HU185787B - Process for preparing benzoxazolone - Google Patents
Process for preparing benzoxazolone Download PDFInfo
- Publication number
- HU185787B HU185787B HU801119A HU111980A HU185787B HU 185787 B HU185787 B HU 185787B HU 801119 A HU801119 A HU 801119A HU 111980 A HU111980 A HU 111980A HU 185787 B HU185787 B HU 185787B
- Authority
- HU
- Hungary
- Prior art keywords
- chlorophenol
- benzoxazolone
- reaction
- ammonia
- pressure
- Prior art date
Links
- ASSKVPFEZFQQNQ-UHFFFAOYSA-N 2-benzoxazolinone Chemical compound C1=CC=C2OC(O)=NC2=C1 ASSKVPFEZFQQNQ-UHFFFAOYSA-N 0.000 title claims abstract description 39
- 238000004519 manufacturing process Methods 0.000 title 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 42
- ISPYQTSUDJAMAB-UHFFFAOYSA-N 2-chlorophenol Chemical compound OC1=CC=CC=C1Cl ISPYQTSUDJAMAB-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 20
- 238000006243 chemical reaction Methods 0.000 claims abstract description 18
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000004202 carbamide Substances 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims description 25
- 239000011541 reaction mixture Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 5
- 239000012429 reaction media Substances 0.000 claims description 5
- 229910021591 Copper(I) chloride Inorganic materials 0.000 claims description 4
- OXBLHERUFWYNTN-UHFFFAOYSA-M copper(I) chloride Chemical group [Cu]Cl OXBLHERUFWYNTN-UHFFFAOYSA-M 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- VMQMZMRVKUZKQL-UHFFFAOYSA-N Cu+ Chemical class [Cu+] VMQMZMRVKUZKQL-UHFFFAOYSA-N 0.000 claims description 2
- BERDEBHAJNAUOM-UHFFFAOYSA-N copper(i) oxide Chemical compound [Cu]O[Cu] BERDEBHAJNAUOM-UHFFFAOYSA-N 0.000 description 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 229910052727 yttrium Inorganic materials 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N hydrochloric acid Substances Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical compound NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 1
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-N Propionic acid Chemical class CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 125000005595 acetylacetonate group Chemical group 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 150000004820 halides Chemical class 0.000 description 1
- 239000003049 inorganic solvent Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D263/00—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings
- C07D263/52—Heterocyclic compounds containing 1,3-oxazole or hydrogenated 1,3-oxazole rings condensed with carbocyclic rings or ring systems
- C07D263/54—Benzoxazoles; Hydrogenated benzoxazoles
- C07D263/58—Benzoxazoles; Hydrogenated benzoxazoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached in position 2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7912140A FR2456095A2 (fr) | 1979-05-08 | 1979-05-08 | Preparation de benzoxazolone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HU185787B true HU185787B (en) | 1985-03-28 |
Family
ID=9225404
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HU801119A HU185787B (en) | 1979-05-08 | 1980-05-07 | Process for preparing benzoxazolone |
Country Status (16)
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2456094A1 (fr) * | 1979-05-08 | 1980-12-05 | Rhone Poulenc Agrochimie | Preparation de benzoxazolone |
| FR2456095A2 (fr) * | 1979-05-08 | 1980-12-05 | Rhone Poulenc Agrochimie | Preparation de benzoxazolone |
| JPS5982511U (ja) * | 1982-11-22 | 1984-06-04 | 石垣機工株式会社 | フイルタプレスにおける濾布の洗浄装置 |
| JPS5982510U (ja) * | 1982-11-22 | 1984-06-04 | 石垣機工株式会社 | フイルタプレスにおける濾布の洗浄装置 |
| JPS5993609U (ja) * | 1982-12-10 | 1984-06-25 | 石垣機工株式会社 | フイルタプレスにおける濾布の洗浄装置 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1269067A (fr) * | 1959-04-16 | 1961-08-11 | Profatec Soc | Procédé de préparation de la benzoxazolone |
| BR7204020D0 (pt) * | 1971-06-24 | 1973-11-01 | Hoechst Ag | Processo para a obtencao de benzoxazolonas-(2) e benzotiazolonas-(2) |
| FR2456095A2 (fr) * | 1979-05-08 | 1980-12-05 | Rhone Poulenc Agrochimie | Preparation de benzoxazolone |
-
1979
- 1979-05-08 FR FR7912140A patent/FR2456095A2/fr active Granted
-
1980
- 1980-03-13 IL IL59610A patent/IL59610A/xx unknown
- 1980-04-25 US US06/143,859 patent/US4309550A/en not_active Expired - Lifetime
- 1980-05-01 GB GB8014438A patent/GB2048270B/en not_active Expired
- 1980-05-06 JP JP6045880A patent/JPS5625173A/ja active Granted
- 1980-05-06 PT PT71192A patent/PT71192B/pt unknown
- 1980-05-06 CA CA000351331A patent/CA1150274A/en not_active Expired
- 1980-05-06 ZA ZA00802716A patent/ZA802716B/xx unknown
- 1980-05-06 DK DK197680A patent/DK151334C/da not_active IP Right Cessation
- 1980-05-06 BR BR8002788A patent/BR8002788A/pt unknown
- 1980-05-06 IE IE923/80A patent/IE49475B1/en unknown
- 1980-05-07 EP EP80420053A patent/EP0020281B1/fr not_active Expired
- 1980-05-07 DE DE8080420053T patent/DE3072019D1/de not_active Expired
- 1980-05-07 ES ES491241A patent/ES8106896A1/es not_active Expired
- 1980-05-07 AT AT80420053T patent/ATE26269T1/de not_active IP Right Cessation
- 1980-05-07 HU HU801119A patent/HU185787B/hu unknown
Also Published As
| Publication number | Publication date |
|---|---|
| GB2048270A (en) | 1980-12-10 |
| PT71192B (fr) | 1981-09-17 |
| BR8002788A (pt) | 1980-12-16 |
| GB2048270B (en) | 1983-05-25 |
| IE800923L (en) | 1980-11-08 |
| JPS5625173A (en) | 1981-03-10 |
| EP0020281B1 (fr) | 1987-04-01 |
| JPH0128025B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1989-05-31 |
| ZA802716B (en) | 1981-05-27 |
| IE49475B1 (en) | 1985-10-16 |
| IL59610A (en) | 1983-07-31 |
| ATE26269T1 (de) | 1987-04-15 |
| ES491241A0 (es) | 1981-04-01 |
| DK151334B (da) | 1987-11-23 |
| FR2456095A2 (fr) | 1980-12-05 |
| IL59610A0 (en) | 1980-06-30 |
| PT71192A (fr) | 1980-06-01 |
| CA1150274A (en) | 1983-07-19 |
| US4309550A (en) | 1982-01-05 |
| EP0020281A1 (fr) | 1980-12-10 |
| DK197680A (da) | 1980-11-09 |
| DE3072019D1 (en) | 1987-10-01 |
| DK151334C (da) | 1988-07-18 |
| FR2456095B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1983-06-24 |
| ES8106896A1 (es) | 1981-04-01 |
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