GEAP202516547A - Method for monitoring a control parameter on a substantially plastic material, relating to apparatus and pyrolysis process which uses this method - Google Patents

Method for monitoring a control parameter on a substantially plastic material, relating to apparatus and pyrolysis process which uses this method

Info

Publication number
GEAP202516547A
GEAP202516547A GEAP202516547A GEAP2025016547A GEAP202516547A GE AP202516547 A GEAP202516547 A GE AP202516547A GE AP202516547 A GEAP202516547 A GE AP202516547A GE AP2025016547 A GEAP2025016547 A GE AP2025016547A GE AP202516547 A GEAP202516547 A GE AP202516547A
Authority
GE
Georgia
Prior art keywords
plastic material
essentially plastic
essentially
molten form
analytical measurement
Prior art date
Application number
GEAP202516547A
Other languages
English (en)
Georgian (ka)
Inventor
Antonio Ponticiello
Francesco Bonacini
Mirco Nodari
Armando Galeotti
Riccardo Felisari
Original Assignee
Versalis Spa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Versalis Spa filed Critical Versalis Spa
Publication of GEAP202516547A publication Critical patent/GEAP202516547A/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3577Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing liquids, e.g. polluted water
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/10Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00Heat treatments such as Calcining; Fusing ; Pyrolysis
    • B01J6/008Pyrolysis reactions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/008Controlling or regulating of liquefaction processes
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K1/00Details of thermometers not specially adapted for particular types of thermometer
    • G01K1/02Means for indicating or recording specially adapted for thermometers
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44Resins; Plastics; Rubber; Leather
    • G01N33/442Resins; Plastics
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05BCONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
    • G05B23/00Testing or monitoring of control systems or parts thereof
    • G05B23/02Electric testing or monitoring
    • G05B23/0205Electric testing or monitoring by means of a monitoring system capable of detecting and responding to faults
    • G05B23/0218Electric testing or monitoring by means of a monitoring system capable of detecting and responding to faults characterised by the fault detection method dealing with either existing or incipient faults
    • G05B23/0221Preprocessing measurements, e.g. data collection rate adjustment; Standardization of measurements; Time series or signal analysis, e.g. frequency analysis or wavelets; Trustworthiness of measurements; Indexes therefor; Measurements using easily measured parameters to estimate parameters difficult to measure; Virtual sensor creation; De-noising; Sensor fusion; Unconventional preprocessing inherently present in specific fault detection methods like PCA-based methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00171Controlling or regulating processes controlling the density
    • B01J2219/00175Optical density
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00193Sensing a parameter
    • B01J2219/00195Sensing a parameter of the reaction system
    • B01J2219/002Sensing a parameter of the reaction system inside the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00209Control algorithm transforming a sensed parameter
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00191Control algorithm
    • B01J2219/00211Control algorithm comparing a sensed parameter with a pre-set value
    • B01J2219/00218Dynamically variable (in-line) parameter values
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10Feedstock materials
    • C10G2300/1003Waste materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/141Feedstock
    • Y02P20/143Feedstock the feedstock being recycled material, e.g. plastics

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Physics & Mathematics (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • General Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • Biochemistry (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Automation & Control Theory (AREA)
  • Thermal Sciences (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
GEAP202516547A 2021-12-30 2022-12-27 Method for monitoring a control parameter on a substantially plastic material, relating to apparatus and pyrolysis process which uses this method GEAP202516547A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
IT102021000033059A IT202100033059A1 (it) 2021-12-30 2021-12-30 Metodo per monitorare un parametro di controllo su un materiale sostanzialmente plastico, relativo apparato e processo di pirolisi che impiega detto metodo

Publications (1)

Publication Number Publication Date
GEAP202516547A true GEAP202516547A (en) 2025-08-11

Family

ID=80685045

Family Applications (1)

Application Number Title Priority Date Filing Date
GEAP202516547A GEAP202516547A (en) 2021-12-30 2022-12-27 Method for monitoring a control parameter on a substantially plastic material, relating to apparatus and pyrolysis process which uses this method

Country Status (12)

Country Link
US (1) US20250085220A1 (https=)
EP (1) EP4457301A1 (https=)
JP (1) JP2025504774A (https=)
KR (1) KR20240131362A (https=)
CN (1) CN118591609A (https=)
CA (1) CA3240732A1 (https=)
GE (1) GEAP202516547A (https=)
IT (1) IT202100033059A1 (https=)
MX (1) MX2024008208A (https=)
TW (1) TW202339850A (https=)
WO (1) WO2023126826A1 (https=)
ZA (1) ZA202405011B (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20240164043A (ko) * 2023-05-11 2024-11-19 주식회사 엘지화학 폐플라스틱의 열분해유 제조 방법
US12468268B1 (en) * 2025-01-17 2025-11-11 Ryan Carter Machine-learning based monitoring of plastic recycling

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5532487A (en) * 1994-11-23 1996-07-02 E. I. Du Pont De Nemours And Company Near-infrared measurement and control of polyamide processes
WO2002031082A1 (en) 2000-10-10 2002-04-18 Rj Lee Group, Inc. Tandem batch feed and tandem batch collection apparatus for continuous pyrolysis of rubber and/or other hydrocarbon-based material
EP2184334A1 (de) 2008-10-31 2010-05-12 Peter Spörri Verfahren und Vorrichtung zum Recycling von kohlenwasserstoff-haltigen Materialien
PT2348254T (pt) 2010-01-22 2018-02-26 Rv Lizenz Ag Sistema de abastecimento de combustível para uma máquina móvel
ES2389799B2 (es) 2011-02-10 2013-06-04 Urbaser, S.A. Procedimiento en dos etapas para la obtención de combustibles tipo gasóleo a partir de residuos plásticos.
EP2721098A4 (en) 2011-06-17 2015-04-01 Amit Tandon METHOD AND DEVICE FOR CONTINUOUS RECYCLING OF PLASTIC WASTE TO LIQUID FUELS
PL399500A1 (pl) 2012-06-12 2013-12-23 Dagas Spólka Z Ograniczona Odpowiedzialnoscia Sposób prowadzenia procesu pirolizy odpadowych tworzyw sztucznych i/lub odpadów gumowych i/lub odpadów organicznych oraz instalacja do realizacji tego sposobu
NL2016124B1 (en) 2016-01-20 2017-07-25 Black Bear Carbon B V A method for sorting tires
DK3408352T3 (da) * 2016-03-31 2025-08-18 H&R Int Beteiligung Gmbh Proces til fremstilling af en c20 til c60-voks ved selektiv termisk nedbrydning af polyolefin plastpolymer
CA2973210A1 (en) * 2017-07-13 2019-01-13 Louis Bertrand Process for producing liquid fuel from waste hydrocarbon and/or organic material, managing system thereof

Also Published As

Publication number Publication date
CN118591609A (zh) 2024-09-03
WO2023126826A1 (en) 2023-07-06
CA3240732A1 (en) 2023-07-06
JP2025504774A (ja) 2025-02-19
US20250085220A1 (en) 2025-03-13
MX2024008208A (es) 2024-07-10
EP4457301A1 (en) 2024-11-06
KR20240131362A (ko) 2024-08-30
IT202100033059A1 (it) 2023-06-30
TW202339850A (zh) 2023-10-16
ZA202405011B (en) 2025-01-29

Similar Documents

Publication Publication Date Title
GEAP202516547A (en) Method for monitoring a control parameter on a substantially plastic material, relating to apparatus and pyrolysis process which uses this method
van den Berg et al. Process analytical technology in the food industry
Webster et al. Development of generic raman models for a GS‐KOTM CHO platform process
US20220068440A1 (en) System and method for predicting quality of a chemical compound and/or of a formulation thereof as a product of a production process
JP2016507113A5 (ja) 製品またはプロセス流の特性を判定するためのシステムおよび方法
JP2016507113A (ja) 製品またはプロセス流の特性を判定するためのシステム、方法、および装置
Kozma et al. Comparison of multivariate data analysis techniques to improve glucose concentration prediction in mammalian cell cultivations by Raman spectroscopy
CN113165243A (zh) 用于改进物理生产过程的方法和系统
CN107015541A (zh) 基于互信息和最小二乘支持向量机相结合的软测量方法
Zhou et al. Influence of temperature and turbidity on water COD detection by UV absorption spectroscopy
US4227083A (en) Apparatus for infrared laser spectroscopy of room temperature vulcanizable silicone compositions
Huang et al. In‐line monitoring of component content of polypropylene/polystyrene blends during melt extrusion using Raman spectroscopy
Ullah et al. An explainable machine learning (XML) approach to determine strength of glass powder concrete
WO2019235542A1 (ja) 光学分析システム及び光学分析方法
US20200086546A1 (en) Method for controlling film production
Matoc et al. Machine learning-driven prediction and digital twins implementation for VOC emissions in VAT photopolymerization additive manufacturing
CN118280464A (zh) 一种用于润滑油添加剂定量分析的方法及系统
Kandelbauer Processing and process control
Ramini et al. Shear heating parameter of rubber compounds useful for process control in injection molding machine
CN118730949A (zh) 一种基于多源光谱数据融合方法的蛋白酶酶活力快速定量方法
KR101187973B1 (ko) 중합체의 제조 방법
JP2007057506A (ja) 樹脂組成物中の微量添加物の分析方法および樹脂組成物の寿命分析方法
CN104049624B (zh) 化工产品生产模式优化方法、装置和连续型化工系统
CN117670578B (zh) 一种基于信息自动化的颗粒冲剂生产监管方法
Jiang et al. Noncontact analysis of the fiber weight per unit area in prepreg by near-infrared spectroscopy