JP2011527955A - 複数層複合体を連続的に製造するための方法 - Google Patents
複数層複合体を連続的に製造するための方法 Download PDFInfo
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- JP2011527955A JP2011527955A JP2011517899A JP2011517899A JP2011527955A JP 2011527955 A JP2011527955 A JP 2011527955A JP 2011517899 A JP2011517899 A JP 2011517899A JP 2011517899 A JP2011517899 A JP 2011517899A JP 2011527955 A JP2011527955 A JP 2011527955A
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
(B)少なくとも1層の結合層、及び
(C)その層厚さ全体を通る毛細管を含む、少なくとも1層のポリウレタン層、
を含む複数層の複合体を連続的に製造するための方法であって、
型を使用してポリウレタン層(C)を製造し、及び前記結合層(B)に変換される材料を使用して、前記ポリウレタン層(C)を、前記支持体材料(A)の上に取り付けることを含み、前記型は、80〜170℃の温度を有し、及び熱容量が100〜20000J/K・m2の範囲であることを特徴とする方法。
【選択図】なし
Description
(A)少なくとも1つの支持体材料、
(B)少なくとも1層の結合層、及び
(C)その層厚さ全体を通る毛細管を含む、少なくとも1層のポリウレタン層、
を含む複数層の複合体を連続的に製造するための方法であって、
型を使用してポリウレタン層(C)を製造し、及び前記結合層(B)に変換される材料を使用して、前記ポリウレタン層(C)を、前記支持体材料(A)の上に取り付けることを含み、前記型は、80〜170℃の温度を有し、及び熱容量が100〜20000J/K・m2の範囲の伝熱媒体を含む、ことを特徴とする方法に関する。
(A)少なくとも1種の支持体材料、
を含む。
好ましくは、水性のポリウレタン分散物が、伝熱媒体によって予備加熱された型に施され、水性相、好ましくは水が蒸発され、そして次にポリウレタンフィルム(C)が、支持体材料(A)に移される。
1)適切であれば、添加剤及び/又は助剤材料を含んだ液体バインダーを、パターン化された表面、例えば、他の型又はオリジナルのパターンに施す工程、
2)バインダーを、例えば、熱硬化、放射硬化によって、又はエージングさせることによって硬化させる工程、
3)このようにして得ることができる構造化された媒体を分離し、及び適切であれば、これを支持体、例えば金属プレート又は金属シリンダーに施す工程、
4)任意に、このようにして得ることができる、複数の比較的小さい型を結合して、比較的長い型、特にシリコーンストリップを形成する工程。
1)レーザー彫刻可能な層、又はレーザー彫刻可能な層を支持体の上に含む積層複合体を提供する工程(レーザー彫刻可能な層は、層、及び好ましくは添加剤と助剤材料も含む)、
2)熱化学的、光化学的、又は化学線的にレーザー彫刻可能な層を硬化処理(アンプリフィケーション:amplification)する工程、
3)レーザーを使用して、レーザー彫刻可能な層に、表面−構造化された被覆物の表面構造に対応する表面構造を彫刻する工程、
4)任意に、レーザー彫刻した層の端部を継ぎ目無しに結合する工程。
−型に、好ましくは水性のポリウレタン分散物を、施すこと、特に吹き付けること、
−適切であれば、硬化して結合層(B)に変換する材料を、ポリウレタン層(C)及び/又は支持体材料(A)に施すこと、
−ポリウレタン層(C)を、適切であれば、結合層(B)に変換する材料と一緒に、支持体層(A)に移すこと、
−支持体層(A)、結合層(B)に変換する材料、及びポリウレタン層(C)を一緒に、例えば熱的に、化学線の放射により、又は圧力により、又はこれらの2種以上の組み合わせによって、固定すること、及び/又は
−このようにして製造された複数層の複合体を取り出すこと、
のための1つ以上の手段を有する。
(a)イソシアネート、好ましくはジイソシアネート、と
(b)典型的には、分子量(モル質量)(Mw)が、500〜10000g/molの範囲、好ましくは500〜5000g/molの範囲、及びより好ましくは800〜3000g/molの範囲の、イソシアネート反応性化合物、及び
(c)分子量が50〜499g/molの範囲の鎖延長剤を、適切であれば、
(d)触媒、
(e)及び/又は通常の添加剤、の存在下に、
反応させることによって製造される。
イソシアネート(a)として、公知の脂肪族、脂環式、アラリファティック、及び/又は芳香族イソシアネート、例えばトリ−、テトラ−、ペンタ−、ヘキサ−、ヘプタ−及び/又はオクタメチレンジイソシアネート、2−メチルペンタメチレン1,5−ジイソシアネート、2−エチルブチレン1,4−ジイソシアネート、ペンタメチレン1,5−ジイソシアネート、ブチレン1,4−ジイソシアネート、1−シソシアナート−3,3,5−トリメチル−5−イソシアナートメチルシクロヘキサン(イソホロンジイソシアネート、IPDI)、1,4−及び/又は1,3−ビス(イソシアナートメチル)シクロヘキサン(HXDI)、1,4−シクロヘキサンジイソシアネート、1−メチル−2,4−及び/又は−2,6−シクロヘキサンジイソシアネート及び/又は4,4’−、2,4’−及び2,2’−ジシクロヘキシルメタンジイソシアネート、2,2−、2,4−及び/又は4,4−ジフェニルメタンジイソシアネート(MDI)、1,5−ナフチレンジイソシアネート(NDI)、2,4−及び/又は2,6−トリレンジイソシアネート(TDI)、ジフェニルメタンジイソシアネート、3,3−ジメチルビフェニルジイソシアネート、1,2−ジフェニルエタンジイソシアネート、及び/又はフェニレンジイソシアネートを使用しても良い。4,4’−MDIが好ましい。好ましいものは、また、脂肪族ジイソシアネート、特にヘキサメチレンジイソシアネート(HDI)、及び特に好ましくは芳香族ジイソシアネート、例えば2,2−、2,4−及び/又は4,4−ジフェニルメタンジイソシアネート(MDI)及び上述した異性体の混合物である。
但し、
A1が、2〜20個の炭素原子を有するスペーサーで、アリーレン、無置換の、又は1〜4個のC1−C4−アルキル基で置換された、アルキレン、及びシクロアルキレン、例えばシクロヘキセンから選ばれる)。好ましいスペーサーA1は、フェニレン、特に、パラ−フェニレン、及びトリレン、特にパラ−トリレン、及びC2−C12−アルキレン、例えば、エチレン(CH2CH2)、及び−(CH2)3−、−(CH2)4−、−(CH2)5−、−(CH2)6−、−(CH2)8−、−(CH2)10−、−(CH2)12−である。
Xは、O(AO)xR6であり、
ここで、
AOは、C2−C4−アルキレンオキシド、例えばブチレンオキシド、特に、エチレンオキシド(CH2CH2O)、又はプロピレンオキシド(CH(CH3)CH2O)又は(CH2CH(CH3)O)であり、
xは、1〜50の整数、好ましくは5〜25の整数であり、及び
R6は、水素、及びC1−C30−アルキルから選ばれ、特に、C1−C10−アルキル、例えば、メチル、エチル、n−プロピル、イソプロピル、n−ブチル、イソブチル、sec−ブチル、tert−ブチル、n−ペンチル、イソペンチル、sec−ペンチル、ネオペンチル、1,2−ジメチルプロピル、イソアミル、n−ヘキシル、イソヘキシル、sec−ヘキシル、n−ヘプチル、n−オクチル、2−エチルヘキシル、n−ノニル、n−デシル、より好ましくはC1−C4−アルキル、例えば、メチル、エチル、n−プロピル、イソプロピル、n−ブチル、イソブチル、sec−ブチル、及びtert−ブチルから選ばれる。
(f)反応性の基を有するシリコーン化合物(シリコーン化合物(f)とも称される)、
を含んでも良い。
−NH−CH2−CH2−NH2基、−NH−CH2−CH2−CH2−NH2基、−NH−CH2−CH2−NH(C2H5)基、−NH−CH2−CH2−CH2−NH(C2H5)基、−NH−CH2−CH2−NH(CH3)基、−NH−CH2−CH2−CH2−NH(CH3)基である。
全体で、20質量%〜30質量%のポリウレタン(PU)、又は全体で20質量%〜30質量%のポリウレタン(PU1)と(PU2)、
1質量%〜10質量%の、好ましくは2質量%〜5質量%の硬化剤、
1質量%〜10質量%のシリコーン化合物(f)、
0〜10質量%、好ましくは0.5〜5質量%のポリジアルキルシロキサン(g)、
を含む。
10質量%〜30質量%のポリウレタン(PU1)、
0質量%〜20質量%のポリウレタン(PU2)、
を含む。
熱容量が100〜20000J/K・m2の範囲の型、好ましくはシリコーン型(これらの型は、少なくとも2個のローラーの上に存在し、そしてこれらは、型を無限ループにターンさせることができる)、
好ましくは水性のポリウレタン分散物を、好ましくは型に吹き付けて施す、少なくとも1個のアプリケーター(供給器)(この水性分散物は、ポリウレタン層(C)を形成する)、
適切であれば、硬化して結合層(B)に変換する材料を施す(供給する)ことができ、特に吹き付けることができる、少なくとも1個のアプリケーター、
硬化して結合層(B)に変換する材料を有する、又は有しない支持体層(A)を、ポリウレタン層(C)に移す、少なくとも1個のユニット、
支持体材料(A)、結合層(B)に変換する材料、及びポリウレタン層(C)を、例えば熱的に、化学線放射を介して、又は圧力によって、又は上述した方法の、すくなくとも2種の組み合わせによって、一緒に固定するユニット、
本発明に従い製造された複数層の複合体を取り出すための装置(デバイス)、
適切であれば、結合層に変換可能な材料を、ポリウレタン層(C)上に施すためのユニット、
を含む。
Claims (12)
- (A)少なくとも1つの支持体材料、
(B)少なくとも1層の結合層、及び
(C)その層厚さ全体を通る毛細管を含む、少なくとも1層のポリウレタン層、
を含む複数層の複合体を連続的に製造するための方法であって、
型を使用してポリウレタン層(C)を製造し、及び前記結合層(B)に変換される材料を使用して、前記ポリウレタン層(C)を、前記支持体材料(A)の上に取り付けることを含み、前記型は、80〜170℃の温度を有し、及び熱容量が100〜20000J/K・m2の範囲であることを特徴とする方法。 - 前記複合体が、通気性の複合体であることを特徴とする請求項1に記載の方法。
- 前記型がシリコーン型又はシリコーン被覆材料であることを特徴とする請求項1又は2の何れかに記載の方法。
- 前記型が、伝熱媒体を含むことを特徴とする請求項1〜3の何れか1項に記載の方法。
- 前記伝熱材料が、加熱された金属体及び熱容量が高い金属体から選ばれることを特徴とする請求項4に記載の方法。
- 前記伝熱媒体が、型に一体化した金属であることを特徴とする請求項4又は5の何れかに記載の方法。
- 前記ポリウレタン層(C)が少なくとも2種のポリウレタンから構成されていることを特徴とする請求項1〜5の何れか1項に記載の方法。
- 前記支持体層(A)が、革、人工革、金属又はプラスチックホイル、テキスタイル、及びセルロース材料から選ばれることを特徴とする請求項1〜6の何れか1項に記載の方法。
- 少なくとも1層の中間層(D)が連続的に挿入され、中間層(D)の材料が、前記支持体材料(A)とは異なることを特徴とする請求項1〜7の何れか1項に記載の方法。
- 前記ポリウレタン層(C)が、少なくとも1種のポリウレタンの少なくとも1種の水性処方物を使用して製造されることを特徴とする請求項1〜8の何れか1項に記載の方法。
- 型を無限ループ内に回転させることができるように備えられた、少なくとも2個のローラー上に存在する、100〜20000J/K・m2の範囲の熱容量を有する、伝熱媒体を有する型、
ポリウレタン層(C)を形成する水性ポリウレタン分散物を前記型の上に吹き付けることができる、少なくとも1個の供給器、
硬化して結合層(B)を形成可能な材料を有するか又は有しない支持体材料(A)を、ポリウレタン層(C)に移す、少なくとも1個のユニット、
支持体材料(A)、結合層(B)を形成する材料、及びポリウレタン層(C)を一緒に固定するユニット、
本発明に従い製造された複数層複合体を取り出すためのデバイス、
任意に、結合層(B)に変換可能な材料を、ポリウレタン層(C)の上に施すためのユニット、
を含む装置。 - 請求項1〜9の何れか1項に記載の方法を行うために、請求項10に記載の装置を使用する方法。
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WO2010007042A1 (de) | 2010-01-21 |
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