HRP20200536T1 - Katalitička obrada pirolitičkih para - Google Patents

Katalitička obrada pirolitičkih para Download PDF

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Publication number
HRP20200536T1
HRP20200536T1 HRP20200536TT HRP20200536T HRP20200536T1 HR P20200536 T1 HRP20200536 T1 HR P20200536T1 HR P20200536T T HRP20200536T T HR P20200536TT HR P20200536 T HRP20200536 T HR P20200536T HR P20200536 T1 HRP20200536 T1 HR P20200536T1
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Croatia
Prior art keywords
heat
heated
catalyst layer
pyrolyzing
pyrolytic
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HRP20200536TT
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English (en)
Inventor
Jukka Heiskanen
Sara Kärki
Erkki VÄLIMÄKI
Reyhaneh SHENASSA
Jussi Mäntyniemi
Pekka Jokela
Andrea Gutierrez
Joakim Autio
Janne Asikkala
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Valmet Technologies Oy
Fortum Oyj
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Application filed by Valmet Technologies Oy, Fortum Oyj filed Critical Valmet Technologies Oy
Publication of HRP20200536T1 publication Critical patent/HRP20200536T1/hr

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K3/00—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide
    • C10K3/02—Modifying the chemical composition of combustible gases containing carbon monoxide to produce an improved fuel, e.g. one of different calorific value, which may be free from carbon monoxide by catalytic treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B49/00—Destructive distillation of solid carbonaceous materials by direct heating with heat-carrying agents including the partial combustion of the solid material to be treated
    • C10B49/16—Destructive distillation of solid carbonaceous materials by direct heating with heat-carrying agents including the partial combustion of the solid material to be treated with moving solid heat-carriers in divided form
    • C10B49/20—Destructive distillation of solid carbonaceous materials by direct heating with heat-carrying agents including the partial combustion of the solid material to be treated with moving solid heat-carriers in divided form in dispersed form
    • C10B49/22—Destructive distillation of solid carbonaceous materials by direct heating with heat-carrying agents including the partial combustion of the solid material to be treated with moving solid heat-carriers in divided form in dispersed form according to the "fluidised bed" technique
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00—Treatment of sludge; Devices therefor
    • C02F11/10—Treatment of sludge; Devices therefor by pyrolysis
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/04—Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition
    • C10B57/06—Other carbonising or coking processes; Features of destructive distillation processes in general using charges of special composition containing additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B57/00—Other carbonising or coking processes; Features of destructive distillation processes in general
    • C10B57/18—Modifying the properties of the distillation gases in the oven
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/42—Catalytic treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G3/00—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids
    • C10G3/50—Production of liquid hydrocarbon mixtures from oxygen-containing organic materials, e.g. fatty oils, fatty acids in the presence of hydrogen, hydrogen donors or hydrogen generating compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/28—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid material
    • C10G9/32—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid material according to the "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/02—Dust removal
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23C—METHODS OR APPARATUS FOR COMBUSTION USING FLUID FUEL OR SOLID FUEL SUSPENDED IN  A CARRIER GAS OR AIR 
    • F23C10/00—Fluidised bed combustion apparatus
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1003—Waste materials
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1011—Biomass
    • C10G2300/1014—Biomass of vegetal origin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00—Technologies relating to oil refining and petrochemical industry
    • Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock

Claims (11)

1. Postupak za proizvodnju sirovih kondenzata iz pirolizirajućeg materijala, naznačen time da se sastoji od - izgaranja goriva u kotlu s fluidnim slojem (100), pritom stvarajući dimni plin i toplinu, - zagrijavanja nekih prvih toplinski otpornih čestica materijala sadržanih u fluidnom sloju (110) u kotlu s fluidnim slojem s navedenom toplinom, - povrat topline iz dimnog plina u medij za prijenos topline uporabom izmjenjivača topline (700) smještenog u kotlu s fluidnim slojem (100), - opcionalno, zagrijavanja nekih drugih toplinski otpornih čestica pomoću zagrijanog prvog materijala koji je otporan na toplinu, - prijenosom barem nekih od zagrijanih prvih toplinski otpornih čestica materijala ili zagrijanih drugih toplinski otpornih čestica materijala u reaktor za pirolizu (200), - prenošenje nešto pirolizirajućeg materijala u reaktor za pirolizu (200), - piroliziranja pirolizirajućeg materijala u reaktoru za pirolizu dovođenjem u doticaj pirolizirajućeg materijala sa zagrijanim prvim materijalom na toplinu otpornih čestica ili zagrijanim drugim na toplinu otpornih čestica materijala, stvarajući pritom barem sirovu pirolitičku paru i ugljen, - čišćenja barem jednog dijela sirovih pirolitičkih para stvarajući pritom čiste paralitičke pare, - dovođenja barem dijela čistih pirolitičkih para kroz sloj katalizatora (410) koji sadrži katalizatorski materijal konfiguriran za deoksigenat oksigeniranog ugljikovodika, pri čemu je parcijalni tlak vodika u parama u sloju katalizatora manji od 0.5 bara, na taj način katalitički obrađuje barem dio sirovih pirolitičkih para, gdje se nikakav vanjski vodik (H2) ne dovodi u proces između pirolitičkog reaktora i sloja katalizatora ili unutar samog sloja katalizatora; - prijenosa dijela ugljena u kotao s fluidnim slojem ili u plamenik, izgarajući ugljen u kotlu s fluidnim slojem ili u plameniku da bi se proizvela toplina, i vraćanje topline proizvedene izgaranjem ugljena; postupak koji nadalje obuhvaća - kondenziranje barem dijela obrađenog pirolitički isparenog proizvoda u sirovi kondenzat, stvarajući pritom neki nekondenzacijski plin kao nusprodukt; - dovođenja barem dijela nekondenzirajućeg plina natrag u postupak, iznad spomenutog kondenziranja; - obnavljanja barem nekog materijala katalizatora katalizatorskog sloja (410), proizvodeći pritom neki drugi dimni plin, i - dovođenja najmanje nekog drugog dimnog plina nazad u postupak, u katalitički reaktor (400) ili iznad, ili u sam reaktor za pirolizu (200).
2. Postupak temeljem zahtjeva 1 , naznačen time da - se barem neki nekondenzirajući plin dovodi u katalitički reaktor (400) koji sadrži sloj katalizatora (410).
3. Postupak temeljem zahtjeva 1 ili 2, naznačen time da - koristi toplina iz kondenzatora (810) konfiguriranog za kondenziranje tretiranih pirolitičkih para.
4. Postupak temeljem bilo kojeg zahtjeva 1 do 3, naznačen time da se sastoji od - proizvodnje struje upotrebom te topline prikupljene iz dimnih plinova u mediju za prikupljanje topline.
5. Postupak temeljem bilo kojeg zahtjeva 1 do 4, naznačen time da je - katalitički materijal u sloju katalizatora (410) odabran iz grupe katalizatora koji ima funkciju kondenzacije, dekarbonizacije i dekarboksilacije.
6. Postupak temeljem bilo kojeg zahtjeva 1 do 5, naznačen time da je - tlak u reaktoru za pirolizu (210) veći ili jednak tlaku u sloju katalizatora (410); poželjno i - tlak u kotlu s fluidiziranim slojem (100) je veći ili jednak tlaku u reaktoru za pirolizu (200).
7. Postupak temeljem bilo kojeg zahtjeva 1 do 6, naznačen time da je - tlak para u sloju katalizatora (410) manji od 2 bara.
8. Postupak temeljem bilo kojeg zahtjeva 1 do 7, naznačen time da se - odvaja voda iz sirovog kondenzata i pritom proizvodi biogorivo.
9. Postupak temeljem bilo kojeg zahtjeva 1 do 8, naznačen time da obuhvaća - piroliziranje pirolizirajućeg materijala tako da sirova pirolitička para prije katalitičke obrade ima prvi sadržaj atoma kisika vezan na kondenzirajuće spojeve koji sadrže i vodik i ugljik i - katalitičku obradu pirolitičke pare u sloju katalizatora (410) tako da tretirani pirolitički proizvod para ima drugi sadržaj atoma kisika vezan na kondenzacijsku spoj (i) koja također uključuju vodik i ugljik, pri čemu - je drugi udio kisika manji od prvog sadržaja kisika i - vrelište svakog kondenzacijskog spoja je najmanje 25 ° C pod tlakom od 1 atm; - pri čemu se prvi sadržaj kisika odnosi na prvi sadržaj atoma kisika, a drugi sadržaj kisika odnosi se na drugi sadržaj atoma kisika.
10. Postupak temeljem bilo kojeg zahtjeva 1 do 9, naznačen time da se sastoji od - prijenosa barem dijela zagrijanih prvih toplinski otpornih čestica materijala iz kotla s fluidnim slojem (100), izravno ili neizravno, u reaktor za pirolizu (200), - piroliziranja materijala koji se pirolizira u reaktoru za pirolizu (200) dovođenjem u doticaj piroliznog materijala sa zagrijanim prvim toplinski otpornih čestica materijala, - prijenosa dijela ugljena iz reaktora za pirolizu (200), izravno ili neizravno, u kotao s fluidnim slojem (100) da tamo izgori, i - izgaranja dijela ugljena u kotlu s fluidnim slojem (100).
11. Postupak temeljem bilo kojeg zahtjeva 1 do 9, naznačen time da se sastoji od - zagrijavanja drugog toplinski otpornih čestica materijala upotrebom zagrijanih prvih toplinski otpornih čestica materijala, - prijenosa barem dijela zagrijanog drugog toplinski otpornih čestica materijala u reaktor za pirolizu (200), i - piroliziranje materijala koji se pirolizira u reaktoru za pirolizu (200) dovođenjem u doticaj piroliznog materijala sa zagrijanim drugim toplinski otpornim česticama materijala.
HRP20200536TT 2015-04-17 2020-03-31 Katalitička obrada pirolitičkih para HRP20200536T1 (hr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20155290A FI127201B (en) 2015-04-17 2015-04-17 Catalytic refining of pyrolysis vapors
EP16722260.3A EP3283603B1 (en) 2015-04-17 2016-04-13 Catalytic upgrading of pyrolytic vapors
PCT/FI2016/050238 WO2016166413A1 (en) 2015-04-17 2016-04-13 Catalytic upgrading of pyrolytic vapors

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HRP20200536T1 true HRP20200536T1 (hr) 2020-06-26

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US (1) US10711198B2 (hr)
EP (1) EP3283603B1 (hr)
BR (1) BR112017022225B8 (hr)
CA (1) CA2983169C (hr)
DK (1) DK3283603T3 (hr)
ES (1) ES2775176T3 (hr)
FI (2) FI127201B (hr)
HR (1) HRP20200536T1 (hr)
HU (1) HUE048684T2 (hr)
LT (1) LT3283603T (hr)
PL (1) PL3283603T3 (hr)
PT (1) PT3283603T (hr)
RU (1) RU2710020C2 (hr)
SI (1) SI3283603T1 (hr)
WO (1) WO2016166413A1 (hr)

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