JP2003504427A5 - - Google Patents
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- Publication number
- JP2003504427A5 JP2003504427A5 JP2001508228A JP2001508228A JP2003504427A5 JP 2003504427 A5 JP2003504427 A5 JP 2003504427A5 JP 2001508228 A JP2001508228 A JP 2001508228A JP 2001508228 A JP2001508228 A JP 2001508228A JP 2003504427 A5 JP2003504427 A5 JP 2003504427A5
- Authority
- JP
- Japan
- Prior art keywords
- acid
- microcrystalline cellulose
- pulp
- less
- peroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 claims 33
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims 13
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims 13
- 239000008108 microcrystalline cellulose Substances 0.000 claims 13
- 229940016286 microcrystalline cellulose Drugs 0.000 claims 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 6
- 239000002253 acid Substances 0.000 claims 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 5
- 239000001301 oxygen Substances 0.000 claims 5
- 229910052760 oxygen Inorganic materials 0.000 claims 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical group OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 150000004965 peroxy acids Chemical class 0.000 claims 4
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 3
- 239000011707 mineral Substances 0.000 claims 3
- 238000006116 polymerization reaction Methods 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- 230000002378 acidificating effect Effects 0.000 claims 2
- LSXWFXONGKSEMY-UHFFFAOYSA-N di-tert-butyl peroxide Chemical compound CC(C)(C)OOC(C)(C)C LSXWFXONGKSEMY-UHFFFAOYSA-N 0.000 claims 2
- ZQMIGQNCOMNODD-UHFFFAOYSA-N diacetyl peroxide Chemical compound CC(=O)OOC(C)=O ZQMIGQNCOMNODD-UHFFFAOYSA-N 0.000 claims 2
- 230000007062 hydrolysis Effects 0.000 claims 2
- 238000006460 hydrolysis reaction Methods 0.000 claims 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- 150000007524 organic acids Chemical class 0.000 claims 2
- 150000002978 peroxides Chemical class 0.000 claims 2
- WYNZXNXFHYJUTE-UHFFFAOYSA-N 1,2-dioxetanedione Chemical compound O=C1OOC1=O WYNZXNXFHYJUTE-UHFFFAOYSA-N 0.000 claims 1
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims 1
- RNXKQMBYNVOCNC-UHFFFAOYSA-N 2-methylpentanoyl 2-methylpentaneperoxoate Chemical compound CCCC(C)C(=O)OOC(=O)C(C)CCC RNXKQMBYNVOCNC-UHFFFAOYSA-N 0.000 claims 1
- FRIBMENBGGCKPD-UHFFFAOYSA-N 3-(2,3-dimethoxyphenyl)prop-2-enal Chemical compound COC1=CC=CC(C=CC=O)=C1OC FRIBMENBGGCKPD-UHFFFAOYSA-N 0.000 claims 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- 239000004342 Benzoyl peroxide Substances 0.000 claims 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims 1
- YIVJZNGAASQVEM-UHFFFAOYSA-N Lauroyl peroxide Chemical compound CCCCCCCCCCCC(=O)OOC(=O)CCCCCCCCCCC YIVJZNGAASQVEM-UHFFFAOYSA-N 0.000 claims 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims 1
- 235000011054 acetic acid Nutrition 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- 235000019400 benzoyl peroxide Nutrition 0.000 claims 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims 1
- 239000004327 boric acid Substances 0.000 claims 1
- 150000001735 carboxylic acids Chemical class 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 150000002432 hydroperoxides Chemical class 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 229910017604 nitric acid Inorganic materials 0.000 claims 1
- 150000001451 organic peroxides Chemical class 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- FHHJDRFHHWUPDG-UHFFFAOYSA-N peroxysulfuric acid Chemical compound OOS(O)(=O)=O FHHJDRFHHWUPDG-UHFFFAOYSA-N 0.000 claims 1
- 238000011084 recovery Methods 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14222299P | 1999-07-02 | 1999-07-02 | |
| US60/142,222 | 1999-07-02 | ||
| PCT/US2000/018127 WO2001002441A1 (en) | 1999-07-02 | 2000-06-30 | Treatment of pulp to produce microcrystalline cellulose |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2003504427A JP2003504427A (ja) | 2003-02-04 |
| JP2003504427A5 true JP2003504427A5 (https=) | 2005-12-22 |
Family
ID=22499050
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2001508228A Pending JP2003504427A (ja) | 1999-07-02 | 2000-06-30 | 微結晶セルロースを製造するためのパルプの処理 |
Country Status (14)
| Country | Link |
|---|---|
| US (2) | US20030131957A1 (https=) |
| EP (1) | EP1226179A4 (https=) |
| JP (1) | JP2003504427A (https=) |
| KR (1) | KR100520813B1 (https=) |
| AU (1) | AU766766C (https=) |
| BR (1) | BR0012204A (https=) |
| CA (1) | CA2377732A1 (https=) |
| FI (1) | FI20012604L (https=) |
| HU (1) | HUP0204334A2 (https=) |
| IL (1) | IL147427A0 (https=) |
| MX (1) | MXPA02000073A (https=) |
| NO (1) | NO20016405L (https=) |
| TW (1) | TWI225491B (https=) |
| WO (1) | WO2001002441A1 (https=) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005537347A (ja) * | 2002-07-26 | 2005-12-08 | エフ エム シー コーポレーション | 微結晶質セルロースの製造 |
| US20060223992A1 (en) * | 2005-03-31 | 2006-10-05 | Mengkui Luo | Microcrystalline cellulose and method for making |
| US20060219376A1 (en) * | 2005-03-31 | 2006-10-05 | Mengkui Luo | Microcrystalline cellulose and method for making |
| BRPI0612651A2 (pt) * | 2005-07-08 | 2017-06-20 | Biopulping Int Inc | métodos para a formação de polpa de um material de lignocelulose fibrosa, para produzir polpa de um material de lignocelulose fibrosa, e, para tratar do material de lignocelulose fibrosa |
| US20070128325A1 (en) * | 2005-12-05 | 2007-06-07 | Conopco, Inc., D/B/A Unilever | Reduced oil dressing composition and a method for making the same |
| KR100924950B1 (ko) * | 2007-09-18 | 2009-11-06 | 한국에너지기술연구원 | 셀룰로우스 섬유를 열처리하여 얻어진 마이크로튜블 하니컴탄소체 및 그 제조방법, 이 마이크로튜블 하니컴 탄소체를이용한 마이크로튜블 반응기 모듈 및 그 제조방법, 이마이크로튜블 반응기 모듈을 이용한 마이크로 촉매반응장치 |
| CA2994066A1 (en) | 2008-12-03 | 2010-06-10 | Synergy Pharmaceuticals, Inc. | Formulations of guanylate cyclase c agonists and methods of use |
| JP5544747B2 (ja) * | 2009-04-21 | 2014-07-09 | 王子ホールディングス株式会社 | 微細繊維状セルロースの製造方法 |
| WO2010138941A2 (en) * | 2009-05-28 | 2010-12-02 | Gp Cellulose Gmbh | Modified cellulose from chemical kraft fiber and methods of making and using the same |
| RU2395636C1 (ru) * | 2009-07-13 | 2010-07-27 | Учреждение Российской академии наук Институт химии и химической технологии Сибирского отделения РАН (ИХХТ СО РАН) | Способ получения микрокристаллической целлюлозы из автогидролизованной древесины |
| DE102009029086B4 (de) | 2009-09-02 | 2015-03-12 | Schott Ag | Solarisationsbeständiges Glas, Verfahren zu seiner Herstellung und seine Verwendung |
| EP2621509A4 (en) | 2010-09-15 | 2016-08-03 | Synergy Pharmaceuticals Inc | FORMULATIONS OF GUANYLATE CYCLASE C AGONISTS AND METHOD OF USE |
| US9616097B2 (en) * | 2010-09-15 | 2017-04-11 | Synergy Pharmaceuticals, Inc. | Formulations of guanylate cyclase C agonists and methods of use |
| WO2013002742A1 (en) | 2011-06-27 | 2013-01-03 | Bukocel, A.S. | Method for preparing powdered cellulose |
| US20130274149A1 (en) * | 2012-04-13 | 2013-10-17 | Schlumberger Technology Corporation | Fluids and methods including nanocellulose |
| JP5953909B2 (ja) * | 2012-04-27 | 2016-07-20 | 王子ホールディングス株式会社 | 溶解パルプの製造方法 |
| EP2994758B1 (en) | 2013-05-08 | 2017-12-20 | Opthea Limited | Biomarkers for age-related macular degeneration (amd) |
| WO2015037424A1 (ja) | 2013-09-12 | 2015-03-19 | 三菱瓦斯化学株式会社 | セルロースの製造方法 |
| RU2542562C1 (ru) * | 2014-01-27 | 2015-02-20 | Закрытое акционерное общество "Инновационный центр "Бирюч" (ЗАО "ИЦ "Бирюч") | Способ получения микрокристаллической целлюлозы для производства картона |
| KR101686550B1 (ko) * | 2014-08-12 | 2016-12-16 | 한국원자력연구원 | 나노셀룰로오스의 제조방법 |
| US20170332684A1 (en) | 2014-11-03 | 2017-11-23 | Fmc Corporation | Effective plant protein drink stabilizers comprising colloidal microcrystalline cellulose made from non-dissolving cellulose pulp |
| JP2018070665A (ja) * | 2015-03-09 | 2018-05-10 | 三菱瓦斯化学株式会社 | セルロースの製造方法 |
| JP2018070664A (ja) * | 2015-03-09 | 2018-05-10 | 三菱瓦斯化学株式会社 | セルロースの製造方法 |
| US10597820B2 (en) * | 2015-05-14 | 2020-03-24 | DuPont Nutrition USA, Inc. | Method of making bleached microcrystalline cellulose |
| JP6187619B2 (ja) * | 2016-03-07 | 2017-08-30 | 王子ホールディングス株式会社 | 溶解パルプの製造方法 |
| KR101915102B1 (ko) * | 2018-04-26 | 2018-11-05 | 주식회사 동구 | 크리스탈 나노 셀룰로오스의 제조방법 |
| CA3224383A1 (en) * | 2023-12-21 | 2025-10-30 | Sixring Inc. | Process for obtaining alpha cellulose |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE564287A (https=) * | 1957-01-28 | |||
| CA973661A (en) * | 1972-09-29 | 1975-09-02 | Pulp And Paper Research Institute Of Canada | Press alkaline extraction of cellulosic pulp |
| BG19462A1 (https=) * | 1973-08-02 | 1975-06-25 | ||
| US4745058A (en) * | 1984-05-10 | 1988-05-17 | Townsley Philip M | Method for producing cellulosic fibers and microcrystalline cellulose |
| US4756800A (en) * | 1986-09-03 | 1988-07-12 | The United States Of America As Represented By The Secretary Of Agriculture | Method for producing salts of monoperoxysulfuric acid and simultaneously bleaching pulp |
| SU1520066A1 (ru) * | 1987-07-01 | 1989-11-07 | Институт химии им.В.И.Никитина | Способ получени микрокристаллической целлюлозы |
| US5405953A (en) * | 1993-08-03 | 1995-04-11 | Biocontrol Incorporated | Microfibrillated oxycellulose |
| DE4342442C2 (de) * | 1993-12-13 | 1996-11-21 | Akzo Nobel Nv | Verfahren zur Herstellung von Level-off DP Cellulose (LODP Cellulose) und ihre Desaggregierung zu mikrokristalliner Cellulose |
| FR2730252B1 (fr) * | 1995-02-08 | 1997-04-18 | Generale Sucriere Sa | Cellulose microfibrillee et son procede d'obtention a partir de pulpe de vegetaux a parois primaires, notamment a partir de pulpe de betteraves sucrieres. |
| US5665414A (en) * | 1995-04-06 | 1997-09-09 | Edward Mendell Co., Inc. | Cellulosic materials for incorporation into food products and methods of making same |
| US5769934A (en) * | 1997-01-15 | 1998-06-23 | Fmc Corporation | Method for producing microcrystalline cellulose |
| RU2119986C1 (ru) * | 1997-07-14 | 1998-10-10 | Институт химии Коми научного центра Уральского отделения РАН | Способ получения микрокристаллической целлюлозы |
-
2000
- 2000-06-30 CA CA002377732A patent/CA2377732A1/en not_active Abandoned
- 2000-06-30 KR KR10-2002-7000004A patent/KR100520813B1/ko not_active Expired - Fee Related
- 2000-06-30 AU AU57832/00A patent/AU766766C/en not_active Ceased
- 2000-06-30 BR BR0012204-1A patent/BR0012204A/pt not_active IP Right Cessation
- 2000-06-30 JP JP2001508228A patent/JP2003504427A/ja active Pending
- 2000-06-30 FI FI20012604A patent/FI20012604L/fi not_active IP Right Cessation
- 2000-06-30 WO PCT/US2000/018127 patent/WO2001002441A1/en not_active Ceased
- 2000-06-30 EP EP20000943347 patent/EP1226179A4/en not_active Withdrawn
- 2000-06-30 MX MXPA02000073A patent/MXPA02000073A/es not_active Application Discontinuation
- 2000-06-30 HU HU0204334A patent/HUP0204334A2/hu unknown
- 2000-06-30 IL IL14742700A patent/IL147427A0/xx unknown
- 2000-07-01 TW TW089113064A patent/TWI225491B/zh not_active IP Right Cessation
-
2001
- 2001-12-28 NO NO20016405A patent/NO20016405L/no not_active Application Discontinuation
-
2002
- 2002-11-20 US US10/301,526 patent/US20030131957A1/en not_active Abandoned
-
2004
- 2004-10-04 US US10/958,188 patent/US20050145351A1/en not_active Abandoned
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