IT1272110B - Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopo - Google Patents
Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopoInfo
- Publication number
- IT1272110B IT1272110B ITMI930519A ITMI930519A IT1272110B IT 1272110 B IT1272110 B IT 1272110B IT MI930519 A ITMI930519 A IT MI930519A IT MI930519 A ITMI930519 A IT MI930519A IT 1272110 B IT1272110 B IT 1272110B
- Authority
- IT
- Italy
- Prior art keywords
- procedure
- determination
- heavy hydrocarbons
- rock
- useful equipment
- Prior art date
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/24—Earth materials
- G01N33/241—Earth materials for hydrocarbon content
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/025—Gas chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/121—Preparation by evaporation cooling; cold traps
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/12—Preparation by evaporation
- G01N2030/126—Preparation by evaporation evaporating sample
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- General Health & Medical Sciences (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Remote Sensing (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
Procedimento per separare ed analizzare gli idrocarburi, particolarmente quelli pesanti, contenuti in rocce sedimentarie, che comprende:A) caricamento in un tubicino portacampioni del campione di roccia sedimentaria e di uno o più solventi inerti;B) preriscaldamento del tubicino portacampioni;C) allontanamento del solvente e degli idrocarburi precedentemente contenuti nella roccia;D) condensazione ed invio ad un mezzo di separazione e di analisi.La presente invenzione comprende anche una apparecchiatura utile alla realizzazione del suddetto procedimento.
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITMI930519A IT1272110B (it) | 1993-03-19 | 1993-03-19 | Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopo |
EP94200658A EP0616214A1 (en) | 1993-03-19 | 1994-03-15 | Method and apparatus for determining heavy hydrocarbons in rock matrices |
US08/213,707 US5390529A (en) | 1993-03-19 | 1994-03-16 | Method for determining heavy hydrocarbons in rock matrices and the apparatus for the purpose |
NO940971A NO940971L (no) | 1993-03-19 | 1994-03-17 | Fremgangsmåte og apparat for å bestemme tunge hydrokarboner i bergarter |
CN94102931.XA CN1094163A (zh) | 1993-03-19 | 1994-03-18 | 脉石中的重烃的鉴定方法及其装置 |
JP6074044A JPH06324024A (ja) | 1993-03-19 | 1994-03-18 | 炭化水素の分離及び分析法及びその装置 |
CA002119415A CA2119415A1 (en) | 1993-03-19 | 1994-03-18 | Method for determining heavy hydrocarbons in rock matrices and the apparatus for the purpose |
BR9401210A BR9401210A (pt) | 1993-03-19 | 1994-03-18 | Método para separar e analisar os hidrocarbonetos, particularmente, hidrocarbonetos pesados, em matrizes de rocha e aparelho para esta finalidade |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITMI930519A IT1272110B (it) | 1993-03-19 | 1993-03-19 | Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopo |
Publications (3)
Publication Number | Publication Date |
---|---|
ITMI930519A0 ITMI930519A0 (it) | 1993-03-19 |
ITMI930519A1 ITMI930519A1 (it) | 1994-09-19 |
IT1272110B true IT1272110B (it) | 1997-06-11 |
Family
ID=11365399
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ITMI930519A IT1272110B (it) | 1993-03-19 | 1993-03-19 | Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopo |
Country Status (8)
Country | Link |
---|---|
US (1) | US5390529A (it) |
EP (1) | EP0616214A1 (it) |
JP (1) | JPH06324024A (it) |
CN (1) | CN1094163A (it) |
BR (1) | BR9401210A (it) |
CA (1) | CA2119415A1 (it) |
IT (1) | IT1272110B (it) |
NO (1) | NO940971L (it) |
Families Citing this family (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5719323A (en) * | 1996-04-12 | 1998-02-17 | The United States Of America As Represented By The Secretary Of The Army | Method of measuring the decomposition of a gaseous material under controlled temperature and time conditions |
CA2293778A1 (en) * | 1997-06-12 | 1998-12-17 | Biosensor Applications Sweden Ab | Apparatus, system and method for the detection of an analyte in air |
DE19810109C2 (de) * | 1998-03-10 | 2000-02-10 | Gerstel Gmbh & Co Kg | Gaschromatograph mit einem temperaturgesteuerten Injektor |
CN1308678C (zh) * | 2005-04-21 | 2007-04-04 | 张刘平 | 土壤吸附烃低温解吸装置及方法 |
DE102009003429B3 (de) * | 2009-02-04 | 2010-07-01 | Joint Analytical Systems Gmbh | Vorrichtung und Verfahren zum Aufbereiten von Proben für die Gaschromatografie |
ITMI20122080A1 (it) * | 2012-12-05 | 2014-06-06 | Geolog S R L | Strumento per la misura totale o frazionata di idrocarburi in un campione solido. |
CN104749303A (zh) * | 2013-12-26 | 2015-07-01 | 中国石油化工股份有限公司 | 泥页岩热释c5~c14烃的制备及在线色谱分析方法 |
CN105606703B (zh) * | 2016-01-28 | 2018-07-31 | 中国石油大学(华东) | 页岩吸附气和游离气的计算方法及其测量装置 |
US10578600B2 (en) * | 2017-08-17 | 2020-03-03 | Saudi Arabian Oil Company | Decontaminating rock samples by thermovaporization |
US10760418B1 (en) * | 2018-04-23 | 2020-09-01 | Revochem Llc | Method and system for preserving and obtaining hydrocarbon information from organic-rich rock samples |
US10753912B2 (en) * | 2018-07-11 | 2020-08-25 | Shimadzu Corporation | Gas chromatograph |
US11492541B2 (en) | 2019-07-24 | 2022-11-08 | Saudi Arabian Oil Company | Organic salts of oxidizing anions as energetic materials |
US11319478B2 (en) | 2019-07-24 | 2022-05-03 | Saudi Arabian Oil Company | Oxidizing gasses for carbon dioxide-based fracturing fluids |
US11352548B2 (en) | 2019-12-31 | 2022-06-07 | Saudi Arabian Oil Company | Viscoelastic-surfactant treatment fluids having oxidizer |
WO2021138355A1 (en) | 2019-12-31 | 2021-07-08 | Saudi Arabian Oil Company | Viscoelastic-surfactant fracturing fluids having oxidizer |
RU2745752C1 (ru) * | 2020-04-30 | 2021-03-31 | Общество с ограниченной ответственностью "УК "Служба Внутреннего Контроля" | Пробоотборные устройства непрерывного и циклического типа и способ обнаружения компонентов смеси с использованием пробоотборных устройств |
US11773715B2 (en) | 2020-09-03 | 2023-10-03 | Saudi Arabian Oil Company | Injecting multiple tracer tag fluids into a wellbore |
US11542815B2 (en) | 2020-11-30 | 2023-01-03 | Saudi Arabian Oil Company | Determining effect of oxidative hydraulic fracturing |
US11660595B2 (en) | 2021-01-04 | 2023-05-30 | Saudi Arabian Oil Company | Microfluidic chip with multiple porosity regions for reservoir modeling |
US12019038B2 (en) | 2021-01-21 | 2024-06-25 | Saudi Arabian Oil Company | Evaluation of source rock samples from subterranean reservoirs |
US11534759B2 (en) | 2021-01-22 | 2022-12-27 | Saudi Arabian Oil Company | Microfluidic chip with mixed porosities for reservoir modeling |
US12071589B2 (en) | 2021-10-07 | 2024-08-27 | Saudi Arabian Oil Company | Water-soluble graphene oxide nanosheet assisted high temperature fracturing fluid |
US12025589B2 (en) | 2021-12-06 | 2024-07-02 | Saudi Arabian Oil Company | Indentation method to measure multiple rock properties |
US12012550B2 (en) | 2021-12-13 | 2024-06-18 | Saudi Arabian Oil Company | Attenuated acid formulations for acid stimulation |
US11885790B2 (en) | 2021-12-13 | 2024-01-30 | Saudi Arabian Oil Company | Source productivity assay integrating pyrolysis data and X-ray diffraction data |
US12000278B2 (en) | 2021-12-16 | 2024-06-04 | Saudi Arabian Oil Company | Determining oil and water production rates in multiple production zones from a single production well |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2492401A (en) * | 1945-02-24 | 1949-12-27 | Lummus Co | Gas adsorption |
US3346341A (en) * | 1965-06-28 | 1967-10-10 | Beckman Instruments Inc | Fragmentation inlet for gas chromatography and method of loading a sample thereinto |
US3847546A (en) * | 1972-10-04 | 1974-11-12 | Chromalytics Corp | Method and system for thermal analysis |
US4244917A (en) * | 1979-05-09 | 1981-01-13 | Conoco, Inc. | Sample pyrolysis oven |
US4305734A (en) * | 1979-09-19 | 1981-12-15 | Mcgill Incorporated | Recovery of hydrocarbon components from a hydrocarbon-carrier gas mixture |
US4384471A (en) * | 1980-12-10 | 1983-05-24 | Engelhard Minerals & Chemicals Corporation | Chromatographic analysis of hydrocarbon mixtures |
US4509855A (en) * | 1982-08-12 | 1985-04-09 | The United States Of America As Represented By The United States Department Of Energy | Dual liquid and gas chromatograph system |
GB2161269B (en) * | 1984-07-02 | 1988-08-10 | Ruska Petroleum Lab Inc | Method and apparatus for analyzing hydrogen and carbon containing materials |
FR2592488B1 (fr) * | 1985-12-30 | 1988-07-15 | Inst Francais Du Petrole | Procede et appareillage de caracterisation de la matiere organique extractible par au moins un solvant dans des conditions de temperature et de pression supercritiques. |
JPS62192657A (ja) * | 1986-02-19 | 1987-08-24 | Shimadzu Corp | 標準試料導入器付き熱分解装置 |
SU1404933A1 (ru) * | 1987-01-19 | 1988-06-23 | Предприятие П/Я В-8644 | Промышленный хроматограф |
US4919893A (en) * | 1988-05-31 | 1990-04-24 | Amoco Corporation | Thermal extraction/pyrolysis gas chromatograph |
JPH02201156A (ja) * | 1989-01-30 | 1990-08-09 | Dow Chem Nippon Kk | ガスクロマトグラフィー用熱分解装置 |
JPH02203268A (ja) * | 1989-02-02 | 1990-08-13 | Nippon Bunseki Kogyo Kk | ガスクロマトグラフの気相試料の濃縮気化分析法 |
US5242245A (en) * | 1991-08-22 | 1993-09-07 | Schellstede Herman J | Method and apparatus for vacuum enhanced thermal desorption of hydrocarbon and other contaminants from soils |
US5191211A (en) * | 1992-03-23 | 1993-03-02 | Bridgestone/Firestone, Inc. | Thermal desorption method for separating volatile additives from vulcanizable rubber |
-
1993
- 1993-03-19 IT ITMI930519A patent/IT1272110B/it active IP Right Grant
-
1994
- 1994-03-15 EP EP94200658A patent/EP0616214A1/en not_active Withdrawn
- 1994-03-16 US US08/213,707 patent/US5390529A/en not_active Expired - Fee Related
- 1994-03-17 NO NO940971A patent/NO940971L/no unknown
- 1994-03-18 BR BR9401210A patent/BR9401210A/pt not_active Application Discontinuation
- 1994-03-18 JP JP6074044A patent/JPH06324024A/ja not_active Withdrawn
- 1994-03-18 CN CN94102931.XA patent/CN1094163A/zh active Pending
- 1994-03-18 CA CA002119415A patent/CA2119415A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
NO940971D0 (no) | 1994-03-17 |
ITMI930519A0 (it) | 1993-03-19 |
CA2119415A1 (en) | 1994-09-20 |
NO940971L (no) | 1994-09-20 |
JPH06324024A (ja) | 1994-11-25 |
CN1094163A (zh) | 1994-10-26 |
EP0616214A1 (en) | 1994-09-21 |
ITMI930519A1 (it) | 1994-09-19 |
US5390529A (en) | 1995-02-21 |
BR9401210A (pt) | 1994-12-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
IT1272110B (it) | Procedimento per la determinazione di idrocarburi pesanti in matrici rocciose ed apparecchiatura utile allo scopo | |
Eigen et al. | Sorting single molecules: application to diagnostics and evolutionary biotechnology. | |
US5741412A (en) | Multiple capillary biochemical analyzer | |
Truong et al. | Data‐dependent acquisition with precursor coisolation improves proteome coverage and measurement throughput for label‐free single‐cell proteomics | |
US3150516A (en) | Analysis of gases in a liquid solution | |
ES2151902T3 (es) | Medio de separacion de globulos rojos para dosificarlos mediante union especifica. | |
ES2051303T3 (es) | Dispositivo de ensayo con puertas multiples. | |
SE9201089D0 (sv) | Detektorer foer separationsprocesser | |
CA2168250A1 (en) | Accelerated Solvent Extraction System | |
ES291778Y (es) | Aparato para la deteccion y determinacion de por lo menos un ligando en una muestra sospechosa de contener dicho ligando | |
DK0479977T3 (da) | Fremgangsmåde og apparat til cytologisk prøveklassifikation | |
DE60110256D1 (de) | Verfahren zum konzentrieren von analyten in proben | |
BR9915268A (pt) | Método e aparelho para separação de bibliotecas de catalizadores | |
US10656157B2 (en) | Rare event detection using mass tags | |
US6752914B1 (en) | Capillary electrophoresis device | |
CA2008591A1 (fr) | Procede d'analyse des spectres de relaxation et des resonances dans les materiaux | |
Juan‐García et al. | Determination of organic contaminants in food by capillary electrophoresis | |
ATE81727T1 (de) | Verfahren zur messung der radioaktivitaet von proben sowie vorrichtung zur durchfuehrung des verfahrens. | |
CN105092733B (zh) | Lc‑ms测试物中不挥发性缓冲盐含量的降低方法和装置 | |
EP1162464A1 (en) | Method and device for increasing efficiency of bioanalysis | |
EP2189792A3 (fr) | Dispositif pour séparer et/ou analyser plusieurs cibles moléculaires en solution dans un mélange complexe | |
GB1049364A (en) | An apparatus for and a method of automatically analyzing a plurality of samples | |
CN217052222U (zh) | 一种Clarity数字PCR仪用反应产物回收装置 | |
JP2001264297A (ja) | 試料分析方法及び装置 | |
EP0609450B1 (en) | Method for high-sensitivity detection of amino acid derivative |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
0001 | Granted | ||
TA | Fee payment date (situation as of event date), data collected since 19931001 |
Effective date: 19970313 |