HUE051426T2 - Eljárás és rendszer aromás vegyületek adiabatikus nitrálására - Google Patents

Eljárás és rendszer aromás vegyületek adiabatikus nitrálására

Info

Publication number
HUE051426T2
HUE051426T2 HUE17828680A HUE17828680A HUE051426T2 HU E051426 T2 HUE051426 T2 HU E051426T2 HU E17828680 A HUE17828680 A HU E17828680A HU E17828680 A HUE17828680 A HU E17828680A HU E051426 T2 HUE051426 T2 HU E051426T2
Authority
HU
Hungary
Prior art keywords
aromates
adiabatic nitration
nitration
adiabatic
Prior art date
Application number
HUE17828680A
Other languages
English (en)
Hungarian (hu)
Inventor
Juergen Poehlmann
Dr Heinrich Hermann
Mirko Händel
Sophie Wernitz
Stefan Fankel
Original Assignee
Meissner Gmbh & Co Kg Josef
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=62910224&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=HUE051426(T2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Meissner Gmbh & Co Kg Josef filed Critical Meissner Gmbh & Co Kg Josef
Publication of HUE051426T2 publication Critical patent/HUE051426T2/hu

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B43/00—Formation or introduction of functional groups containing nitrogen
    • C07B43/02—Formation or introduction of functional groups containing nitrogen of nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00477—Controlling the temperature by thermal insulation means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/0015—Controlling the temperature by thermal insulation means
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00479—Means for mixing reactants or products in the reaction vessels
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
HUE17828680A 2017-02-03 2017-12-14 Eljárás és rendszer aromás vegyületek adiabatikus nitrálására HUE051426T2 (hu)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102017000973 2017-02-03
DE102017106881 2017-03-30
DE102017110084.9A DE102017110084B4 (de) 2017-02-03 2017-05-10 Verfahren und Anlage zur adiabatischen Nitrierung von Aromaten

Publications (1)

Publication Number Publication Date
HUE051426T2 true HUE051426T2 (hu) 2021-03-01

Family

ID=62910224

Family Applications (1)

Application Number Title Priority Date Filing Date
HUE17828680A HUE051426T2 (hu) 2017-02-03 2017-12-14 Eljárás és rendszer aromás vegyületek adiabatikus nitrálására

Country Status (12)

Country Link
US (1) US10941087B2 (pl)
EP (1) EP3555039B1 (pl)
JP (1) JP2020506188A (pl)
KR (1) KR102214750B1 (pl)
CN (1) CN110546130B (pl)
CA (1) CA3052335C (pl)
DE (1) DE102017110084B4 (pl)
EA (1) EA201991832A1 (pl)
HU (1) HUE051426T2 (pl)
PL (1) PL3555039T3 (pl)
PT (1) PT3555039T (pl)
WO (1) WO2018141451A1 (pl)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN112707822B (zh) * 2020-12-30 2022-02-08 东营安诺其纺织材料有限公司 一种氯苯一步绝热连续硝化制备2,4-二硝基氯苯的方法
WO2024003050A1 (en) 2022-06-28 2024-01-04 Basf Se Process for producing nitrobenzene
CN115466182B (zh) * 2022-09-05 2023-08-29 清华大学 一种高选择性合成间二硝基苯的方法

Family Cites Families (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2256999A (en) 1939-03-08 1941-09-23 Du Pont Nitration of organic compounds
NL127396C (pl) 1962-04-30
US4091042A (en) 1977-08-19 1978-05-23 American Cyanamid Company Continuous adiabatic process for the mononitration of benzene
DE2818680A1 (de) 1978-04-27 1979-10-31 Bayer Ag Verfahren zur aufarbeitung von nitro-hydroxy-aromaten enthaltenden abwaessern
US4241229A (en) 1979-08-08 1980-12-23 American Cyanamid Company Recovery of nitrated aromatic compounds from nitration wash liquors
JPS5759837A (en) 1980-09-24 1982-04-10 American Cyanamid Co Recovery of nitrated aromatic compounds from nitration rinsing water
US4482769A (en) 1983-09-16 1984-11-13 Air Products And Chemicals, Inc. Reducing 2,4-dinitroortho-cresol in effluent stream from dinitrotoluene process
DE3409717C2 (de) 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
US4597875A (en) 1985-05-07 1986-07-01 Air Products And Chemicals, Inc. Precipitative removal of nitrocresols from dinitrotoluene waste streams
US4994242A (en) 1988-08-15 1991-02-19 Noram Engineering And Constructors Ltd. Jet impingement reactor
US4973770A (en) 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds
US5313009A (en) 1990-01-04 1994-05-17 Nrm International Technologies C.V. Nitration process
DE69026590T2 (de) 1990-01-04 1996-10-31 Nrm Int Tech Nitrierungsverfahren
TW236610B (en) 1992-11-13 1994-12-21 Bayer Ag Preparation of dinitrotoluene
DE4437047A1 (de) 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
DE19539205A1 (de) 1995-10-22 1997-04-24 Meissner Gmbh & Co Kg Josef Verfahren zur Aromatennitrierung
US5763687A (en) 1995-12-15 1998-06-09 Mitsui Chemicals, Inc. Preparation process for aromatic mononitro compounds
JP3244636B2 (ja) 1995-12-15 2002-01-07 三井化学株式会社 芳香族モノニトロ化合物の製造方法
DE19745119A1 (de) * 1997-10-13 1999-04-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol in adiabatischer Fahrweise
HUP0100200A3 (en) * 1997-11-03 2002-03-28 Bayer Ag Method for producing aromatic nitro compounds
DE19815844A1 (de) 1998-04-08 1999-10-14 Basf Ag Verfahren zum Abbau von aromatischen Nitroverbindungen in Abwässern
US5963878A (en) 1998-07-30 1999-10-05 Noram Engineering & Constructors Ltd. Nitration process
US6288289B1 (en) 2000-01-27 2001-09-11 Noram Engineering And Constructors Ltd. Integrated effluent treatment process for nitroaromatic manufacture
PT1272268E (pt) 2000-03-02 2012-07-24 Dow Global Technologies Llc Reator tubular, processo de realização de reações multifásicas líquido/ líquido num reator tubular, e um processo de nitração cíclica de compostos aromáticos num reator tubular
FR2806325B1 (fr) 2000-03-17 2002-10-18 Air Liquide Module de garnissage, son procede de fabrication, et appareil de traitement de fluide(s) comportant un garnissage correspondant
EP1291078A3 (de) 2001-09-10 2004-01-28 Bayer Ag Rohrreaktor zur adiabatischen Nitrierung
DE102006004943A1 (de) 2006-02-03 2007-08-09 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol
DE102008048713A1 (de) 2008-09-24 2010-03-25 Bayer Materialscience Ag Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
HUE035115T2 (hu) 2008-11-10 2018-05-02 Noram International Ltd Adiabatikus eljárás mononitrobenzol elõállítására
BR112012004604A2 (pt) 2009-08-31 2016-04-05 Basf Se processo para preparar de maneira contínua aromáticos nitrados
DE102010006984A1 (de) 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
WO2012110839A1 (en) 2011-02-17 2012-08-23 Noram International Limited Removal of non-aromatic impurities from a nitration process
CA2835121C (en) * 2011-05-19 2015-12-29 Josef Meissner Gmbh & Co. Kg Method and apparatus for purifying nitration products
CN104487413B (zh) * 2012-07-27 2017-03-29 科思创德国股份有限公司 通过绝热硝化制备硝基苯的方法
EP2877442B1 (de) 2012-07-27 2016-11-16 Covestro Deutschland AG Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
KR102066764B1 (ko) * 2012-07-27 2020-01-15 코베스트로 도이칠란드 아게 단열 니트로화에 의한 니트로벤젠의 제조방법
US9227909B2 (en) 2012-10-10 2016-01-05 Covestro Deutschland Ag Method for the continuous production of nitrobenzene

Also Published As

Publication number Publication date
DE102017110084A1 (de) 2018-08-09
EP3555039B1 (de) 2020-08-05
WO2018141451A1 (de) 2018-08-09
US20200017421A1 (en) 2020-01-16
DE102017110084B4 (de) 2019-07-04
JP2020506188A (ja) 2020-02-27
EP3555039A1 (de) 2019-10-23
PL3555039T3 (pl) 2021-02-08
KR102214750B1 (ko) 2021-02-10
CA3052335A1 (en) 2018-08-09
CN110546130A (zh) 2019-12-06
CN110546130B (zh) 2022-07-15
PT3555039T (pt) 2020-10-01
EA201991832A1 (ru) 2020-01-09
US10941087B2 (en) 2021-03-09
CA3052335C (en) 2022-06-21
KR20190115007A (ko) 2019-10-10

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