JP2014501327A - 加水分解性官能基を含むポリマーの安定化 - Google Patents

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Publication number

JP2014501327A

JP2014501327A JP2013547721A JP2013547721A JP2014501327A JP 2014501327 A JP2014501327 A JP 2014501327A JP 2013547721 A JP2013547721 A JP 2013547721A JP 2013547721 A JP2013547721 A JP 2013547721A JP 2014501327 A JP2014501327 A JP 2014501327A

Authority

JP

Japan

Prior art keywords

polymer

silyl

group

hydrocarbyl

chloride

Prior art date

2010-12-31

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

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• 229920000642 polymer Polymers 0.000 title claims abstract description 215
• 125000000524 functional group Chemical group 0.000 title claims abstract description 48
• 230000006641 stabilisation Effects 0.000 title description 2
• 238000011105 stabilization Methods 0.000 title description 2
• 239000003381 stabilizer Substances 0.000 claims abstract description 38
• 125000001183 hydrocarbyl group Chemical group 0.000 claims abstract description 34
• 125000005843 halogen group Chemical group 0.000 claims abstract description 16
• 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 9
• 230000002378 acidificating effect Effects 0.000 claims abstract description 6
• 230000007062 hydrolysis Effects 0.000 claims abstract description 6
• -1 silyl halide Chemical class 0.000 claims description 163
• 238000000034 method Methods 0.000 claims description 38
• 125000001181 organosilyl group Chemical group [SiH3]* 0.000 claims description 29
• 238000006243 chemical reaction Methods 0.000 claims description 24
• 239000002904 solvent Substances 0.000 claims description 17
• XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 15
• 229910052710 silicon Inorganic materials 0.000 claims description 15
• 125000000962 organic group Chemical group 0.000 claims description 11
• 150000004820 halides Chemical class 0.000 claims description 7
• 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 3
• VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 92
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 65
• 239000000203 mixture Substances 0.000 description 57
• 239000000178 monomer Substances 0.000 description 52
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 51
• 235000019441 ethanol Nutrition 0.000 description 50
• 239000003999 initiator Substances 0.000 description 49
• 239000003795 chemical substances by application Substances 0.000 description 46
• 238000006116 polymerization reaction Methods 0.000 description 45
• 150000001875 compounds Chemical class 0.000 description 40
• 229920001971 elastomer Polymers 0.000 description 31
• 239000003963 antioxidant agent Substances 0.000 description 29
• 239000004568 cement Substances 0.000 description 29
• 239000005060 rubber Substances 0.000 description 26
• 239000000377 silicon dioxide Substances 0.000 description 24
• PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 22
• 239000011414 polymer cement Substances 0.000 description 22
• 239000000945 filler Substances 0.000 description 21
• 239000000523 sample Substances 0.000 description 21
• 150000001993 dienes Chemical group 0.000 description 20
• CNBZTHQYUOSCDJ-UHFFFAOYSA-N n-(3-triethoxysilylpropyl)butan-2-imine Chemical compound CCO[Si](OCC)(OCC)CCCN=C(C)CC CNBZTHQYUOSCDJ-UHFFFAOYSA-N 0.000 description 20
• 229920013730 reactive polymer Polymers 0.000 description 19
• 241001441571 Hiodontidae Species 0.000 description 18
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 17
• KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 16
• 239000003054 catalyst Substances 0.000 description 15
• 238000003756 stirring Methods 0.000 description 15
• MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 description 14
• ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 14
• 239000012967 coordination catalyst Substances 0.000 description 14
• VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 12
• 125000000129 anionic group Chemical group 0.000 description 12
• 239000006229 carbon black Substances 0.000 description 11
• 239000007822 coupling agent Substances 0.000 description 11
• 238000010791 quenching Methods 0.000 description 11
• 230000000171 quenching effect Effects 0.000 description 11
• 238000010539 anionic addition polymerization reaction Methods 0.000 description 10
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
• 229930195733 hydrocarbon Natural products 0.000 description 9
• 238000002156 mixing Methods 0.000 description 9
• 229910052757 nitrogen Inorganic materials 0.000 description 9
• 239000002994 raw material Substances 0.000 description 9
• 239000010703 silicon Substances 0.000 description 9
• 239000004594 Masterbatch (MB) Substances 0.000 description 8
• MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 description 8
• 229960003493 octyltriethoxysilane Drugs 0.000 description 8
• 150000002900 organolithium compounds Chemical class 0.000 description 8
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
• 239000012298 atmosphere Substances 0.000 description 7
• 229910052744 lithium Inorganic materials 0.000 description 7
• 239000003921 oil Substances 0.000 description 7
• 239000001294 propane Substances 0.000 description 7
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
• 125000003118 aryl group Chemical group 0.000 description 6
• 238000009833 condensation Methods 0.000 description 6
• 230000005494 condensation Effects 0.000 description 6
• 238000011049 filling Methods 0.000 description 6
• 125000005842 heteroatom Chemical group 0.000 description 6
• 150000002430 hydrocarbons Chemical class 0.000 description 6
• 238000002360 preparation method Methods 0.000 description 6
• 229910052718 tin Inorganic materials 0.000 description 6
• RCHUVCPBWWSUMC-UHFFFAOYSA-N trichloro(octyl)silane Chemical compound CCCCCCCC[Si](Cl)(Cl)Cl RCHUVCPBWWSUMC-UHFFFAOYSA-N 0.000 description 6
• 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 6
• 229920002554 vinyl polymer Polymers 0.000 description 6
• 238000004073 vulcanization Methods 0.000 description 6
• VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 5
• WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 5
• NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
• 125000000217 alkyl group Chemical group 0.000 description 5
• 230000003078 antioxidant effect Effects 0.000 description 5
• QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
• 230000008901 benefit Effects 0.000 description 5
• 125000004432 carbon atom Chemical group C* 0.000 description 5
• 229920001577 copolymer Polymers 0.000 description 5
• 230000008878 coupling Effects 0.000 description 5
• 238000010168 coupling process Methods 0.000 description 5
• 238000005859 coupling reaction Methods 0.000 description 5
• 238000001035 drying Methods 0.000 description 5
• 239000000806 elastomer Substances 0.000 description 5
• 238000009472 formulation Methods 0.000 description 5
• 229910052760 oxygen Inorganic materials 0.000 description 5
• 239000001301 oxygen Substances 0.000 description 5
• 239000005049 silicon tetrachloride Substances 0.000 description 5
• 229910052717 sulfur Inorganic materials 0.000 description 5
• 239000011593 sulfur Substances 0.000 description 5
• ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 4
• RRHGJUQNOFWUDK-UHFFFAOYSA-N Isoprene Chemical compound CC(=C)C=C RRHGJUQNOFWUDK-UHFFFAOYSA-N 0.000 description 4
• WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
• ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 4
• 230000032683 aging Effects 0.000 description 4
• 125000004429 atom Chemical group 0.000 description 4
• 229910052796 boron Inorganic materials 0.000 description 4
• 229910052801 chlorine Inorganic materials 0.000 description 4
• 230000000052 comparative effect Effects 0.000 description 4
• 238000012718 coordination polymerization Methods 0.000 description 4
• 238000001723 curing Methods 0.000 description 4
• 125000000392 cycloalkenyl group Chemical group 0.000 description 4
• AFABGHUZZDYHJO-UHFFFAOYSA-N dimethyl butane Natural products CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 4
• 238000005516 engineering process Methods 0.000 description 4
• 238000007306 functionalization reaction Methods 0.000 description 4
• 238000005227 gel permeation chromatography Methods 0.000 description 4
• 229910052736 halogen Inorganic materials 0.000 description 4
• 150000002367 halogens Chemical class 0.000 description 4
• QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 4
• 150000002642 lithium compounds Chemical class 0.000 description 4
• 238000004519 manufacturing process Methods 0.000 description 4
• 229910001507 metal halide Inorganic materials 0.000 description 4
• 125000004437 phosphorous atom Chemical group 0.000 description 4
• 239000000047 product Substances 0.000 description 4
• 229920003048 styrene butadiene rubber Polymers 0.000 description 4
• 125000001424 substituent group Chemical group 0.000 description 4
• 238000012360 testing method Methods 0.000 description 4
• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
• ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
• KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
• IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 3
• 239000006057 Non-nutritive feed additive Substances 0.000 description 3
• 239000005062 Polybutadiene Substances 0.000 description 3
• 239000004793 Polystyrene Substances 0.000 description 3
• BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 3
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
• 238000002679 ablation Methods 0.000 description 3
• 239000000654 additive Substances 0.000 description 3
• 125000003545 alkoxy group Chemical group 0.000 description 3
• 238000009835 boiling Methods 0.000 description 3
• 229910052799 carbon Inorganic materials 0.000 description 3
• 239000006231 channel black Substances 0.000 description 3
• 239000000460 chlorine Substances 0.000 description 3
• IJOOHPMOJXWVHK-UHFFFAOYSA-N chlorotrimethylsilane Chemical compound C[Si](C)(C)Cl IJOOHPMOJXWVHK-UHFFFAOYSA-N 0.000 description 3
• 238000010924 continuous production Methods 0.000 description 3
• 238000007334 copolymerization reaction Methods 0.000 description 3
• 125000004122 cyclic group Chemical group 0.000 description 3
• 150000002148 esters Chemical group 0.000 description 3
• 229910052732 germanium Inorganic materials 0.000 description 3
• GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical group [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 3
• 125000001841 imino group Chemical group [H]N=* 0.000 description 3
• 239000003112 inhibitor Substances 0.000 description 3
• 229910052747 lanthanoid Inorganic materials 0.000 description 3
• 150000002602 lanthanoids Chemical class 0.000 description 3
• 229910052751 metal Inorganic materials 0.000 description 3
• 150000002736 metal compounds Chemical class 0.000 description 3
• 150000005309 metal halides Chemical class 0.000 description 3
• 229910052752 metalloid Inorganic materials 0.000 description 3
• 239000003960 organic solvent Substances 0.000 description 3
• 229920002857 polybutadiene Polymers 0.000 description 3
• 229920002223 polystyrene Polymers 0.000 description 3
• 238000012545 processing Methods 0.000 description 3
• 238000011084 recovery Methods 0.000 description 3
• 229910000077 silane Inorganic materials 0.000 description 3
• OSNBTPSLVMAKGI-UHFFFAOYSA-N silyl pentanoate Chemical compound CCCCC(=O)O[SiH3] OSNBTPSLVMAKGI-UHFFFAOYSA-N 0.000 description 3
• 230000000087 stabilizing effect Effects 0.000 description 3
• 229920003051 synthetic elastomer Polymers 0.000 description 3
• KVNYFPKFSJIPBJ-UHFFFAOYSA-N 1,2-diethylbenzene Chemical compound CCC1=CC=CC=C1CC KVNYFPKFSJIPBJ-UHFFFAOYSA-N 0.000 description 2
• RXYPXQSKLGGKOL-UHFFFAOYSA-N 1,4-dimethylpiperazine Chemical compound CN1CCN(C)CC1 RXYPXQSKLGGKOL-UHFFFAOYSA-N 0.000 description 2
• HNRMPXKDFBEGFZ-UHFFFAOYSA-N 2,2-dimethylbutane Chemical compound CCC(C)(C)C HNRMPXKDFBEGFZ-UHFFFAOYSA-N 0.000 description 2
• SDJHPPZKZZWAKF-UHFFFAOYSA-N 2,3-dimethylbuta-1,3-diene Chemical compound CC(=C)C(C)=C SDJHPPZKZZWAKF-UHFFFAOYSA-N 0.000 description 2
• UWNADWZGEHDQAB-UHFFFAOYSA-N 2,5-dimethylhexane Chemical group CC(C)CCC(C)C UWNADWZGEHDQAB-UHFFFAOYSA-N 0.000 description 2
• RCJMVGJKROQDCB-UHFFFAOYSA-N 2-methylpenta-1,3-diene Chemical compound CC=CC(C)=C RCJMVGJKROQDCB-UHFFFAOYSA-N 0.000 description 2
• 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 2
• WBUSESIMOZDSHU-UHFFFAOYSA-N 3-(4,5-dihydroimidazol-1-yl)propyl-triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN1CCN=C1 WBUSESIMOZDSHU-UHFFFAOYSA-N 0.000 description 2
• CJSBUWDGPXGFGA-UHFFFAOYSA-N 4-methylpenta-1,3-diene Chemical compound CC(C)=CC=C CJSBUWDGPXGFGA-UHFFFAOYSA-N 0.000 description 2
• WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 2
• IEOFUVKZPDZCRI-UHFFFAOYSA-N CCCC(CC)(C(O)=O)[SiH](OC)OC Chemical compound CCCC(CC)(C(O)=O)[SiH](OC)OC IEOFUVKZPDZCRI-UHFFFAOYSA-N 0.000 description 2
• QVKYKDBLGJRAFR-UHFFFAOYSA-N CCCCCC(=O)O[Si](C1CCCC1)(C2CCCC2)C3CCCC3 Chemical compound CCCCCC(=O)O[Si](C1CCCC1)(C2CCCC2)C3CCCC3 QVKYKDBLGJRAFR-UHFFFAOYSA-N 0.000 description 2
• 239000004215 Carbon black (E152) Substances 0.000 description 2
• CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
• LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 description 2
• RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 2
• XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 2
• LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
• YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 2
• 244000043261 Hevea brasiliensis Species 0.000 description 2
• 239000002879 Lewis base Substances 0.000 description 2
• KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 description 2
• SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 2
• OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
• 241000220317 Rosa Species 0.000 description 2
• BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 2
• GCTFWCDSFPMHHS-UHFFFAOYSA-M Tributyltin chloride Chemical compound CCCC[Sn](Cl)(CCCC)CCCC GCTFWCDSFPMHHS-UHFFFAOYSA-M 0.000 description 2
• XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
• 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 2
• 125000003342 alkenyl group Chemical group 0.000 description 2
• 125000002877 alkyl aryl group Chemical group 0.000 description 2
• 239000002168 alkylating agent Substances 0.000 description 2
• 229940100198 alkylating agent Drugs 0.000 description 2
• 125000000304 alkynyl group Chemical group 0.000 description 2
• 150000001450 anions Chemical class 0.000 description 2
• 150000004945 aromatic hydrocarbons Chemical class 0.000 description 2
• 125000003710 aryl alkyl group Chemical group 0.000 description 2
• 125000004104 aryloxy group Chemical group 0.000 description 2
• 239000002585 base Substances 0.000 description 2
• HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 2
• 230000001588 bifunctional effect Effects 0.000 description 2
• 230000015572 biosynthetic process Effects 0.000 description 2
• 235000010290 biphenyl Nutrition 0.000 description 2
• 239000004305 biphenyl Substances 0.000 description 2
• GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 2
• 229910052794 bromium Inorganic materials 0.000 description 2
• DCFKHNIGBAHNSS-UHFFFAOYSA-N chloro(triethyl)silane Chemical compound CC[Si](Cl)(CC)CC DCFKHNIGBAHNSS-UHFFFAOYSA-N 0.000 description 2
• WZQSBCHNVPAYOC-UHFFFAOYSA-N chloro(trihexyl)silane Chemical compound CCCCCC[Si](Cl)(CCCCCC)CCCCCC WZQSBCHNVPAYOC-UHFFFAOYSA-N 0.000 description 2
• HZSATSWHBKSURR-UHFFFAOYSA-N chloro(trioctyl)silane Chemical compound CCCCCCCC[Si](Cl)(CCCCCCCC)CCCCCCCC HZSATSWHBKSURR-UHFFFAOYSA-N 0.000 description 2
• MNKYQPOFRKPUAE-UHFFFAOYSA-N chloro(triphenyl)silane Chemical compound C=1C=CC=CC=1[Si](C=1C=CC=CC=1)(Cl)C1=CC=CC=C1 MNKYQPOFRKPUAE-UHFFFAOYSA-N 0.000 description 2
• KQIADDMXRMTWHZ-UHFFFAOYSA-N chloro-tri(propan-2-yl)silane Chemical compound CC(C)[Si](Cl)(C(C)C)C(C)C KQIADDMXRMTWHZ-UHFFFAOYSA-N 0.000 description 2
• KOPOQZFJUQMUML-UHFFFAOYSA-N chlorosilane Chemical compound Cl[SiH3] KOPOQZFJUQMUML-UHFFFAOYSA-N 0.000 description 2
• 239000013068 control sample Substances 0.000 description 2
• 125000004465 cycloalkenyloxy group Chemical group 0.000 description 2
• 125000000753 cycloalkyl group Chemical group 0.000 description 2
• DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 2
• 230000007423 decrease Effects 0.000 description 2
• 238000004807 desolvation Methods 0.000 description 2
• 230000006866 deterioration Effects 0.000 description 2
• OSXYHAQZDCICNX-UHFFFAOYSA-N dichloro(diphenyl)silane Chemical compound C=1C=CC=CC=1[Si](Cl)(Cl)C1=CC=CC=C1 OSXYHAQZDCICNX-UHFFFAOYSA-N 0.000 description 2
• KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 2
• 230000009477 glass transition Effects 0.000 description 2
• 229910001385 heavy metal Inorganic materials 0.000 description 2
• 125000000623 heterocyclic group Chemical group 0.000 description 2
• 125000000743 hydrocarbylene group Chemical group 0.000 description 2
• 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
• 238000011065 in-situ storage Methods 0.000 description 2
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• 230000003993 interaction Effects 0.000 description 2
• 238000002955 isolation Methods 0.000 description 2
• 150000007527 lewis bases Chemical class 0.000 description 2
• WGOPGODQLGJZGL-UHFFFAOYSA-N lithium;butane Chemical compound [Li+].CC[CH-]C WGOPGODQLGJZGL-UHFFFAOYSA-N 0.000 description 2
• 239000000463 material Substances 0.000 description 2
• UAEPNZWRGJTJPN-UHFFFAOYSA-N methylcyclohexane Chemical compound CC1CCCCC1 UAEPNZWRGJTJPN-UHFFFAOYSA-N 0.000 description 2
• GDOPTJXRTPNYNR-UHFFFAOYSA-N methylcyclopentane Chemical compound CC1CCCC1 GDOPTJXRTPNYNR-UHFFFAOYSA-N 0.000 description 2
• JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 2
• 239000003607 modifier Substances 0.000 description 2
• 229920003052 natural elastomer Polymers 0.000 description 2
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• QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
• BKIMMITUMNQMOS-UHFFFAOYSA-N nonane Chemical compound CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 description 2
• TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
• 239000012766 organic filler Substances 0.000 description 2
• 150000002902 organometallic compounds Chemical class 0.000 description 2
• 239000003208 petroleum Substances 0.000 description 2
• ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
• 229920001195 polyisoprene Polymers 0.000 description 2
• 230000002028 premature Effects 0.000 description 2
• 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 2
• 230000003014 reinforcing effect Effects 0.000 description 2
• 239000011347 resin Substances 0.000 description 2
• 229920005989 resin Polymers 0.000 description 2
• 238000010058 rubber compounding Methods 0.000 description 2
• 238000012216 screening Methods 0.000 description 2
• 241000894007 species Species 0.000 description 2
• 239000000126 substance Substances 0.000 description 2
• 125000003107 substituted aryl group Chemical group 0.000 description 2
• 125000005346 substituted cycloalkyl group Chemical group 0.000 description 2
• 239000005061 synthetic rubber Substances 0.000 description 2
• YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
• LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 2
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