HU207672B - Method for producing catalyzer and producing acid amides by applying the same - Google Patents

Method for producing catalyzer and producing acid amides by applying the same Download PDF

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Publication number
HU207672B
HU207672B HU894854A HU485489A HU207672B HU 207672 B HU207672 B HU 207672B HU 894854 A HU894854 A HU 894854A HU 485489 A HU485489 A HU 485489A HU 207672 B HU207672 B HU 207672B
Authority
HU
Hungary
Prior art keywords
catalyst
copper
weight
alkali metal
acid amides
Prior art date
Application number
HU894854A
Other languages
English (en)
Other versions
HUT54924A (en
Inventor
Dr Lukacs Julia Paalne
Galina Putirszkaja
Laszlo Botar
Agnes Keszler
Istvan Nemes
Tamas Vidoczy
Dezsoe Gal
Gabor Vasvari
Rezsoene Metzger
Janosne Horvath
Jozsefne Soenfeld
Barlai Agnes Bandine
Jozsef Fodor
Kalman Rajnai
Original Assignee
Mta Koezponti Kemiai Kutato In
Nitrokemia Ipartelepek
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mta Koezponti Kemiai Kutato In, Nitrokemia Ipartelepek filed Critical Mta Koezponti Kemiai Kutato In
Priority to HU894854A priority Critical patent/HU207672B/hu
Priority to EP19900117034 priority patent/EP0418646A3/en
Priority to KR1019900014706A priority patent/KR910006215A/ko
Priority to JP2248580A priority patent/JPH03218339A/ja
Priority to FI904585A priority patent/FI904585A0/fi
Publication of HUT54924A publication Critical patent/HUT54924A/hu
Publication of HU207672B publication Critical patent/HU207672B/hu

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/847Vanadium, niobium or tantalum or polonium
    • B01J23/8472Vanadium
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00Carboxylic acid amides
    • C07C233/01Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/09Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/06Preparation of carboxylic acid amides from nitriles by transformation of cyano groups into carboxamide groups
    • C07C231/065By hydration using metals or metallic ions as catalyst

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Claims (2)

1. Eljárás savamidok, nitrilek, vanádium(V)- és réz(II)-ionokat és fémrezet tartalmazó katalizátor jelenlétében végzett hidratálásával történő előállítására alkalmazható katalizátor előállítására, azzal jellemezve, hogy alkálifém-vanadátot és alkálifém-szilikátot 1: (22,5) tömegarányban tartalmazó vizes oldathoz 1 mól alkálifém-szilikátra vonatkoztatva 0,1-0,3 mól vízben oldódó magnézium- vagy kalciumsót és annyi vízben oldódó réz(II)-sóf adunk, hogy a fémionban kifejezett vanádium(V): réz(II) tömegarány 1 : (1-2) legyen, a ki4
HU 207 672 Β vált csapadékot elkülönítjük, a nedves csapadékhoz
1 tömegrész jelen lévő réz(II)-ionra vonatkoztatva 12 tömegrész fémrezet keverünk, és a kapott keveréket 150-200 °C-on szárítjuk.
2. Eljárás savamidok előállítására nitrilek katalizá- 5 tor jelenlétében végzett hidratálásával, azzal jellemez ve, hogy katalizátorként az 1. igénypont szerinti eljá rással előállított katalizátort alkalmazzunk, adott eset ben emulgeálószer jelenlétében.
HU894854A 1989-09-18 1989-09-18 Method for producing catalyzer and producing acid amides by applying the same HU207672B (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
HU894854A HU207672B (en) 1989-09-18 1989-09-18 Method for producing catalyzer and producing acid amides by applying the same
EP19900117034 EP0418646A3 (en) 1989-09-18 1990-09-05 Process for the preparation of acyl amides by subjecting nitriles to catalytic hydration
KR1019900014706A KR910006215A (ko) 1989-09-18 1990-09-18 니트릴의 촉매수화반응에 의한 아실 아미드의 제조방법
JP2248580A JPH03218339A (ja) 1989-09-18 1990-09-18 ニトリルの接触水和によるアシルアミドの製造方法及びその実施に使用する触媒とその製造方法
FI904585A FI904585A0 (fi) 1989-09-18 1990-09-18 Foerfarande foer framstaellning av acylamider genom katalytisk hydration av nitriler.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
HU894854A HU207672B (en) 1989-09-18 1989-09-18 Method for producing catalyzer and producing acid amides by applying the same

Publications (2)

Publication Number Publication Date
HUT54924A HUT54924A (en) 1991-04-29
HU207672B true HU207672B (en) 1993-05-28

Family

ID=10969027

Family Applications (1)

Application Number Title Priority Date Filing Date
HU894854A HU207672B (en) 1989-09-18 1989-09-18 Method for producing catalyzer and producing acid amides by applying the same

Country Status (5)

Country Link
EP (1) EP0418646A3 (hu)
JP (1) JPH03218339A (hu)
KR (1) KR910006215A (hu)
FI (1) FI904585A0 (hu)
HU (1) HU207672B (hu)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102636998B1 (ko) * 2023-04-28 2024-02-14 이을용 과수봉지 바인더 제조장치 및 이에 의해 제조된 과수봉지 바인더

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2320060C2 (de) * 1973-04-19 1982-10-14 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Carbonsäureamiden
ZA761185B (en) * 1975-03-17 1977-02-23 American Cyanamid Co Catalyst for hydration of nitriles
US4096184A (en) * 1976-01-19 1978-06-20 Sumitomo Chemical Company, Limited Process for preparing acid amides
BR8306403A (pt) * 1983-11-17 1985-06-25 Rhodia Processo tipo batelada para a obtencao de solucoes aquosas de monomero de acrilamida a 50% em peso,a partir de misturas acrilonitrila/agua
GB8727379D0 (en) * 1987-11-23 1987-12-23 Allied Colloids Ltd Catalysts

Also Published As

Publication number Publication date
EP0418646A3 (en) 1991-09-25
EP0418646A2 (en) 1991-03-27
FI904585A0 (fi) 1990-09-18
HUT54924A (en) 1991-04-29
KR910006215A (ko) 1991-04-27
JPH03218339A (ja) 1991-09-25

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Legal Events

Date Code Title Description
HMM4 Cancellation of final prot. due to non-payment of fee