IL43428A - Reduction of metallic chloride by powdered metal - Google Patents
Reduction of metallic chloride by powdered metalInfo
- Publication number
- IL43428A IL43428A IL43428A IL4342873A IL43428A IL 43428 A IL43428 A IL 43428A IL 43428 A IL43428 A IL 43428A IL 4342873 A IL4342873 A IL 4342873A IL 43428 A IL43428 A IL 43428A
- Authority
- IL
- Israel
- Prior art keywords
- process according
- aluminum
- manganese
- chloride
- metal
- Prior art date
Links
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 title claims 3
- 239000012255 powdered metal Substances 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract 14
- 229910052782 aluminium Inorganic materials 0.000 claims abstract 13
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract 12
- 239000011572 manganese Substances 0.000 claims abstract 12
- 229910052748 manganese Inorganic materials 0.000 claims abstract 9
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims abstract 8
- 229910052751 metal Inorganic materials 0.000 claims abstract 7
- 239000002184 metal Substances 0.000 claims abstract 7
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims abstract 6
- 239000007788 liquid Substances 0.000 claims abstract 6
- 238000006243 chemical reaction Methods 0.000 claims abstract 4
- 239000000376 reactant Substances 0.000 claims abstract 3
- 239000012530 fluid Substances 0.000 claims 4
- 239000012071 phase Substances 0.000 claims 4
- 239000007790 solid phase Substances 0.000 claims 4
- 239000000843 powder Substances 0.000 claims 3
- 229910021380 Manganese Chloride Inorganic materials 0.000 claims 2
- GLFNIEUTAYBVOC-UHFFFAOYSA-L Manganese chloride Chemical compound Cl[Mn]Cl GLFNIEUTAYBVOC-UHFFFAOYSA-L 0.000 claims 2
- 239000003638 chemical reducing agent Substances 0.000 claims 2
- 239000011565 manganese chloride Substances 0.000 claims 2
- 235000002867 manganese chloride Nutrition 0.000 claims 2
- 229910001510 metal chloride Inorganic materials 0.000 claims 2
- 101100536354 Drosophila melanogaster tant gene Proteins 0.000 claims 1
- 229910003910 SiCl4 Inorganic materials 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- FDNAPBUWERUEDA-UHFFFAOYSA-N silicon tetrachloride Chemical group Cl[Si](Cl)(Cl)Cl FDNAPBUWERUEDA-UHFFFAOYSA-N 0.000 claims 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical group Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- 239000004411 aluminium Substances 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- -1 preferably powdered Substances 0.000 abstract 2
- 229910018657 Mn—Al Inorganic materials 0.000 abstract 1
- 229910045601 alloy Inorganic materials 0.000 abstract 1
- 239000000956 alloy Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1277—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using other metals, e.g. Al, Si, Mn
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B21/00—Obtaining aluminium
- C22B21/0038—Obtaining aluminium by other processes
- C22B21/0053—Obtaining aluminium by other processes from other aluminium compounds
- C22B21/0061—Obtaining aluminium by other processes from other aluminium compounds using metals, e.g. Hg or Mn
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B5/00—General methods of reducing to metals
- C22B5/02—Dry methods smelting of sulfides or formation of mattes
- C22B5/04—Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B5/00—General methods of reducing to metals
- C22B5/02—Dry methods smelting of sulfides or formation of mattes
- C22B5/06—Dry methods smelting of sulfides or formation of mattes by carbides or the like
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Metallurgy (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Catalysts (AREA)
Abstract
1419450 Producing Al from AlCl 3 TOTH ALUMINUM CORP 16 Oct 1973 [16 Oct 1972] 48120/73 Heading C7D Aluminium is produced by reacting liquid or gaseous aluminium chloride with solid, preferably powdered, manganese at temperatures and pressures at which the reactants maintain their respective phases, the preferred range being 180 to 600C 1 to 30 atmospheres. Although aluminium metal is normally separated from the product it is possible to produce an Mn-Al alloy ingot by this method. The reactions may be carried out with the AlCl 3 in gaseous form by passing the gas through a bed of Mn particles, Fig. (not shown); if the AlCl 3 is liquid it is added to a charge of Mn particles, Fig.2 (not shown), the process being adapted for batch operation Fig.3 (not shown) or continuous operation, Fig.4 (not shown). Inert metal salts, e.g. NaCl, CaCl 2 , KCI, MgCl 2 or BaCl 2 may be added to lower the vapour pressure of the AlCl 3 .
[GB1419450A]
Claims (1)
1. 6. A process according to. Claim 1 wherein the chloride in fluid phase is titanium chloride and the reduc.tant' metal in solid phase is aluminum. 7. A process according, to Claim 1 wherein the metal chloride in fluid phase is aluminum chloride and the . rcductant metal in solid phase is manganese. . 8.· A process according to Claim 7 wherein the reaction is carried out in a temperature range between 180-606°C and pressure range of from 15-450 psia.. 9. A process according to Claim .7 wherein the aluminum chloride is in gaseous form and including the steps of passing the gas ous .AlCl^ through a bed- of manganese in powder form to form HnCl, and aluminum; and separating the so produced aluminum from the, Mn'C -, and manganese. " : .10. A process according to Claim 9 wherein the gaseous A1C13 and Hn react at' temperature of from approximately 300--600°C and 15-450psia pressure. 11. A process according to Claim 10 wherein sai produced aluminum is';-: alloyed with Tin and takes the form of Αΐ6Ι·ίη, ,/d^in, Al o . A1 n5. . 12. A process according to Claim 8 wherein the .. . * AICI3 is: in liquid form and the manganese is in powde form, including the furthe step's of introducing -the . < liquid /.ICI3 and powdered- manganese into a closable vessel; agitating the reactants at a temperature of from 180-600°C and. a pressure of from 15-450 psia to form aluminum and MnCl^; · and removing the MnCl2 from the aluminum. 13. A process according to Claim 8 wherein the AICI3" is in liquid form and the manganese is in powder form, including the further steps of introducing the liquid AlCl^ and the powder manganese from opposite ends of a reactor and' passing the reactants in counter- curren fashion to achieve continuous . production o'f aluminum and MnCl^; and removing the MnCl2 from the ■ ' ' · . , '· · ' . \ ; ' ·' aluminum.. \ . 1 ■ 14. A process according to Claim 1 wherein the metal . chloride in fluid phase, is siCl_j and the reductant metal in solid phase is manganese. . 15. A process according to Claim 13 wherein the reaction Is carried out in a . temperature range between about T-70°C and -1040°C and a pressure range of .from 15-550 psia. 16. A process according to Claim 1 wherein the .·■'■· metal chloride' in fluid phase is SiCl4 and the reductant metal in solid phase is aluminum. ., .* 17. A process according' to Claim 15 wherein the reaction is carried out in a temperature range between about -70°C to 577°C. and a pressure range of' from 15-550 psia. · · · ■ .. . COHEN ZEDE & SPISBACH P. 0. Box 331 16 , T e l - A v i v Attorneys f o r A p p l i c a n t
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US297695A US3900312A (en) | 1972-10-16 | 1972-10-16 | Reduction of aluminum chloride by manganese |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IL43428A0 IL43428A0 (en) | 1974-01-14 |
| IL43428A true IL43428A (en) | 1976-05-31 |
Family
ID=23147359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL43428A IL43428A (en) | 1972-10-16 | 1973-10-15 | Reduction of metallic chloride by powdered metal |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US3900312A (en) |
| JP (1) | JPS4974109A (en) |
| AR (1) | AR201746A1 (en) |
| AT (1) | ATA849873A (en) |
| BE (1) | BE805797A (en) |
| BR (1) | BR7308093D0 (en) |
| DD (1) | DD108324A5 (en) |
| DE (1) | DE2348450A1 (en) |
| ES (1) | ES419700A1 (en) |
| FR (1) | FR2202946B1 (en) |
| GB (1) | GB1419450A (en) |
| HU (1) | HU167894B (en) |
| IL (1) | IL43428A (en) |
| IS (1) | IS948B6 (en) |
| IT (1) | IT995540B (en) |
| NL (1) | NL7314252A (en) |
| NO (1) | NO134304C (en) |
| OA (1) | OA04493A (en) |
| RO (1) | RO67591A (en) |
| ZA (1) | ZA737706B (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1092787A (en) * | 1976-03-15 | 1981-01-06 | Westinghouse Electric Corporation | Chlorination process for producing aluminum |
| US4035180A (en) * | 1976-03-16 | 1977-07-12 | Toth Aluminum Corporation | Catalytic process for the reduction of aluminum chloride by manganese |
| JPS6067603A (en) * | 1983-09-21 | 1985-04-18 | Toho Aen Kk | Treatment of ultrafine metal powder |
| US6143362A (en) | 1998-02-25 | 2000-11-07 | Micron Technology, Inc. | Chemical vapor deposition of titanium |
| US6284316B1 (en) | 1998-02-25 | 2001-09-04 | Micron Technology, Inc. | Chemical vapor deposition of titanium |
| US6955703B2 (en) * | 2002-12-26 | 2005-10-18 | Millennium Inorganic Chemicals, Inc. | Process for the production of elemental material and alloys |
| US20060183958A1 (en) * | 2003-04-01 | 2006-08-17 | Breneman William C | Process for the treatment of waste metal chlorides |
| KR101148573B1 (en) * | 2003-07-04 | 2012-05-21 | 커먼웰쓰 사이언티픽 앤드 인더스트리얼 리서치 오가니제이션 | A method and apparatus for the production of metal compounds |
| ES2394851T3 (en) * | 2006-03-27 | 2013-02-06 | Commonwealth Scientific And Industrial Research Organisation | Apparatus and methods for the production of metal compounds |
| CN102065992B (en) | 2008-04-21 | 2014-07-30 | 联邦科学及工业研究组织 | Method and apparatus for forming titanium-aluminium based alloys |
| CA2784196C (en) * | 2009-12-18 | 2019-12-10 | Jawad Haidar | Method for producing low aluminium titanium-aluminium alloys |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2452665A (en) * | 1944-03-31 | 1948-11-02 | Electro Metallurgical Co | Process for the separation of metals |
| US2847205A (en) * | 1954-10-13 | 1958-08-12 | Nat Res Corp | Production of metals |
| US3161500A (en) * | 1961-08-04 | 1964-12-15 | Aluminium Lab Ltd | Protection of graphite surfaces from attack by aluminum monohalide |
| US3455678A (en) * | 1967-01-16 | 1969-07-15 | Ethyl Corp | Process for the concurrent production of aif3 and a metallic titanium product |
-
1972
- 1972-10-16 US US297695A patent/US3900312A/en not_active Expired - Lifetime
-
1973
- 1973-09-26 DE DE19732348450 patent/DE2348450A1/en active Pending
- 1973-10-01 IT IT29602/73A patent/IT995540B/en active
- 1973-10-02 ZA ZA737706A patent/ZA737706B/en unknown
- 1973-10-04 AT AT849873A patent/ATA849873A/en not_active Application Discontinuation
- 1973-10-05 IS IS2178A patent/IS948B6/en unknown
- 1973-10-08 BE BE136454A patent/BE805797A/en unknown
- 1973-10-11 NO NO3948/73A patent/NO134304C/no unknown
- 1973-10-13 OA OA55037A patent/OA04493A/en unknown
- 1973-10-15 IL IL43428A patent/IL43428A/en unknown
- 1973-10-16 JP JP48116256A patent/JPS4974109A/ja active Pending
- 1973-10-16 DD DD174088A patent/DD108324A5/xx unknown
- 1973-10-16 BR BR8093/73A patent/BR7308093D0/en unknown
- 1973-10-16 NL NL7314252A patent/NL7314252A/xx unknown
- 1973-10-16 ES ES419700A patent/ES419700A1/en not_active Expired
- 1973-10-16 AR AR250546A patent/AR201746A1/en active
- 1973-10-16 GB GB4812073A patent/GB1419450A/en not_active Expired
- 1973-10-16 FR FR7336935A patent/FR2202946B1/fr not_active Expired
- 1973-10-16 HU HUAI229A patent/HU167894B/hu not_active IP Right Cessation
- 1973-10-16 RO RO7376351A patent/RO67591A/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE805797A (en) | 1974-04-08 |
| NO134304B (en) | 1976-06-08 |
| FR2202946A1 (en) | 1974-05-10 |
| HU167894B (en) | 1976-01-28 |
| BR7308093D0 (en) | 1974-07-11 |
| IL43428A0 (en) | 1974-01-14 |
| ZA737706B (en) | 1974-08-28 |
| OA04493A (en) | 1980-03-30 |
| IS948B6 (en) | 1976-08-09 |
| NO134304C (en) | 1976-09-15 |
| ES419700A1 (en) | 1976-04-16 |
| AR201746A1 (en) | 1975-04-15 |
| DE2348450A1 (en) | 1974-04-25 |
| RO67591A (en) | 1981-08-17 |
| DD108324A5 (en) | 1974-09-12 |
| JPS4974109A (en) | 1974-07-17 |
| IT995540B (en) | 1975-11-20 |
| IS2178A7 (en) | 1973-11-02 |
| US3900312A (en) | 1975-08-19 |
| NL7314252A (en) | 1974-04-18 |
| ATA849873A (en) | 1976-11-15 |
| AU6100473A (en) | 1975-04-10 |
| GB1419450A (en) | 1975-12-31 |
| FR2202946B1 (en) | 1977-09-09 |
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