JP2005520685A - サイクロンを使用するガスと固形物との分離 - Google Patents
サイクロンを使用するガスと固形物との分離 Download PDFInfo
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04C—APPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
- B04C5/00—Apparatus in which the axial direction of the vortex is reversed
- B04C5/02—Construction of inlets by which the vortex flow is generated, e.g. tangential admission, the fluid flow being forced to follow a downward path by spirally wound bulkheads, or with slightly downwardly-directed tangential admission
- B04C5/04—Tangential inlets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D45/00—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces
- B01D45/12—Separating dispersed particles from gases or vapours by gravity, inertia, or centrifugal forces by centrifugal forces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/0055—Separating solid material from the gas/liquid stream using cyclones
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04C—APPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES
- B04C5/00—Apparatus in which the axial direction of the vortex is reversed
- B04C5/08—Vortex chamber constructions
- B04C5/081—Shapes or dimensions
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Organic Chemistry (AREA)
- Geometry (AREA)
- Fluid Mechanics (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Health & Medical Sciences (AREA)
- Cyclones (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
Description
−サイクロン入口高さ(Hi)、サイクロン入口幅(Wi)およびサイクロン入口アスペクト比(Hi/Wi)を特徴とする入口デバイスと、
−ガス出口パイプ直径(Di)およびガス出口パイプ浸入度(P)を特徴とするガス出口パイプと、
−円筒部分および円錐部分で作成され、上側バレル(Lb1)直径(Db)、バレル長さ(Lb=Lb1+Lb2)およびバレル長さと直径との比(Lb/Db)を特徴とするバレル、並びに
−固形物出口パイプ(O)
を備える。
SBR(スチレンと共重合されたブタジエンに基づくポリマー);
ABS(アクリロニトリル−ブタジエン−スチレンポリマー);
ニトリル(アクリロニトリルと共重合されたブタジエンに基づくポリマー);
ブチル(イソプレンと共重合されたイソブチレンに基づくポリマー);
EPR(エチレン−プロピレンポリマー);
EPDM(プロピレンおよびたとえばヘキサジエン、ジシクロペンタジエンもしくはエチリデンノルボルネンのようなジエンと共重合されたエチレンに基づくポリマー);
エチレン−ビニルトリメトキシシランコポリマー、エチレンとアクリロニトリル、マレイン酸エステル、酢酸ビニル、アクリルおよびメタクリル酸エステル、並びにその同族体から選択される1種もしくはそれ以上の化合物のコポリマー。
圧力 350psig(24バール、g)
温度 158°F(70℃)
固形物負荷 ガス1m3当たり0.004〜0.8kgの固形物
ガス入口速度 5−20m/sec
ガス出口速度 5−10m/sec
メルトインデックス(IF2)=1.60
Al/Ti=1.40
活性=25.1g/グラムモル/hr
嵩密度(MVA)=320kg/m3
通常のアスペクト比、充分な浸入度、短いバレル(Hi/Wi=2.5、P/Hi=1.25、Lb/Db=4.0)
サイクロン1A −図2−
1.サイクロン効率測定の再現性は0.01%以内である
2.増大させた操作温度は収集効率に作用を持たなかったが、全体的圧力低下を僅かに減少させる
3.たとえば次の条件で操作される標準的気相サイクロンの圧力低下は400ミリバールに等しい。
Ug、i=20m/s
4.渦流スタビライザなしの標準的気相サイクロン(Ug、i=20m/sec)のサイクロン収集効率は99.834%±0.012%に等しい。
次の一連の実施例にて、大バレル直径気相サイクロンの配置を改変させて、そのサイクロン効率を最適化させた。先の実施例におけるように、各サイクロンを一定圧力(24brag)、温度(70℃)にて固形物負荷の範囲(0.004〜0.8kg固形物/ガス1m3)にわたり試験した。表は、N°3、3Aおよび3Bと称するサイクロンの配置を要約する。
大アスペクト比、短い浸入度、短いバレル(Hi/Wi=5.0、P/Hi=0.47、Lb/Db=4.0)
サイクロンN°3 −図2−
大アスペクト比、充分な浸入度、短いバレル(Hi/Wi=2.5、P/Hi=1.0、Lb/Db=4.0)
サイクロンN°3A −図3−
サイクロンN°3Aをその入口アスペクト比Hi/Wiを5から2.5まで減少させるよう建設し、これはその入口面積を標準的サイクロンより1.8倍効果的に大にする。予想通り、その圧力低下はその初期値の1/1.8^2=1/3だけ減少した(400ミリバールから132ミリバールまで)。
低アスペクト比、充分な浸入度、長バレル(Hi/Wi=2.5、P/Hi=1.0、Lb/Db=5.0)
サイクロンN°3B −図4−
当業界では、バレル長さを増大させればサイクロンバレルにて一層多くのサイクロンを許すことによりサイクロン効率を増大させうると報告されている。大バレル直径サイクロンのバレルを25%だけ長くした。サイクロン3Bと称するこのサイクロンは先の実施例におけるサイクロンと同じ配置を有したが、バレル長さと直径との比(Lb/Hb)を4.0から5.0まで増大させた。サイクロン出口チューブ浸入度は同一であった(P/Hi=1.0)。
Claims (7)
- 入口高さ(Hi)および入口幅(Wi)を有する入口デバイスと、パイプ直径(Di)およびパイプ浸入度(P)を有するガス出口パイプと、上側バレル直径(Db)およびバレル長さ(Lb)を有するバレルとを備え、前記バレルは円錐容積部の頂部における円筒容積部と固形物出口パイプ(O)と入口ガス速度(Ug、i)と入口ガス流量(Q)とからなるサイクロンデザインにおいて、上側バレル直径の平方に対する入口ガス流量の比(Q/Db2)は0.5より大、好ましくは0.7より大かつ1.5より小、好ましくは1.2(m/s)より小であると共に、直径に対するバレル長さの比(Lb/Db)は3より大、好ましくは3.5より大かつ6より小、好ましくは4.5より小であることを特徴とするサイクロンデザイン。
- 入口ガス速度が6m/sである請求項1に記載のサイクロン。
- サイクロン入口高さ(Hi)およびガス出口パイプ浸入度(P)を、比P/Hiが0.62より大かつ1.25より小となるようにする請求項1または2に記載のサイクロン。
- 渦流スタビライザを含まないことを特徴とする請求項1〜3のいずれか一項に記載のサイクロン。
- 上側バレル直径の平方に対する入口ガス流量の比(Q/Db2)が0.5より大、好ましくは0.7より大かつ1.5より小、好ましくは1.2より小である請求項1〜4のいずれか一項に記載のサイクロンを使用するガスと固形物との混合物の分離方法。
- 上側バレル直径の平方に対する入口ガス流量の比(Q/Db2)が0.5より大、好ましくは0.7より大かつ1.5より小、好ましくは1.2(m/s)より小である、気相重合流動床反応器から流出するガスと固形物との混合物から触媒とポリマー粒子とを分離するための請求項1〜5のいずれか一項に記載のサイクロンの使用。
- 気相重合流動床反応器を0.5〜6MPaの絶対圧力にて操作する請求項6に記載の使用。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02358004 | 2002-03-19 | ||
PCT/GB2003/001072 WO2003080253A1 (en) | 2002-03-19 | 2003-03-13 | Separation of gases and solids using a cyclone |
Publications (1)
Publication Number | Publication Date |
---|---|
JP2005520685A true JP2005520685A (ja) | 2005-07-14 |
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JP2003578069A Pending JP2005520685A (ja) | 2002-03-19 | 2003-03-13 | サイクロンを使用するガスと固形物との分離 |
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US (1) | US7323038B2 (ja) |
EP (1) | EP1487588B1 (ja) |
JP (1) | JP2005520685A (ja) |
KR (1) | KR100916732B1 (ja) |
CN (1) | CN1304120C (ja) |
AT (1) | ATE366621T1 (ja) |
AU (1) | AU2003216809A1 (ja) |
DE (1) | DE60314852T2 (ja) |
ES (1) | ES2287455T3 (ja) |
WO (1) | WO2003080253A1 (ja) |
ZA (1) | ZA200407413B (ja) |
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JP2010017675A (ja) * | 2008-07-14 | 2010-01-28 | Panasonic Corp | 集塵装置 |
JP2010036054A (ja) * | 2008-07-31 | 2010-02-18 | Sumco Corp | サイクロン集塵装置及び単結晶引き上げシステム |
KR101267878B1 (ko) | 2011-09-07 | 2013-05-27 | 한국에너지기술연구원 | 고압상태의 선회유동을 이용한 입자분리장치 |
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DE102004054304A1 (de) * | 2004-11-09 | 2006-05-11 | Basell Polyolefine Gmbh | Vorrichtung und Verfahren zur Gasphasenpolymerisation von Olefinen |
DE102004054628A1 (de) * | 2004-11-11 | 2006-05-18 | Basell Polyolefine Gmbh | Vorrichtung zur Gasphasenpolymerisation von Olefinen, insbesondere Ethylen |
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JP4852366B2 (ja) * | 2006-07-12 | 2012-01-11 | 財団法人 国際石油交流センター | 気固分離器の設計方法 |
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US8034143B2 (en) * | 2008-03-18 | 2011-10-11 | Uti Limited Partnership | Cyclone |
US8951421B2 (en) | 2009-03-02 | 2015-02-10 | Convex B.V. | Apparatus and method for purifying a liquid |
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EP2431096B1 (en) | 2010-09-17 | 2013-12-25 | Alstom Technology Ltd | Cyclone separator |
EP2457647A1 (en) | 2010-11-29 | 2012-05-30 | Ineos Commercial Services UK Limited | Apparatus and process |
EP2990123B1 (en) * | 2013-04-23 | 2018-07-04 | Shizuoka Plant Co., Ltd. | Cyclone device |
CN103286012A (zh) * | 2013-06-18 | 2013-09-11 | 无锡市石油化工设备有限公司 | 高温高效旋风分离器 |
PT107312B (pt) | 2013-11-25 | 2022-05-10 | Advanced Cyclone Systems S A | Ciclone aglomerador de fluxo invertido e respectivo processo |
US9334336B2 (en) | 2013-12-20 | 2016-05-10 | Chevron Phillips Chemical Company, Lp | Polyolefin reactor system having a gas phase reactor and solids recovery |
CN104624401B (zh) | 2015-03-06 | 2019-01-15 | 英尼奥斯欧洲股份公司 | 改进的旋风分离器构造 |
CN108058378A (zh) * | 2017-12-21 | 2018-05-22 | 广州市爱司凯科技股份有限公司 | 3d打印机气砂分离装置及分离方法 |
EP3834923A1 (en) * | 2019-12-11 | 2021-06-16 | Basell Polyolefine GmbH | Apparatus and process for the gas-phase polymerization |
WO2021176130A1 (en) * | 2020-03-06 | 2021-09-10 | Outotec (Finland) Oy | Cyclone separator arrangement |
CN114470979A (zh) * | 2020-11-13 | 2022-05-13 | 中国石油天然气股份有限公司 | 吹扫装置及聚乙烯生产设备 |
CN114273098B (zh) * | 2021-12-29 | 2024-04-26 | 上海赛科石油化工有限责任公司 | 在丙烯腈生产流程中分离聚合物的系统及方法 |
US11850605B2 (en) * | 2022-03-01 | 2023-12-26 | Saudi Arabian Oil Company | Apparatus and method to separate and condition multiphase flow |
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- 2003-03-13 EP EP03712344A patent/EP1487588B1/en not_active Expired - Lifetime
- 2003-03-13 AU AU2003216809A patent/AU2003216809A1/en not_active Abandoned
- 2003-03-13 DE DE60314852T patent/DE60314852T2/de not_active Expired - Lifetime
- 2003-03-13 WO PCT/GB2003/001072 patent/WO2003080253A1/en active IP Right Grant
- 2003-03-13 ES ES03712344T patent/ES2287455T3/es not_active Expired - Lifetime
- 2003-03-13 AT AT03712344T patent/ATE366621T1/de active
- 2003-03-13 KR KR1020047014749A patent/KR100916732B1/ko not_active IP Right Cessation
- 2003-03-13 JP JP2003578069A patent/JP2005520685A/ja active Pending
- 2003-03-13 CN CNB038114763A patent/CN1304120C/zh not_active Expired - Fee Related
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Publication number | Priority date | Publication date | Assignee | Title |
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JP2010017675A (ja) * | 2008-07-14 | 2010-01-28 | Panasonic Corp | 集塵装置 |
JP2010036054A (ja) * | 2008-07-31 | 2010-02-18 | Sumco Corp | サイクロン集塵装置及び単結晶引き上げシステム |
KR101267878B1 (ko) | 2011-09-07 | 2013-05-27 | 한국에너지기술연구원 | 고압상태의 선회유동을 이용한 입자분리장치 |
Also Published As
Publication number | Publication date |
---|---|
DE60314852T2 (de) | 2007-11-08 |
AU2003216809A1 (en) | 2003-10-08 |
ATE366621T1 (de) | 2007-08-15 |
CN1304120C (zh) | 2007-03-14 |
KR20040101325A (ko) | 2004-12-02 |
ZA200407413B (en) | 2005-10-06 |
ES2287455T3 (es) | 2007-12-16 |
CN1655873A (zh) | 2005-08-17 |
EP1487588B1 (en) | 2007-07-11 |
DE60314852D1 (de) | 2007-08-23 |
EP1487588A1 (en) | 2004-12-22 |
KR100916732B1 (ko) | 2009-09-14 |
US7323038B2 (en) | 2008-01-29 |
WO2003080253A1 (en) | 2003-10-02 |
US20050126394A1 (en) | 2005-06-16 |
WO2003080253A8 (en) | 2004-10-28 |
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