JP2011105658A5 - - Google Patents
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- Publication number
- JP2011105658A5 JP2011105658A5 JP2009263316A JP2009263316A JP2011105658A5 JP 2011105658 A5 JP2011105658 A5 JP 2011105658A5 JP 2009263316 A JP2009263316 A JP 2009263316A JP 2009263316 A JP2009263316 A JP 2009263316A JP 2011105658 A5 JP2011105658 A5 JP 2011105658A5
- Authority
- JP
- Japan
- Prior art keywords
- group
- reaction
- bonded
- ethyl
- ring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 6
- -1 difluoromethylene group Chemical group 0.000 description 4
- SNHMUERNLJLMHN-IDEBNGHGSA-N iodobenzene Chemical group I[13C]1=[13CH][13CH]=[13CH][13CH]=[13CH]1 SNHMUERNLJLMHN-IDEBNGHGSA-N 0.000 description 3
- SAVQQRYWWAGSQW-UHFFFAOYSA-N n-methyl-n-(trifluoro-$l^{4}-sulfanyl)methanamine Chemical compound CN(C)S(F)(F)F SAVQQRYWWAGSQW-UHFFFAOYSA-N 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- MMYKTRPLXXWLBC-UHFFFAOYSA-N 1-bromo-2-ethoxyethane Chemical compound CCOCCBr MMYKTRPLXXWLBC-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- 238000003747 Grignard reaction Methods 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- 125000004036 acetal group Chemical group 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- RDHPKYGYEGBMSE-UHFFFAOYSA-N bromoethane Chemical compound CCBr RDHPKYGYEGBMSE-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 238000005695 dehalogenation reaction Methods 0.000 description 1
- 125000001028 difluoromethyl group Chemical group [H]C(F)(F)* 0.000 description 1
- NZZFYRREKKOMAT-UHFFFAOYSA-N diiodomethane Chemical compound ICI NZZFYRREKKOMAT-UHFFFAOYSA-N 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 125000001475 halogen functional group Chemical group 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- HVTICUPFWKNHNG-UHFFFAOYSA-N iodoethane Chemical compound CCI HVTICUPFWKNHNG-UHFFFAOYSA-N 0.000 description 1
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 125000000446 sulfanediyl group Chemical group *S* 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- 125000002813 thiocarbonyl group Chemical group *C(*)=S 0.000 description 1
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009263316A JP5712481B2 (ja) | 2009-11-18 | 2009-11-18 | 芳香族ジフルオロ酢酸エステルの製造方法 |
| US13/510,227 US8802886B2 (en) | 2009-11-18 | 2010-10-26 | Method for producing aromatic difluoroacetic acid ester |
| PCT/JP2010/068920 WO2011062033A1 (ja) | 2009-11-18 | 2010-10-26 | 芳香族ジフルオロ酢酸エステルの製造方法 |
| CN201080052457.7A CN102639483B (zh) | 2009-11-18 | 2010-10-26 | 芳香族二氟乙酸酯的制造方法 |
| EP10831429.5A EP2502898A4 (en) | 2009-11-18 | 2010-10-26 | PROCESS FOR PREPARING AROMATIC DIFLUOROIC ACID ESTERS |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009263316A JP5712481B2 (ja) | 2009-11-18 | 2009-11-18 | 芳香族ジフルオロ酢酸エステルの製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011105658A JP2011105658A (ja) | 2011-06-02 |
| JP2011105658A5 true JP2011105658A5 (cg-RX-API-DMAC7.html) | 2012-08-16 |
| JP5712481B2 JP5712481B2 (ja) | 2015-05-07 |
Family
ID=44059516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009263316A Expired - Fee Related JP5712481B2 (ja) | 2009-11-18 | 2009-11-18 | 芳香族ジフルオロ酢酸エステルの製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US8802886B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2502898A4 (cg-RX-API-DMAC7.html) |
| JP (1) | JP5712481B2 (cg-RX-API-DMAC7.html) |
| CN (1) | CN102639483B (cg-RX-API-DMAC7.html) |
| WO (1) | WO2011062033A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013135674A1 (en) * | 2012-03-12 | 2013-09-19 | Syngenta Participations Ag | Insecticidal 2-aryl-acetamide compounds |
| WO2019025250A1 (en) | 2017-08-04 | 2019-02-07 | Basf Se | SUBSTITUTED TRIFLUOROMETHYLOXADIAZOLES FOR COMBATING PHYTOPATHOGENIC FUNGI |
| CN111205188A (zh) * | 2018-11-22 | 2020-05-29 | 上海盛迪医药有限公司 | 环烷烃化合物的制备方法 |
| CN111517954A (zh) * | 2020-06-08 | 2020-08-11 | 浙江师范大学 | 一种（z)-5-氟-2-二氟亚甲基烯烃衍生物及其制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3560840B2 (ja) * | 1999-02-09 | 2004-09-02 | セントラル硝子株式会社 | ２−トリアルキルシリル２，２−ジフルオロ酢酸エステルの製造方法 |
| JP3560905B2 (ja) * | 2000-08-01 | 2004-09-02 | セントラル硝子株式会社 | ２−トリアルキルシリル２，２−ジフルオロ酢酸エステルの製造方法 |
| JPWO2007018248A1 (ja) * | 2005-08-10 | 2009-02-19 | 萬有製薬株式会社 | ピリドン化合物 |
| JP2009263316A (ja) | 2008-04-30 | 2009-11-12 | Konishi Kagaku Ind Co Ltd | 不完全縮合オリゴシルセスキオキサンの製造方法 |
-
2009
- 2009-11-18 JP JP2009263316A patent/JP5712481B2/ja not_active Expired - Fee Related
-
2010
- 2010-10-26 EP EP10831429.5A patent/EP2502898A4/en not_active Withdrawn
- 2010-10-26 US US13/510,227 patent/US8802886B2/en not_active Expired - Fee Related
- 2010-10-26 WO PCT/JP2010/068920 patent/WO2011062033A1/ja not_active Ceased
- 2010-10-26 CN CN201080052457.7A patent/CN102639483B/zh not_active Expired - Fee Related
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