JP2007514199A

JP2007514199A - フォトサーモグラフィ用途のための化学増感法

フォトサーモグラフィ用途のための化学増感法 Download PDF

Info

Publication number: JP2007514199A
Authority: JP; Japan
Prior art keywords: silver; photothermographic; photosensitive; silver halide; halide grains
Prior art date: 2003-12-09
Legal status : Withdrawn

Application number

JP2006543862A

Other languages

English (en)

Japanese (ja)

Other versions

JP2007514199A5 (enExample

Inventor

ペトロブナバーレバ，リリア

チャールズスキナー，マーク

サキザデー，クマーズ

マリーシンプソン，シャロン

Original Assignee

イーストマンコダックカンパニー

Priority date

2003-12-09

Filing date

2004-11-29

Publication date

2007-05-31

2004-11-29 Application filed by イーストマンコダックカンパニー filed Critical イーストマンコダックカンパニー

2007-05-31 Publication of JP2007514199A publication Critical patent/JP2007514199A/ja

2007-12-27 Publication of JP2007514199A5 publication Critical patent/JP2007514199A5/ja

Status Withdrawn legal-status Critical Current

Links

239000000126 substance Substances 0.000 title claims description 35
206010070834 Sensitisation Diseases 0.000 title claims description 26
230000008313 sensitization Effects 0.000 title claims description 26
-1 silver halide Chemical class 0.000 claims abstract description 319
229910052709 silver Inorganic materials 0.000 claims abstract description 313
239000004332 silver Substances 0.000 claims abstract description 311
239000000463 material Substances 0.000 claims abstract description 252
150000001875 compounds Chemical class 0.000 claims abstract description 196
239000000839 emulsion Substances 0.000 claims abstract description 115
238000000034 method Methods 0.000 claims abstract description 89
125000001741 organic sulfur group Chemical group 0.000 claims abstract description 46
230000001235 sensitizing effect Effects 0.000 claims abstract description 38
238000004519 manufacturing process Methods 0.000 claims abstract description 16
239000000975 dye Substances 0.000 claims description 103
239000000203 mixture Substances 0.000 claims description 100
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 65
238000003384 imaging method Methods 0.000 claims description 61
238000009472 formulation Methods 0.000 claims description 46
230000003595 spectral effect Effects 0.000 claims description 46
239000003638 chemical reducing agent Substances 0.000 claims description 39
239000011230 binding agent Substances 0.000 claims description 37
238000000576 coating method Methods 0.000 claims description 33
239000011248 coating agent Substances 0.000 claims description 31
238000011161 development Methods 0.000 claims description 28
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 27
229910052717 sulfur Inorganic materials 0.000 claims description 25
FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 claims description 23
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 23
239000003795 chemical substances by application Substances 0.000 claims description 23
239000011593 sulfur Substances 0.000 claims description 23
239000006185 dispersion Substances 0.000 claims description 22
239000002253 acid Substances 0.000 claims description 20
NSBNSZAXNUGWDJ-UHFFFAOYSA-O monopyridin-1-ium tribromide Chemical compound Br[Br-]Br.C1=CC=[NH+]C=C1 NSBNSZAXNUGWDJ-UHFFFAOYSA-O 0.000 claims description 18
239000007800 oxidant agent Substances 0.000 claims description 17
125000004432 carbon atom Chemical group C* 0.000 claims description 16
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 15
229910052736 halogen Inorganic materials 0.000 claims description 13
150000002367 halogens Chemical class 0.000 claims description 13
125000000217 alkyl group Chemical group 0.000 claims description 12
239000003381 stabilizer Substances 0.000 claims description 12
230000001590 oxidative effect Effects 0.000 claims description 11
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 claims description 11
239000002904 solvent Substances 0.000 claims description 11
238000012545 processing Methods 0.000 claims description 10
230000001681 protective effect Effects 0.000 claims description 10
238000002156 mixing Methods 0.000 claims description 9
239000002243 precursor Substances 0.000 claims description 9
229910052739 hydrogen Inorganic materials 0.000 claims description 8
239000001257 hydrogen Substances 0.000 claims description 8
230000002209 hydrophobic effect Effects 0.000 claims description 8
125000005647 linker group Chemical group 0.000 claims description 8
125000003118 aryl group Chemical group 0.000 claims description 7
125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 claims description 6
125000005843 halogen group Chemical group 0.000 claims description 6
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
230000009467 reduction Effects 0.000 claims description 6
AQRYNYUOKMNDDV-UHFFFAOYSA-M silver behenate Chemical compound [Ag+].CCCCCCCCCCCCCCCCCCCCCC([O-])=O AQRYNYUOKMNDDV-UHFFFAOYSA-M 0.000 claims description 6
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 5
125000001931 aliphatic group Chemical group 0.000 claims description 5
CHYUXCABJMXHJN-UHFFFAOYSA-N diphenyl(sulfanylidene)phosphanium Chemical compound C=1C=CC=CC=1[P+](=S)C1=CC=CC=C1 CHYUXCABJMXHJN-UHFFFAOYSA-N 0.000 claims description 5
238000001035 drying Methods 0.000 claims description 5
239000006224 matting agent Substances 0.000 claims description 5
KIWUVOGUEXMXSV-UHFFFAOYSA-N rhodanine Chemical compound O=C1CSC(=S)N1 KIWUVOGUEXMXSV-UHFFFAOYSA-N 0.000 claims description 5
125000004434 sulfur atom Chemical group 0.000 claims description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 claims description 4
150000003842 bromide salts Chemical class 0.000 claims description 4
229910052799 carbon Inorganic materials 0.000 claims description 4
235000014113 dietary fatty acids Nutrition 0.000 claims description 4
BULYQPQVGJVSJD-UHFFFAOYSA-N diphenyl(sulfanylidene)-lambda5-phosphane Chemical class C=1C=CC=CC=1P(=S)C1=CC=CC=C1 BULYQPQVGJVSJD-UHFFFAOYSA-N 0.000 claims description 4
229930195729 fatty acid Natural products 0.000 claims description 4
239000000194 fatty acid Substances 0.000 claims description 4
229910052757 nitrogen Inorganic materials 0.000 claims description 4
125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 claims description 4
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
239000002216 antistatic agent Substances 0.000 claims description 3
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 3
125000001246 bromo group Chemical group Br* 0.000 claims description 3
125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 3
229910052760 oxygen Inorganic materials 0.000 claims description 3
239000001301 oxygen Substances 0.000 claims description 3
UGWULZWUXSCWPX-UHFFFAOYSA-N 2-sulfanylideneimidazolidin-4-one Chemical compound O=C1CNC(=S)N1 UGWULZWUXSCWPX-UHFFFAOYSA-N 0.000 claims description 2
150000007942 carboxylates Chemical class 0.000 claims description 2
239000002872 contrast media Substances 0.000 claims description 2
230000002708 enhancing effect Effects 0.000 claims description 2
150000004665 fatty acids Chemical class 0.000 claims description 2
238000012805 post-processing Methods 0.000 claims description 2
125000000446 sulfanediyl group Chemical group *S* 0.000 claims description 2
125000002813 thiocarbonyl group Chemical group *C(*)=S 0.000 claims description 2
125000004663 dialkyl amino group Chemical group 0.000 claims 1
230000008569 process Effects 0.000 abstract description 21
238000006864 oxidative decomposition reaction Methods 0.000 abstract 1
239000010410 layer Substances 0.000 description 150
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 67
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 48
239000000243 solution Substances 0.000 description 48
150000003378 silver Chemical group 0.000 description 41
CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical class OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 33
230000018109 developmental process Effects 0.000 description 26
230000005855 radiation Effects 0.000 description 26
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 23
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 20
239000002245 particle Substances 0.000 description 17
238000006243 chemical reaction Methods 0.000 description 16
VNDYJBBGRKZCSX-UHFFFAOYSA-L zinc bromide Chemical compound Br[Zn]Br VNDYJBBGRKZCSX-UHFFFAOYSA-L 0.000 description 16
229960005070 ascorbic acid Drugs 0.000 description 15
230000035945 sensitivity Effects 0.000 description 15
238000007792 addition Methods 0.000 description 14
235000010323 ascorbic acid Nutrition 0.000 description 14
239000011668 ascorbic acid Substances 0.000 description 14
230000000694 effects Effects 0.000 description 13
238000011065 in-situ storage Methods 0.000 description 13
229920000642 polymer Polymers 0.000 description 13
238000002360 preparation method Methods 0.000 description 13
150000003839 salts Chemical class 0.000 description 13
238000003860 storage Methods 0.000 description 13
239000002585 base Substances 0.000 description 12
230000015572 biosynthetic process Effects 0.000 description 12
150000004820 halides Chemical class 0.000 description 12
238000011160 research Methods 0.000 description 12
238000010438 heat treatment Methods 0.000 description 11
229910052751 metal Inorganic materials 0.000 description 11
239000002184 metal Substances 0.000 description 11
229910052761 rare earth metal Inorganic materials 0.000 description 11
239000000344 soap Substances 0.000 description 11
239000000654 additive Substances 0.000 description 10
125000001424 substituent group Chemical group 0.000 description 10
108010010803 Gelatin Proteins 0.000 description 9
229920000159 gelatin Polymers 0.000 description 9
239000008273 gelatin Substances 0.000 description 9
235000019322 gelatine Nutrition 0.000 description 9
235000011852 gelatine desserts Nutrition 0.000 description 9
RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 9
239000011941 photocatalyst Substances 0.000 description 9
229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 9
239000004793 Polystyrene Substances 0.000 description 8
239000013078 crystal Substances 0.000 description 8
IJAPPYDYQCXOEF-UHFFFAOYSA-N phthalazin-1(2H)-one Chemical compound C1=CC=C2C(=O)NN=CC2=C1 IJAPPYDYQCXOEF-UHFFFAOYSA-N 0.000 description 8
JUJWROOIHBZHMG-UHFFFAOYSA-N pyridine Substances C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 8
238000002601 radiography Methods 0.000 description 8
150000002910 rare earth metals Chemical class 0.000 description 8
229940102001 zinc bromide Drugs 0.000 description 8
150000001732 carboxylic acid derivatives Chemical class 0.000 description 7
229920006217 cellulose acetate butyrate Polymers 0.000 description 7
239000011258 core-shell material Substances 0.000 description 7
238000000354 decomposition reaction Methods 0.000 description 7
230000003647 oxidation Effects 0.000 description 7
238000007254 oxidation reaction Methods 0.000 description 7
238000011282 treatment Methods 0.000 description 7
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
238000002835 absorbance Methods 0.000 description 6
125000004429 atom Chemical group 0.000 description 6
239000008199 coating composition Substances 0.000 description 6
230000005670 electromagnetic radiation Effects 0.000 description 6
230000006870 function Effects 0.000 description 6
230000001965 increasing effect Effects 0.000 description 6
AMXOYNBUYSYVKV-UHFFFAOYSA-M lithium bromide Chemical compound [Li+].[Br-] AMXOYNBUYSYVKV-UHFFFAOYSA-M 0.000 description 6
LFSXCDWNBUNEEM-UHFFFAOYSA-N phthalazine Chemical group C1=NN=CC2=CC=CC=C21 LFSXCDWNBUNEEM-UHFFFAOYSA-N 0.000 description 6
239000011347 resin Substances 0.000 description 6
KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical compound O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 description 6
UAYWVJHJZHQCIE-UHFFFAOYSA-L zinc iodide Chemical compound I[Zn]I UAYWVJHJZHQCIE-UHFFFAOYSA-L 0.000 description 6
229910052693 Europium Inorganic materials 0.000 description 5
AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 5
229910052771 Terbium Inorganic materials 0.000 description 5
229910052946 acanthite Inorganic materials 0.000 description 5
229910052783 alkali metal Inorganic materials 0.000 description 5
229910052784 alkaline earth metal Inorganic materials 0.000 description 5
XSCHRSMBECNVNS-UHFFFAOYSA-N benzopyrazine Natural products N1=CC=NC2=CC=CC=C21 XSCHRSMBECNVNS-UHFFFAOYSA-N 0.000 description 5
QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 5
239000012964 benzotriazole Substances 0.000 description 5
230000003197 catalytic effect Effects 0.000 description 5
230000000052 comparative effect Effects 0.000 description 5
238000001723 curing Methods 0.000 description 5
239000002019 doping agent Substances 0.000 description 5
125000001072 heteroaryl group Chemical group 0.000 description 5
125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
239000003446 ligand Substances 0.000 description 5
DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 5
230000003287 optical effect Effects 0.000 description 5
239000003960 organic solvent Substances 0.000 description 5
229920005989 resin Polymers 0.000 description 5
229940056910 silver sulfide Drugs 0.000 description 5
XUARKZBEFFVFRG-UHFFFAOYSA-N silver sulfide Chemical compound [S-2].[Ag+].[Ag+] XUARKZBEFFVFRG-UHFFFAOYSA-N 0.000 description 5
239000000988 sulfur dye Substances 0.000 description 5
229910052714 tellurium Inorganic materials 0.000 description 5
229920002554 vinyl polymer Polymers 0.000 description 5
QGKMIGUHVLGJBR-UHFFFAOYSA-M (4z)-1-(3-methylbutyl)-4-[[1-(3-methylbutyl)quinolin-1-ium-4-yl]methylidene]quinoline;iodide Chemical compound [I-].C12=CC=CC=C2N(CCC(C)C)C=CC1=CC1=CC=[N+](CCC(C)C)C2=CC=CC=C12 QGKMIGUHVLGJBR-UHFFFAOYSA-M 0.000 description 4
VZSRBBMJRBPUNF-UHFFFAOYSA-N 2-(2,3-dihydro-1H-inden-2-ylamino)-N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]pyrimidine-5-carboxamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C(=O)NCCC(N1CC2=C(CC1)NN=N2)=O VZSRBBMJRBPUNF-UHFFFAOYSA-N 0.000 description 4
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 4
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
NVXLIZQNSVLKPO-UHFFFAOYSA-N Glucosereductone Chemical compound O=CC(O)C=O NVXLIZQNSVLKPO-UHFFFAOYSA-N 0.000 description 4
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 4
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
229910021612 Silver iodide Inorganic materials 0.000 description 4
235000010724 Wisteria floribunda Nutrition 0.000 description 4
150000007933 aliphatic carboxylic acids Chemical class 0.000 description 4
150000001342 alkaline earth metals Chemical class 0.000 description 4
230000008901 benefit Effects 0.000 description 4
238000004061 bleaching Methods 0.000 description 4
229920001577 copolymer Polymers 0.000 description 4
238000011066 ex-situ storage Methods 0.000 description 4
125000000623 heterocyclic group Chemical group 0.000 description 4
239000012535 impurity Substances 0.000 description 4
238000005259 measurement Methods 0.000 description 4
XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 4
229920000139 polyethylene terephthalate Polymers 0.000 description 4
239000005020 polyethylene terephthalate Substances 0.000 description 4
239000011241 protective layer Substances 0.000 description 4
229910052711 selenium Inorganic materials 0.000 description 4
229940045105 silver iodide Drugs 0.000 description 4
241000894007 species Species 0.000 description 4
238000006467 substitution reaction Methods 0.000 description 4
PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 description 4
150000003585 thioureas Chemical class 0.000 description 4
ZPANWZBSGMDWON-UHFFFAOYSA-N 1-[(2-hydroxynaphthalen-1-yl)methyl]naphthalen-2-ol Chemical compound C1=CC=C2C(CC3=C4C=CC=CC4=CC=C3O)=C(O)C=CC2=C1 ZPANWZBSGMDWON-UHFFFAOYSA-N 0.000 description 3
DVWQNBIUTWDZMW-UHFFFAOYSA-N 1-naphthalen-1-ylnaphthalen-2-ol Chemical compound C1=CC=C2C(C3=C4C=CC=CC4=CC=C3O)=CC=CC2=C1 DVWQNBIUTWDZMW-UHFFFAOYSA-N 0.000 description 3
KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 3
PHXLONCQBNATSL-UHFFFAOYSA-N 2-[[2-hydroxy-5-methyl-3-(1-methylcyclohexyl)phenyl]methyl]-4-methyl-6-(1-methylcyclohexyl)phenol Chemical compound OC=1C(C2(C)CCCCC2)=CC(C)=CC=1CC(C=1O)=CC(C)=CC=1C1(C)CCCCC1 PHXLONCQBNATSL-UHFFFAOYSA-N 0.000 description 3
BOTGCZBEERTTDQ-UHFFFAOYSA-N 4-Methoxy-1-naphthol Chemical compound C1=CC=C2C(OC)=CC=C(O)C2=C1 BOTGCZBEERTTDQ-UHFFFAOYSA-N 0.000 description 3
CWJJAFQCTXFSTA-UHFFFAOYSA-N 4-methylphthalic acid Chemical compound CC1=CC=C(C(O)=O)C(C(O)=O)=C1 CWJJAFQCTXFSTA-UHFFFAOYSA-N 0.000 description 3
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 3
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 3
229910052765 Lutetium Inorganic materials 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
WTKZEGDFNFYCGP-UHFFFAOYSA-N Pyrazole Chemical compound C=1C=NNC=1 WTKZEGDFNFYCGP-UHFFFAOYSA-N 0.000 description 3
RWRDLPDLKQPQOW-UHFFFAOYSA-N Pyrrolidine Chemical compound C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 3
BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 3
229920002472 Starch Polymers 0.000 description 3
150000001241 acetals Chemical class 0.000 description 3
150000007513 acids Chemical class 0.000 description 3
239000004480 active ingredient Substances 0.000 description 3
125000003545 alkoxy group Chemical group 0.000 description 3
238000013459 approach Methods 0.000 description 3
229910001622 calcium bromide Inorganic materials 0.000 description 3
WGEFECGEFUFIQW-UHFFFAOYSA-L calcium dibromide Chemical compound [Ca+2].[Br-].[Br-] WGEFECGEFUFIQW-UHFFFAOYSA-L 0.000 description 3
239000003054 catalyst Substances 0.000 description 3
229910052798 chalcogen Inorganic materials 0.000 description 3
150000001787 chalcogens Chemical class 0.000 description 3
230000008859 change Effects 0.000 description 3
229910052802 copper Inorganic materials 0.000 description 3
239000010949 copper Substances 0.000 description 3
238000009826 distribution Methods 0.000 description 3
AFOSIXZFDONLBT-UHFFFAOYSA-N divinyl sulfone Chemical class C=CS(=O)(=O)C=C AFOSIXZFDONLBT-UHFFFAOYSA-N 0.000 description 3
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 3
LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 3
150000002430 hydrocarbons Chemical group 0.000 description 3
XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 3
150000002443 hydroxylamines Chemical class 0.000 description 3
229910001502 inorganic halide Inorganic materials 0.000 description 3
OHSVLFRHMCKCQY-UHFFFAOYSA-N lutetium atom Chemical compound [Lu] OHSVLFRHMCKCQY-UHFFFAOYSA-N 0.000 description 3
239000010955 niobium Substances 0.000 description 3
125000004433 nitrogen atom Chemical group N* 0.000 description 3
239000004417 polycarbonate Substances 0.000 description 3
229920000515 polycarbonate Polymers 0.000 description 3
229920000728 polyester Polymers 0.000 description 3
229920002689 polyvinyl acetate Polymers 0.000 description 3
239000011118 polyvinyl acetate Substances 0.000 description 3
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 3
JUJWROOIHBZHMG-UHFFFAOYSA-O pyridinium Chemical compound C1=CC=[NH+]C=C1 JUJWROOIHBZHMG-UHFFFAOYSA-O 0.000 description 3
230000004044 response Effects 0.000 description 3
239000011669 selenium Substances 0.000 description 3
239000007787 solid Substances 0.000 description 3
235000019698 starch Nutrition 0.000 description 3
239000008107 starch Substances 0.000 description 3
238000003756 stirring Methods 0.000 description 3
229960002317 succinimide Drugs 0.000 description 3
GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 description 3
125000000101 thioether group Chemical group 0.000 description 3
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AUHHYELHRWCWEZ-UHFFFAOYSA-N tetrachlorophthalic anhydride Chemical compound ClC1=C(Cl)C(Cl)=C2C(=O)OC(=O)C2=C1Cl AUHHYELHRWCWEZ-UHFFFAOYSA-N 0.000 description 1
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NZFNXWQNBYZDAQ-UHFFFAOYSA-N thioridazine hydrochloride Chemical compound Cl.C12=CC(SC)=CC=C2SC2=CC=CC=C2N1CCC1CCCCN1C NZFNXWQNBYZDAQ-UHFFFAOYSA-N 0.000 description 1
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239000004408 titanium dioxide Substances 0.000 description 1
VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
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125000002221 trityl group Chemical group [H]C1=C([H])C([H])=C([H])C([H])=C1C([*])(C1=C(C(=C(C(=C1[H])[H])[H])[H])[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
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