少なくとも1つの装置(6)も含み、前記物質注入装置(6)はプレートのそれぞれの接合領域(5)の熱交換プレート(1)を通過する、化学反応器。
- 物質注入装置(6)がガスの注入のための装置であり、好ましくは酸素含有ガスの注入のための装置である、請求項1に記載の化学反応器。
- 物質注入装置(6)が、複数の注入オリフィスを有するパイプである、請求項1または2に記載の化学反応器。
- 接合領域(5)が、ストリップ状の、好ましくは平行なストリップ状の、または点状の、熱交換プレート(1)の上に配置される、請求項1から3のいずれか一項に記載の化学反応器。
- 好ましくは互いに平行であり、好ましくは物質分配システム(8)に接続された、複数の物質注入装置(6)を含む、請求項1から4のいずれか一項に記載の化学反応器。
- 熱交換プレート(1)が、放射状に、または互いに平行になるように、チャンバ内に位置決めされ、好ましくはモジュールとしてグループ分けされる、請求項1から5のいずれか一項に記載の化学反応器。
- 2つの熱交換プレート(1)の間に画定された反応区画(3)の注入口における反応物質の受け入れ、反応区画(3)の排出口における反応生成物の取り出し、および反応区画(3)内への物質の注入を含む化学反応プロセスであって、各熱交換プレート(1)は、その間に少なくとも1つの熱交換空間(4)を画定する2つの壁(2a、2b)を含み、それぞれの壁(2a、2b)は接合領域(5)によって互いに固定されており、物質の注入は、プレートのそれぞれの接合領域(5)の熱交換プレート(1)を通過する少なくとも1つの物質注入装置(6)よって実行される、化学反応プロセス。
- 反応が不均一触媒タイプであり、触媒は、好ましくは固体粒子の形態で、反応区画(3)内に配置される、請求項7に記載のプロセス。
- 生成の相および触媒の再生の相を交互に含み、物質の注入が、反応相の間および/または再生相の間に実行される、請求項7または8に記載のプロセス。
- 物質が、反応物質、または触媒化合物、または触媒を再生することが可能な化合物である、請求項7から9のいずれか一項に記載のプロセス。
- 物質が酸素含有ガスである、請求項7から10のいずれか一項に記載のプロセス。
- 物質が、反応区画(3)内の反応物質の経路のいくつかの点で注入される、請求項7から11のいずれか一項に記載のプロセス。
- 請求項1から6のいずれか一項に記載の化学反応器において実行される、請求項7から12のいずれか一項に記載のプロセス。
- アクロレインを生成するためのグリセリンの脱水のためのプロセス、または
アクリル酸を生成するための乳酸の脱水のためのプロセス、または
アクリル酸を生成するための3−ヒドロキシプロピオン酸の脱水のためのプロセス、または
メタクリル酸を生成するための3−ヒドロキシイソ酪酸の脱水のためのプロセス、または
メタクリル酸を生成するための2−ヒドロキシイソ酪酸の脱水のためのプロセス、または
塩素化合物のフッ素化化合物への変換のためのプロセス、好ましくはハイドロフルオロオレフィンの、もしくはハイドロフルオロカーボンの調製のためのプロセス、具体的にはフルオロプロペンの調製のためのプロセス、および非常に特に好ましくは2,3,3,3−テトラフルオロプロペンの調製のためのプロセス、または
ホルムアルデヒドもしくはジメトキシメタンを生成するためのメタノールの酸化、アセトアルデヒドもしくはジエトキシエタンを生成するためのエタノールの酸化、無水フタル酸を生成するためのオルトキシレンもしくはナフタレンの酸化、無水マレイン酸を生成するためのベンゼン、ブテン、ブタノール、もしくはブタンの酸化、アクロレインを生成するためのプロピレンの酸化、もしくはメタクロレインを生成するためのイソブテンもしくはtert−ブタノールの酸化などの選択的酸化プロセスである、請求項7から13のいずれか一項に記載のプロセス。
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Application Number | Priority Date | Filing Date | Title |
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FR1154885 | 2011-06-06 | ||
FR1154885A FR2975922B1 (fr) | 2011-06-06 | 2011-06-06 | Reacteur a plaques avec injection in situ |
PCT/FR2012/051233 WO2012168631A1 (fr) | 2011-06-06 | 2012-06-01 | Reacteur a plaques avec injection in situ |
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JP2014523337A true JP2014523337A (ja) | 2014-09-11 |
JP2014523337A5 JP2014523337A5 (ja) | 2016-06-30 |
JP5970543B2 JP5970543B2 (ja) | 2016-08-17 |
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US (2) | US9205403B2 (ja) |
EP (1) | EP2718006B1 (ja) |
JP (1) | JP5970543B2 (ja) |
KR (1) | KR101800070B1 (ja) |
CN (1) | CN103717301B (ja) |
BR (1) | BR112013031150B1 (ja) |
FR (1) | FR2975922B1 (ja) |
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EP3401299B1 (de) | 2017-05-12 | 2021-11-03 | L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude | Reaktor zum durchführen exothermer gleichgewichtsreaktionen |
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US11325090B1 (en) | 2019-12-09 | 2022-05-10 | Precision Combustion, Inc. | Catalytic solar reactor |
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Also Published As
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WO2012168631A1 (fr) | 2012-12-13 |
JP5970543B2 (ja) | 2016-08-17 |
CN103717301A (zh) | 2014-04-09 |
BR112013031150A2 (pt) | 2017-02-07 |
US9205403B2 (en) | 2015-12-08 |
KR101800070B1 (ko) | 2017-11-21 |
KR20140039020A (ko) | 2014-03-31 |
FR2975922B1 (fr) | 2013-05-31 |
CN103717301B (zh) | 2016-06-22 |
BR112013031150B1 (pt) | 2019-11-05 |
US20140094617A1 (en) | 2014-04-03 |
EP2718006B1 (fr) | 2015-03-25 |
EP2718006A1 (fr) | 2014-04-16 |
US20160052853A1 (en) | 2016-02-25 |
US9738582B2 (en) | 2017-08-22 |
MY173895A (en) | 2020-02-26 |
FR2975922A1 (fr) | 2012-12-07 |
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