HUP9800615A2 - Eljárás bisz(hidroxi-metil)-vegyületek előállítására - Google Patents
Eljárás bisz(hidroxi-metil)-vegyületek előállításáraInfo
- Publication number
- HUP9800615A2 HUP9800615A2 HU9800615A HUP9800615A HUP9800615A2 HU P9800615 A2 HUP9800615 A2 HU P9800615A2 HU 9800615 A HU9800615 A HU 9800615A HU P9800615 A HUP9800615 A HU P9800615A HU P9800615 A2 HUP9800615 A2 HU P9800615A2
- Authority
- HU
- Hungary
- Prior art keywords
- compounds
- general formula
- formula
- reaction
- anhydrous
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- -1 bis-hydroxy-methyl Chemical class 0.000 title 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- 150000003868 ammonium compounds Chemical class 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000012264 purified product Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 230000009466 transformation Effects 0.000 abstract 1
- 238000000844 transformation Methods 0.000 abstract 1
- 239000002351 wastewater Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
- C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
- C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
A találmány tárgya eljárás az (I) általánős képletű bisz-(hidrőxi-metil)-vegyületek előállítására - ahől az (I) képletben X1 és X2azőnős vagy különböző elektrőnvőnzó csőpőrtőt jelent - a (II)általánős képletű C-H-acid vegyületek - ahől a (II) képletben X1 és X2jelentése a fenti - és főrmaldehid reakciójával. A találmány szerintieljárásra jellemző, hőgy ezt a reakciót vízmentes közegben hajtjákvégre. A találmány különös előnye, hőgy az (I) általánős képletű vegyületekvízmentes, vagy lényegében vízmentes közegben állíthatók elő, ésáltalában az előállításűk reakcióelegyében tővábbi átalakításőknakvethetők alá izőlálás vagy tisztítás nélkül, így a kapőtt hőzamőkmegközelítik azőkat a hőzamőkat, amelyeket izőlált és tisztítőtttermékekkel lehet elérni. A vízmentes körülmények közöttfőganatősítőtt eljárás tővábbi előnye, hőgy szennyvizek nemtermelődnek, és más termékek, példáűl nitrőgéntartalmú vegyületek(ammóniűmvegyületek) megsemmisítésének nehézségei nem lépnek fel. ŕ
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19711762A DE19711762A1 (de) | 1997-03-21 | 1997-03-21 | Verfahren zur Herstellung von Bishydroxymethylverbindungen |
Publications (3)
Publication Number | Publication Date |
---|---|
HU9800615D0 HU9800615D0 (en) | 1998-05-28 |
HUP9800615A2 true HUP9800615A2 (hu) | 1999-01-28 |
HUP9800615A3 HUP9800615A3 (en) | 2000-04-28 |
Family
ID=7824094
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU9800615A HUP9800615A3 (en) | 1997-03-21 | 1998-03-20 | Process for producing bis-hydroxy-methyl derivatives |
Country Status (5)
Country | Link |
---|---|
US (1) | US5902896A (hu) |
EP (1) | EP0866047B1 (hu) |
JP (1) | JPH10279506A (hu) |
DE (2) | DE19711762A1 (hu) |
HU (1) | HUP9800615A3 (hu) |
Families Citing this family (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9249265B1 (en) | 2014-09-08 | 2016-02-02 | Sirrus, Inc. | Emulsion polymers including one or more 1,1-disubstituted alkene compounds, emulsion methods, and polymer compositions |
US10414839B2 (en) | 2010-10-20 | 2019-09-17 | Sirrus, Inc. | Polymers including a methylene beta-ketoester and products formed therefrom |
US9279022B1 (en) | 2014-09-08 | 2016-03-08 | Sirrus, Inc. | Solution polymers including one or more 1,1-disubstituted alkene compounds, solution polymerization methods, and polymer compositions |
US9828324B2 (en) | 2010-10-20 | 2017-11-28 | Sirrus, Inc. | Methylene beta-diketone monomers, methods for making methylene beta-diketone monomers, polymerizable compositions and products formed therefrom |
EP2632889B1 (en) | 2010-10-28 | 2018-08-29 | Mapi Pharma Limited | Intermediate compounds and process for the preparation of fingolimod |
US9221739B2 (en) | 2011-10-19 | 2015-12-29 | Sirrus, Inc. | Methylene beta-diketone monomers, methods for making methylene beta-diketone monomers, polymerizable compositions and products formed therefrom |
CA2869108A1 (en) | 2012-03-30 | 2013-10-03 | Bioformix Inc. | Methods for activating polymerizable compositions, polymerizable systems, and products formed thereby |
US10913875B2 (en) | 2012-03-30 | 2021-02-09 | Sirrus, Inc. | Composite and laminate articles and polymerizable systems for producing the same |
WO2013149173A1 (en) | 2012-03-30 | 2013-10-03 | Bioformix Inc. | Ink and coating formulations and polymerizable systems for producing the same |
WO2013181600A2 (en) | 2012-06-01 | 2013-12-05 | Bioformix Inc. | Optical material and articles formed therefrom |
CN102775808B (zh) * | 2012-08-23 | 2013-08-21 | 楚源高新科技集团股份有限公司 | 一种利用t酸母液废水回收硫酸铵和合成酸性染料的工艺 |
WO2014078689A1 (en) | 2012-11-16 | 2014-05-22 | Bioformix Inc. | Plastics bonding systems and methods |
EP2926368B1 (en) | 2012-11-30 | 2020-04-08 | Sirrus, Inc. | Electronic assembly |
CN110204441A (zh) | 2013-01-11 | 2019-09-06 | 瑟拉斯公司 | 经过双(羟甲基)丙二酸酯的途径获得亚甲基丙二酸酯的方法 |
US9416091B1 (en) | 2015-02-04 | 2016-08-16 | Sirrus, Inc. | Catalytic transesterification of ester compounds with groups reactive under transesterification conditions |
US9315597B2 (en) | 2014-09-08 | 2016-04-19 | Sirrus, Inc. | Compositions containing 1,1-disubstituted alkene compounds for preparing polymers having enhanced glass transition temperatures |
US10501400B2 (en) | 2015-02-04 | 2019-12-10 | Sirrus, Inc. | Heterogeneous catalytic transesterification of ester compounds with groups reactive under transesterification conditions |
US9334430B1 (en) | 2015-05-29 | 2016-05-10 | Sirrus, Inc. | Encapsulated polymerization initiators, polymerization systems and methods using the same |
US9217098B1 (en) | 2015-06-01 | 2015-12-22 | Sirrus, Inc. | Electroinitiated polymerization of compositions having a 1,1-disubstituted alkene compound |
US20170327454A1 (en) * | 2016-05-13 | 2017-11-16 | Sirrus, Inc. | High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation |
US9518001B1 (en) | 2016-05-13 | 2016-12-13 | Sirrus, Inc. | High purity 1,1-dicarbonyl substituted-1-alkenes and methods for their preparation |
US10428177B2 (en) | 2016-06-03 | 2019-10-01 | Sirrus, Inc. | Water absorbing or water soluble polymers, intermediate compounds, and methods thereof |
US9567475B1 (en) | 2016-06-03 | 2017-02-14 | Sirrus, Inc. | Coatings containing polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes |
US10196481B2 (en) | 2016-06-03 | 2019-02-05 | Sirrus, Inc. | Polymer and other compounds functionalized with terminal 1,1-disubstituted alkene monomer(s) and methods thereof |
US9617377B1 (en) | 2016-06-03 | 2017-04-11 | Sirrus, Inc. | Polyester macromers containing 1,1-dicarbonyl-substituted 1 alkenes |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3903105A1 (de) * | 1989-02-02 | 1990-08-09 | Huels Chemische Werke Ag | Fluessige enthalogenierungsmittel |
DE4134771A1 (de) * | 1991-10-22 | 1993-04-29 | Basf Ag | Verfahren zur herstellung von 2,2-bis-hydroxymethyl-butandiol-(1,4) |
-
1997
- 1997-03-21 DE DE19711762A patent/DE19711762A1/de not_active Withdrawn
-
1998
- 1998-02-07 EP EP98102135A patent/EP0866047B1/de not_active Expired - Lifetime
- 1998-02-07 DE DE59801235T patent/DE59801235D1/de not_active Expired - Fee Related
- 1998-03-20 HU HU9800615A patent/HUP9800615A3/hu unknown
- 1998-03-20 JP JP10072190A patent/JPH10279506A/ja not_active Ceased
- 1998-03-20 US US09/044,994 patent/US5902896A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
HU9800615D0 (en) | 1998-05-28 |
JPH10279506A (ja) | 1998-10-20 |
US5902896A (en) | 1999-05-11 |
HUP9800615A3 (en) | 2000-04-28 |
DE19711762A1 (de) | 1998-09-24 |
EP0866047B1 (de) | 2001-08-22 |
EP0866047A1 (de) | 1998-09-23 |
DE59801235D1 (de) | 2001-09-27 |
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