JP2008534715A - 低酸ポリブチレンテレフタレートの調製、および低酸ポリブチレンテレフタレートからの大環状ポリエステルオリゴマーの調製 - Google Patents

低酸ポリブチレンテレフタレートの調製、および低酸ポリブチレンテレフタレートからの大環状ポリエステルオリゴマーの調製 Download PDF

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JP2008534715A
JP2008534715A JP2008503177A JP2008503177A JP2008534715A JP 2008534715 A JP2008534715 A JP 2008534715A JP 2008503177 A JP2008503177 A JP 2008503177A JP 2008503177 A JP2008503177 A JP 2008503177A JP 2008534715 A JP2008534715 A JP 2008534715A
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mixture
catalyst
less
depolymerization
concentration
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Japanese (ja)
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ピーター ディー. フェルプス,
ジミー ライアン ウェブ,
デイビッド パトリック フェロン,
ポール エム. アンドラシスジン,
ゲイリー アール. フェイラー,
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サイクリクス コーポレイション
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/82Preparation processes characterised by the catalyst used
    • C08G63/85Germanium, tin, lead, arsenic, antimony, bismuth, titanium, zirconium, hafnium, vanadium, niobium, tantalum, or compounds thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16Dicarboxylic acids and dihydroxy compounds
    • C08G63/18Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181Acids containing aromatic rings
    • C08G63/183Terephthalic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/81Preparation processes using solvents
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2008503177A 2005-03-25 2006-03-24 低酸ポリブチレンテレフタレートの調製、および低酸ポリブチレンテレフタレートからの大環状ポリエステルオリゴマーの調製 Withdrawn JP2008534715A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US66564805P 2005-03-25 2005-03-25
PCT/US2006/010541 WO2006104821A1 (en) 2005-03-25 2006-03-24 Preparation of low-acid polyalkylene terephthalate and preparation of macrocyclic polyester oligomer therefrom

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JP2008534715A true JP2008534715A (ja) 2008-08-28

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JP2008503177A Withdrawn JP2008534715A (ja) 2005-03-25 2006-03-24 低酸ポリブチレンテレフタレートの調製、および低酸ポリブチレンテレフタレートからの大環状ポリエステルオリゴマーの調製

Country Status (5)

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US (1) US7732557B2 (US07732557-20100608-C00008.png)
EP (1) EP1879940A1 (US07732557-20100608-C00008.png)
JP (1) JP2008534715A (US07732557-20100608-C00008.png)
CN (1) CN101208370A (US07732557-20100608-C00008.png)
WO (1) WO2006104821A1 (US07732557-20100608-C00008.png)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011132318A1 (ja) * 2010-04-23 2011-10-27 日華化学株式会社 非結晶性ポリエステル樹脂、静電荷像現像用トナー用結着樹脂、及び非結晶性ポリエステル樹脂の製造方法
WO2011132319A1 (ja) * 2010-04-23 2011-10-27 日華化学株式会社 非結晶性ポリエステル樹脂、静電荷像現像用トナー用結着樹脂、及び非結晶性ポリエステル樹脂の製造方法
KR20180024320A (ko) 2016-08-29 2018-03-08 주식회사 엘지화학 폴리부틸렌테레프탈레이트의 제조방법
KR20240015493A (ko) 2022-07-27 2024-02-05 주식회사 엘지화학 비스-4-히드록시부틸테레프탈레이트의 제조 방법 및 이에 따라 제조된 비스-4-히드록시부틸테레프탈레이트

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7767781B2 (en) * 2000-09-01 2010-08-03 Cyclics Corporation Preparation of low-acid polyalkylene terephthalate and preparation of macrocyclic polyester oligomer therefrom
US7750109B2 (en) 2000-09-01 2010-07-06 Cyclics Corporation Use of a residual oligomer recyclate in the production of macrocyclic polyester oligomer
US20040260034A1 (en) 2003-06-19 2004-12-23 Haile William Alston Water-dispersible fibers and fibrous articles
US8513147B2 (en) 2003-06-19 2013-08-20 Eastman Chemical Company Nonwovens produced from multicomponent fibers
US7892993B2 (en) 2003-06-19 2011-02-22 Eastman Chemical Company Water-dispersible and multicomponent fibers from sulfopolyesters
US20090137749A1 (en) * 2007-10-23 2009-05-28 Phelps Peter D Processes for reducing acid content of a polyalkylene terephthalate and using such in the production of macrocyclic polyester oligomer
US20090137836A1 (en) * 2007-10-23 2009-05-28 Phelps Peter D Processes for preparing low-acid polyalkylene terephthalate from diol-capped pre-polymer and linear oligomer recyclate and using such in the production of macrocyclic polyester oligomer
US9624342B2 (en) * 2008-02-06 2017-04-18 Valspar Sourcing, Inc. Process for manufacturing medium and high molecular weight polyesters
US8512519B2 (en) 2009-04-24 2013-08-20 Eastman Chemical Company Sulfopolyesters for paper strength and process
US9273417B2 (en) 2010-10-21 2016-03-01 Eastman Chemical Company Wet-Laid process to produce a bound nonwoven article
EP2678371B1 (en) * 2011-02-23 2015-01-07 Cyclics Corporation Methods for preparation of macrocyclic polyester oligomer via heterogeneous catalysis
US8840757B2 (en) 2012-01-31 2014-09-23 Eastman Chemical Company Processes to produce short cut microfibers
WO2014160317A1 (en) 2013-03-13 2014-10-02 Liquid Thermo Plastics, Inc. Methods for preparation of polyester oligomer via base catalysis
US9303357B2 (en) 2013-04-19 2016-04-05 Eastman Chemical Company Paper and nonwoven articles comprising synthetic microfiber binders
US9598802B2 (en) 2013-12-17 2017-03-21 Eastman Chemical Company Ultrafiltration process for producing a sulfopolyester concentrate
US9605126B2 (en) 2013-12-17 2017-03-28 Eastman Chemical Company Ultrafiltration process for the recovery of concentrated sulfopolyester dispersion
WO2016126757A1 (en) * 2015-02-05 2016-08-11 Liquid Thermo Plastics, Inc. Methods for preparation of macrocyclic polyester oligomer from linear polyester
KR102432504B1 (ko) 2016-09-14 2022-08-16 바스프 에스이 프로파일 압출용 및/또는 파이프 압출용 폴리에스테르
US10759899B2 (en) 2017-08-03 2020-09-01 Colorado State University Research Foundation Recyclable polymers based on ring-fused gamma-butyrolactones
KR20220041177A (ko) * 2019-07-29 2022-03-31 이스트만 케미칼 컴파니 열분해 및 가메탄올분해로부터의 재활용된 단량체를 갖는 폴리에스테르의 제조 방법
CN114957627A (zh) * 2022-05-16 2022-08-30 万华化学集团股份有限公司 一种低副产四氢呋喃的聚酯制备方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT549917A (US07732557-20100608-C00008.png) * 1954-09-30
DE2514116C3 (de) * 1975-03-29 1983-03-17 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung von linearen, hochmolekularen Polybutylenterephthalaten
US5039783A (en) * 1990-11-05 1991-08-13 General Electric Company Method for preparing and polymerizing macrocyclic poly(alkylene discarboxylate) oligomers
US5466744A (en) * 1990-11-05 1995-11-14 General Electric Company Polymerization of macrocyclic poly(alkylene dicarboxylate) oligomers
KR940010346B1 (ko) * 1991-06-12 1994-10-22 한국과학기술연구원 폴리부틸렌테레프탈레이트계 중합체의 제조방법
US5231161A (en) * 1992-10-22 1993-07-27 General Electric Company Method for preparation of macrocyclic poly(alkylene dicarboxylate) oligomers from bis(hydroxyalkyl) dicarboxylates
US5407984A (en) * 1994-08-31 1995-04-18 General Electric Company Process for preparing macrocyclic polyester oligomers
DE19509551A1 (de) * 1995-03-16 1996-09-19 Basf Ag Verfahren zur kontinuierlichen Herstellung von thermoplastischen Polyestern
US5516879A (en) * 1995-03-28 1996-05-14 Industrial Technology Research Institute Catalytic compositions for the preparation of poly(butylene terephthalate)
GB2315755B (en) * 1995-06-06 1999-12-08 Univ North Carolina Process for the preparation of polyester in carbon dioxide
US5519108A (en) * 1995-06-07 1996-05-21 Industrial Technology Research Institute Catalytic compositions containing tetrabutyl titanate and a mixture of cocatalysts for the preparation of poly(butylene terephthalate)
US5668186A (en) * 1996-03-20 1997-09-16 General Electric Company Process for depolymerizing polyesters
US5900474A (en) * 1997-08-20 1999-05-04 National Science Council Of Republic Of China Catalyst composition for production of polybutylene terephthalate via direct esterification process
US6127436A (en) * 1998-10-26 2000-10-03 Sun Chemical Corporation Reclaimed poly (ethylene terephthalate) coating
US7256241B2 (en) * 2000-01-21 2007-08-14 Cyclics Corporation Methods for polymerizing macrocyclic polyester oligomers using catalyst promoters
US6472500B2 (en) * 2000-06-17 2002-10-29 General Electric Company Crystalline polyester resins and processes for their preparation
JP2004507599A (ja) * 2000-09-01 2004-03-11 サイクリクス コーポレイション 線形ポリエステルを、大環状オリゴエステル組成物および大環状オリゴエステルに変換する方法
US7750109B2 (en) * 2000-09-01 2010-07-06 Cyclics Corporation Use of a residual oligomer recyclate in the production of macrocyclic polyester oligomer
US7767781B2 (en) * 2000-09-01 2010-08-03 Cyclics Corporation Preparation of low-acid polyalkylene terephthalate and preparation of macrocyclic polyester oligomer therefrom
US6436548B1 (en) * 2000-09-12 2002-08-20 Cyclics Corporation Species modification in macrocyclic polyester oligomers, and compositions prepared thereby
EP1409475B1 (en) * 2001-06-27 2005-10-05 Cyclics Corporation Isolation, formulation, and shaping of macrocyclic oligoesters
US6436549B1 (en) * 2001-07-16 2002-08-20 Cyclics Corporation Block copolymers from macrocyclic oligoesters and dihydroxyl-functionalized polymers
US6787632B2 (en) * 2001-10-09 2004-09-07 Cyclics Corporation Organo-titanate catalysts for preparing pure macrocyclic oligoesters
DE10393926T5 (de) * 2002-12-20 2006-09-28 Cyclics Corp. Reinigung von makrocyclischen Oligoestern
JP4290015B2 (ja) * 2003-01-10 2009-07-01 キヤノン株式会社 カラートナー及び画像形成装置

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011132318A1 (ja) * 2010-04-23 2011-10-27 日華化学株式会社 非結晶性ポリエステル樹脂、静電荷像現像用トナー用結着樹脂、及び非結晶性ポリエステル樹脂の製造方法
WO2011132319A1 (ja) * 2010-04-23 2011-10-27 日華化学株式会社 非結晶性ポリエステル樹脂、静電荷像現像用トナー用結着樹脂、及び非結晶性ポリエステル樹脂の製造方法
JP5010759B2 (ja) * 2010-04-23 2012-08-29 日華化学株式会社 非結晶性ポリエステル樹脂、静電荷像現像用トナー用結着樹脂、及び非結晶性ポリエステル樹脂の製造方法
US8598300B2 (en) 2010-04-23 2013-12-03 Nicca Chemical Co., Ltd. Amorphous polyester resin, binder resin for toner for electrostatic image development and amorphous polyester resin production method
KR20180024320A (ko) 2016-08-29 2018-03-08 주식회사 엘지화학 폴리부틸렌테레프탈레이트의 제조방법
KR20240015493A (ko) 2022-07-27 2024-02-05 주식회사 엘지화학 비스-4-히드록시부틸테레프탈레이트의 제조 방법 및 이에 따라 제조된 비스-4-히드록시부틸테레프탈레이트

Also Published As

Publication number Publication date
EP1879940A1 (en) 2008-01-23
CN101208370A (zh) 2008-06-25
US20060235233A1 (en) 2006-10-19
WO2006104821A1 (en) 2006-10-05
US7732557B2 (en) 2010-06-08

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