JP2013256476A - Solubilized cosmetic - Google Patents

Solubilized cosmetic Download PDF

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JP2013256476A
JP2013256476A JP2012134612A JP2012134612A JP2013256476A JP 2013256476 A JP2013256476 A JP 2013256476A JP 2012134612 A JP2012134612 A JP 2012134612A JP 2012134612 A JP2012134612 A JP 2012134612A JP 2013256476 A JP2013256476 A JP 2013256476A
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cosmetic
oil
fatty acid
solubilized
acid ester
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JP2013256476A5 (en
JP6088158B2 (en
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Masumi Komoriya
真澄 小森谷
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Pola Chemical Industries Inc
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Abstract

PROBLEM TO BE SOLVED: To provide a solubilized cosmetic, excellent in transparency and stably solubilizing an aqueous plant extract.SOLUTION: A solubilized cosmetic contains 0.5-5 mass% of a polyglycerol fatty acid ester; wherein the polyglycerol fatty acid ester is preferably a polyglyceryl diisostearate having an average glycerol polymerization degree of 3. The solubilized cosmetic such as a cosmetic material with excellent transparency for a treatment oil, a cleansing oil and the like which is capable of stably solubilizing an aqueous plant extract can be provided.

Description

本発明は、可溶化型化粧料に関するものである。   The present invention relates to a solubilized cosmetic.

可溶化型化粧料は、フレグランスあるいは油性の有効成分を溶かす溶剤としての機能と、皮膚上に水分散逸防止膜を形成するエモリエント機能との2つの機能を併せ持つ。さらに、このような可溶化型化粧料のエモリエント機能に加えて、モイスチャー機能も付与する目的で、そのような機能を有する植物抽出エキスのような水溶性成分を可溶化することが試みられてきており、可溶化にイソステアロイル加水分解コラーゲン塩とオレイン酸ジグリセリルを用いることが知られている(例えば、特許文献1を参照)。しかしながら、イソステアロイル加水分解コラーゲン塩は、牛血液抽出エキスや酵母抽出エキスといった、動物由来の抽出エキスに対しては可溶化効果が高いものの、より安全性の高い水溶性の植物抽出エキスに対しては可溶化効果が高くないといった課題が残った。   Solubilized cosmetics have two functions: a function as a solvent that dissolves a fragrance or an oily active ingredient, and an emollient function that forms a water dispersion prevention film on the skin. Furthermore, in addition to the emollient function of such a solubilized cosmetic, an attempt has been made to solubilize a water-soluble component such as a plant extract having such a function for the purpose of imparting a moisture function. In addition, it is known to use isostearoyl hydrolyzed collagen salt and diglyceryl oleate for solubilization (see, for example, Patent Document 1). However, isostearoyl hydrolyzed collagen salt is highly soluble in animal-derived extracts such as bovine blood extract and yeast extract, but is safer than water-soluble plant extract. The problem remains that the solubilizing effect is not high.

特開H03−68504号公報JP H03-68504 A

本発明は、水溶性の植物抽出エキスを安定に可溶化する、透明性に優れた可溶化型化粧料を提供することを課題とする。   It is an object of the present invention to provide a solubilized cosmetic material that is capable of stably solubilizing a water-soluble plant extract and having excellent transparency.

このような状況に鑑みて、本発明者らは鋭意研究した結果、ポリグリセリン脂肪酸エステルを含有せしめることにより、水溶性の植物抽出エキスを安定に可溶化する、透明性に優れた可溶化型化粧料を見出し、本発明を完成させた。すなわち本発明の可溶化型化粧料は、以下に示すとおりである。
(1)ポリグリセリン脂肪酸エステルを含有することを特徴とする、可溶化型化粧料。
(2)前記ポリグリセリン脂肪酸エステルが、ジイソステアリン酸ポリグリセリルであることを特徴とする、(1)に記載の可溶化型化粧料。
(3)前記ポリグリセリン脂肪酸エステルを、化粧料全体に対して、0.5質量%〜5質量%含有することを特徴とする、(1)又は(2)に記載の可溶化型化粧料。
In view of such a situation, the present inventors have intensively studied, and as a result, by incorporating a polyglycerin fatty acid ester, a water-soluble plant extract can be stably solubilized and solubilized makeup with excellent transparency. The materials were found and the present invention was completed. That is, the solubilized cosmetic of the present invention is as follows.
(1) A solubilized cosmetic comprising a polyglycerol fatty acid ester.
(2) The solubilized cosmetic according to (1), wherein the polyglycerin fatty acid ester is polyglyceryl diisostearate.
(3) The solubilized cosmetic according to (1) or (2), wherein the polyglycerin fatty acid ester is contained in an amount of 0.5% by mass to 5% by mass with respect to the entire cosmetic.

本発明によれば、水溶性の植物抽出エキスを安定に可溶化する、透明性に優れた可溶化型化粧料を提供することができる。 ADVANTAGE OF THE INVENTION According to this invention, the solubilization-type cosmetics excellent in transparency which can solubilize a water-soluble plant extract stably can be provided.

<本発明のポリグリセリン脂肪酸エステル>
本発明の可溶化型化粧料は、必須成分としてポリグリセリン脂肪酸エステルを含有することを特徴とする。かかる成分は、水溶性の植物抽出エキスを可溶化せしめ、高い透明性を付与する作用を有する。前記ポリグリセリン脂肪酸エステルの脂肪酸残基としては、炭素数10〜18の直鎖、分岐又は環状構造を有するものが好ましく例示できる。このような脂肪酸残基としては、例えば、ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、イソステアリン酸等が好ましく例示できる。これらの中ではイソステアリン酸が特に好ましい。又、ポリグリセリンとしては、グリセリンの平均重合度が2〜9のものが好ましく、3〜5のものが特に好ましい。かかるポリグリセリンのフリーの水酸基の内、前記脂肪酸残基で修飾されるものは半分以下であることが好ましい。具体的には、本発明の可溶化型化粧料においては、平均重合度が3のジイソステアリン酸ポリグリセリルが好ましく例示できる。かかる成分は、市販されているものを使用することもできる。このようなポリグリセリン脂肪酸エステルとしては、高級アルコール工業株式会社製の「リソレックスPGIS32」等が好ましく例示される。本発明の可溶化型化粧料においては、かかる成分は化粧料全体に対して0.5質量%〜5質量%が好ましく含有され、より好ましくは1質量%〜3質量%含有される。この範囲を外れると、水溶性の植物抽出エキスの可溶化の安定性が著しく低下する。
<Polyglycerin fatty acid ester of the present invention>
The solubilized cosmetic of the present invention is characterized by containing a polyglycerol fatty acid ester as an essential component. Such components have the effect of solubilizing water-soluble plant extract and imparting high transparency. Preferred examples of the fatty acid residue of the polyglycerin fatty acid ester include those having a linear, branched or cyclic structure having 10 to 18 carbon atoms. Preferred examples of such fatty acid residues include lauric acid, myristic acid, palmitic acid, stearic acid, and isostearic acid. Of these, isostearic acid is particularly preferred. As the polyglycerol, those having an average degree of polymerization of glycerol of 2 to 9 are preferable, and those of 3 to 5 are particularly preferable. Among the free hydroxyl groups of polyglycerin, those modified with the fatty acid residue are preferably less than half. Specifically, in the solubilized cosmetic of the present invention, polyglyceryl diisostearate having an average degree of polymerization of 3 can be preferably exemplified. As this component, a commercially available product can be used. As such a polyglycerin fatty acid ester, “Risolex PGIS32” manufactured by Higher Alcohol Industry Co., Ltd. is preferably exemplified. In the solubilized cosmetic of the present invention, the component is preferably contained in an amount of 0.5 to 5% by mass, more preferably 1 to 3% by mass, based on the entire cosmetic. Outside this range, the solubilization stability of the water-soluble plant extract is significantly reduced.

本発明の可溶化型化粧料としては、トリートメントオイル化粧料、オイルクレンジング化粧料等が例示されるが、これらに限定されるものではない。トリートメントオイル化粧料の長所としては、特に水溶性物質の有効性成分による保温効果の向上が挙げられる。また、オイルクレンジング化粧料の長所としては、特に、可溶化水が含まれることになるウオッシュオフ性(すすぎやすさ)の向上が挙げられる。本発明の可溶化型化粧料においては、前記必須成分以外に、化粧品で通常使用されている任意成分を本発明の効果を損なわない範囲において、含有することができる。 Examples of the solubilized cosmetic of the present invention include, but are not limited to, treatment oil cosmetics and oil cleansing cosmetics. As an advantage of the treatment oil cosmetic, there is an improvement in the heat retaining effect due to the effective component of the water-soluble substance. In addition, as an advantage of the oil cleansing cosmetic, in particular, an improvement in wash-off property (ease of rinsing) in which solubilized water is contained can be mentioned. In the solubilized cosmetic of the present invention, in addition to the essential components, optional components usually used in cosmetics can be contained within a range that does not impair the effects of the present invention.

このような任意成分としては、例えば、マカデミアナッツ油、アボカド油、トウモロコシ油、オリーブ油、ナタネ油、ゴマ油、ヒマシ油、サフラワー油、綿実油、ホホバ油、ヤシ油、パーム油、液状ラノリン、硬化ヤシ油、硬化油、モクロウ、硬化ヒマシ油、ミツロウ、キャンデリラロウ、カルナウバロウ、イボタロウ、ラノリン、還元ラノリン、硬質ラノリン、ホホバロウ等のオイル、ワックス類、流動パラフィン、スクワラン、プリスタン、オゾケライト、パラフィン、セレシン、ワセリン、マイクロクリスタリンワックス等の炭化水素類、オレイン酸、イソステアリン酸、ラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、ベヘン酸、ウンデシレン酸等の高級脂肪酸類、セチルアルコール、ステアリルアルコール、イソステアリルアルコール、ベヘニルアルコール、オクチルドデカノール、ミリスチルアルコール、セトステアリルアルコール等の高級アルコール等、炭酸ジエステル、イソオクタン酸セチル、ミリスチン酸イソプロピル、イソステアリン酸ヘキシルデシル、アジピン酸ジイソプロピル、セバチン酸ジ−2−エチルヘキシル、乳酸セチル、リンゴ酸ジイソステアリル、ジ−2−エチルヘキサン酸エチレングリコール、ジカプリン酸ネオペンチルグリコール、ジ−2−ヘプチルウンデカン酸グリセリン、トリ−2−エチルヘキサン酸グリセリン、トリ−2−エチルヘキサン酸トリメチロールプロパン、トリイソステアリン酸トリメチロールプロパン、テトラ−2−エチルヘキサン酸ペンタンエリトリット等の合成エステル油類、ジメチルポリシロキサン、メチルフェニルポリシロキサン、ジフェニルポリシロキサン等の鎖状ポリシロキサン、オクタメチルシクロテトラシロキサン、デカメチルシクロペンタシロキサン、ドデカメチルシクロヘキサンシロキサン等の環状ポリシロキサン、アミノ変性ポリシロキサン、ポリエーテル変性ポリシロキサン、アルキル変性ポリシロキサン、フッ素変性ポリシロキサン等の変性ポリシロキサン等のシリコーン油等の油剤類、脂肪酸セッケン(ラウリン酸ナトリウム、パルミチン酸ナトリウム等)、ラウリル硫酸カリウム、アルキル硫酸トリエタノールアミンエーテル等のアニオン界面活性剤類、塩化ステアリルトリメチルアンモニウム、塩化ベンザルコニウム、ラウリルアミンオキサイド等のカチオン界面活性剤類、イミダゾリン系両性界面活性剤(2−ココイル−2−イミダゾリニウムヒドロキサイド−1−カルボキシエチロキシ2ナトリウム塩等)、ベタイン系界面活性剤(アルキルベタイン、アミドベタイン、スルホベタイン等)、アシルメチルタウリン等の両性界面活性剤類、ソルビタン脂肪酸エステル類(ソルビタンモノステアレート、セスキオレイン酸ソルビタン等)、グリセリン脂肪酸類(モノステアリン酸グリセリン等)、プロピレングリコール脂肪酸エステル類(モノステアリン酸プロピレングリコール等)、硬化ヒマシ油誘導体、グリセリンアルキルエーテル、POEソルビタン脂肪酸エステル類(POEソルビタンモノオレエート、モノステアリン酸ポリオキシエチレンソルビタン等)、POEソルビット脂肪酸エステル類(POE−ソルビットモノラウレート等)、POEグリセリン脂肪酸エステル類(POE−グリセリンモノイソステアレート等)、POE脂肪酸エステル類(ポリエチレングリコールモノオレート、POEジステアレート等)、POEアルキルエーテル類(POE2−オクチルドデシルエーテル等)、POEアルキルフェニルエーテル類(POEノニルフェニルエーテル等)、プルロニック型類、POE・POPアルキルエーテル類(POE・POP2−デシルテトラデシルエーテル等)、テトロニック類、POEヒマシ油・硬化ヒマシ油誘導体(POEヒマシ油、POE硬化ヒマシ油等)、ショ糖脂肪酸エステル、アルキルグルコシド等の非イオン界面活性剤類、ポリエチレングリコール、グリセリン、1,3−ブタンジオール、エリスリトール、ソルビトール、キシリトール、マルチトール、プロピレングリコール、ジプロピレングリコール、ジグリセリン、イソプレングリコール、1,2−ペンタンジオール、2,4−ヘキシレングリコール、1,2−ヘキサンジオール、1,2−オクタンジオール等の多価アルコール類、α-トコフェロール等の脂溶性ビタミン等が好ましく例示できる。 Examples of such optional ingredients include macadamia nut oil, avocado oil, corn oil, olive oil, rapeseed oil, sesame oil, castor oil, safflower oil, cottonseed oil, jojoba oil, coconut oil, palm oil, liquid lanolin, and hardened coconut oil. Oil, wax, liquid paraffin, squalane, pristane, ozokerite, paraffin, ceresin, petrolatum, oil, wax, liquid wax, liquid paraffin, squalane, bean wax, candelilla wax, carnauba wax, ibotarou, lanolin, reduced lanolin, hard lanolin, jojoba wax , Hydrocarbons such as microcrystalline wax, higher fatty acids such as oleic acid, isostearic acid, lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, undecylenic acid, cetyl alcohol, stearyl alcohol, isostear Alcohol, behenyl alcohol, octyldodecanol, higher alcohol such as myristyl alcohol, cetostearyl alcohol, carbonic acid diester, cetyl isooctanoate, isopropyl myristate, hexyldecyl isostearate, diisopropyl adipate, di-2-ethylhexyl sebacate, lactic acid Cetyl, diisostearyl malate, ethylene glycol di-2-ethylhexanoate, neopentyl glycol dicaprate, glycerin di-2-heptylundecanoate, glycerin tri-2-ethylhexanoate, tri-2-ethylhexanoate tri Synthetic ester oils such as methylolpropane, trimethylolpropane triisostearate, pentane erythritol tetra-2-ethylhexanoate, dimethylpolysiloxane, Chain polysiloxane such as tilphenyl polysiloxane, diphenyl polysiloxane, cyclic polysiloxane such as octamethylcyclotetrasiloxane, decamethylcyclopentasiloxane, dodecamethylcyclohexanesiloxane, amino-modified polysiloxane, polyether-modified polysiloxane, alkyl-modified Oil agents such as silicone oil such as polysiloxane, modified polysiloxane such as fluorine-modified polysiloxane, fatty acid soap (sodium laurate, sodium palmitate, etc.), potassium lauryl sulfate, alkylsulfuric acid triethanolamine ether, etc. , Cationic surfactants such as stearyltrimethylammonium chloride, benzalkonium chloride, laurylamine oxide, imidazoline-based amphoteric surfactants (2-copolymers) Coil-2-imidazolinium hydroxide-1-carboxyethyloxy disodium salt, etc.), betaine surfactants (alkyl betaines, amide betaines, sulfobetaines, etc.), amphoteric surfactants such as acylmethyltaurine, sorbitan Fatty acid esters (such as sorbitan monostearate, sorbitan sesquioleate), glycerin fatty acids (such as glyceryl monostearate), propylene glycol fatty acid esters (such as propylene glycol monostearate), hydrogenated castor oil derivatives, glycerin alkyl ethers, POE sorbitan fatty acid esters (POE sorbitan monooleate, polyoxyethylene sorbitan monostearate, etc.), POE sorbite fatty acid esters (POE-sorbite monolaurate, etc.), PO Glycerin fatty acid esters (such as POE-glycerin monoisostearate), POE fatty acid esters (such as polyethylene glycol monooleate and POE distearate), POE alkyl ethers (such as POE2-octyldodecyl ether), POE alkylphenyl ethers (POE) Nonylphenyl ether, etc.), Pluronic types, POE / POP alkyl ethers (POE / POP2-decyltetradecyl ether, etc.), Tetronics, POE castor oil / hardened castor oil derivatives (POE castor oil, POE hardened castor oil, etc.) ), Nonionic surfactants such as sucrose fatty acid ester and alkyl glucoside, polyethylene glycol, glycerin, 1,3-butanediol, erythritol, sorbitol, xylitol, maltitol Polyhydric alcohols such as styrene, propylene glycol, dipropylene glycol, diglycerin, isoprene glycol, 1,2-pentanediol, 2,4-hexylene glycol, 1,2-hexanediol, 1,2-octanediol, Preferred examples include fat-soluble vitamins such as α-tocopherol.

以下に実施例を示して本発明について更に詳細に説明を加えるが、本発明は、これらの実施例にのみ限定を受けないことはいうまでもない。 Hereinafter, the present invention will be described in more detail with reference to examples. However, it goes without saying that the present invention is not limited to these examples.

下記に示す表1の処方に従って、実施例1〜3として、本発明の可溶化型化粧料である、トリートメントオイル化粧料及び比較例1〜5を作製した。即ち、イを秤込み40℃に加熱溶解する。ロを秤込み室温にて均一に溶解する。室温にて撹拌しながらロをイに徐々に加えていき、トリートメントオイル化粧料を得た。   Treatment oil cosmetics and Comparative Examples 1 to 5, which are solubilized cosmetics of the present invention, were prepared as Examples 1 to 3 in accordance with the formulations shown in Table 1 below. That is, a is weighed and dissolved by heating at 40 ° C. Weigh and dissolve uniformly at room temperature. While stirring at room temperature, ro was gradually added to i to obtain a treatment oil cosmetic.

Figure 2013256476
Figure 2013256476

<試験例>
本発明のトリートメントオイル化粧料と、比較例について、安定性及び透明性の比較試験を実施した。安定性試験については、各化粧料を5、20、40℃に1ヶ月間放置し、分離・沈殿の有無を肉眼観察した。分離も沈殿もない場合を○、少量の分離、沈殿がある場合を△、完全に分離がある場合を×で評価した。透明性試験については、各化粧料を40℃に3日間放置後、上下に30回振動させたものを肉眼観察した。結果を下記の表2に示すが、本発明の可溶化型化粧料であるトリートメントオイル化粧料は、比較例に比べて安定性、透明性に優れていることが判る。
<Test example>
A comparative test of stability and transparency was performed on the treatment oil cosmetic of the present invention and a comparative example. For the stability test, each cosmetic was left at 5, 20, and 40 ° C. for 1 month, and the presence or absence of separation / precipitation was visually observed. The case where there was neither separation nor precipitation was evaluated as ◯, the case where there was a small amount of separation, the case where there was precipitation, Δ, and the case where there was complete separation was evaluated as ×. For the transparency test, each cosmetic was left to stand at 40 ° C. for 3 days, and was then visually observed after being vibrated up and down 30 times. The results are shown in Table 2 below, and it can be seen that the treatment oil cosmetic which is the solubilized cosmetic of the present invention is superior in stability and transparency as compared with the comparative example.

Figure 2013256476
Figure 2013256476

下記に示す表3の処方に従って、実施例4として、本発明の可溶化型化粧料である、オイルクレンジング化粧料を作製した。即ち、イを秤込み40℃に加熱溶解する。ロを秤込み室温にて均一に溶解する。室温にて撹拌しながらロをイに徐々に加えていき、オイルクレンジング化粧料を得た。さらに、前記試験例と同様の評価を行った結果を表4に示すが、本発明の可溶化型化粧料であるオイルクレンジング化粧料は、安定性、透明性に優れていることが判る。   In accordance with the formulation shown in Table 3 below, as Example 4, an oil cleansing cosmetic that is a solubilized cosmetic of the present invention was prepared. That is, a is weighed and dissolved by heating at 40 ° C. Weigh and dissolve uniformly at room temperature. While stirring at room temperature, ro was gradually added to i to obtain an oil cleansing cosmetic. Furthermore, the results of the same evaluation as in the test example are shown in Table 4. It can be seen that the oil cleansing cosmetic which is the solubilized cosmetic of the present invention is excellent in stability and transparency.

Figure 2013256476
Figure 2013256476

Figure 2013256476
Figure 2013256476

Claims (3)

ポリグリセリン脂肪酸エステルを含有することを特徴とする、可溶化型化粧料。 A solubilized cosmetic comprising a polyglycerol fatty acid ester. 前記ポリグリセリン脂肪酸エステルが、ジイソステアリン酸ポリグリセリルであることを特徴とする、請求項1に記載の可溶化型化粧料。 The solubilized cosmetic according to claim 1, wherein the polyglycerin fatty acid ester is polyglyceryl diisostearate. 前記ポリグリセリン脂肪酸エステルを、化粧料全体に対して、0.5質量%〜5質量%含有することを特徴とする、請求項1又は2に記載の可溶化型化粧料。 The solubilized cosmetic according to claim 1 or 2, wherein the polyglycerin fatty acid ester is contained in an amount of 0.5% by mass to 5% by mass with respect to the entire cosmetic.
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JPS5910505A (en) * 1982-07-07 1984-01-20 Nisshin Oil Mills Ltd:The Oily beautifying cosmetic
JPH0368504A (en) * 1989-08-08 1991-03-25 Pola Chem Ind Inc Soluble cosmetic
JP2002179526A (en) * 2000-12-08 2002-06-26 Sakamoto Yakuhin Kogyo Co Ltd Gel-shaped cleansing cosmetic
JP2004075566A (en) * 2002-08-12 2004-03-11 Kao Corp Cleansing cosmetic
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