GB996306A - Process for the manufacture of 1:1:2-trichloroethane - Google Patents
Process for the manufacture of 1:1:2-trichloroethaneInfo
- Publication number
- GB996306A GB996306A GB1048662A GB1048662A GB996306A GB 996306 A GB996306 A GB 996306A GB 1048662 A GB1048662 A GB 1048662A GB 1048662 A GB1048662 A GB 1048662A GB 996306 A GB996306 A GB 996306A
- Authority
- GB
- United Kingdom
- Prior art keywords
- temperature
- reaction
- gaseous
- chloroethane
- trichloroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1 : 1 : 2-trichloroethane is made by reacting gaseous chlorine with gaseous ethylene at 30 DEG to 200 DEG C., preferably 70 DEG to 150 DEG C, while irradiated with light in the range of 350 to 900 mm in the presence of at least one gaseous chloroethane, the partial pressure of which in the reaction zone prior to reaction is 10 to 50% of the total pressure and preferably in the presence of water in an amount sufficient to absorb the hydrogen chloride formed. The reaction velocity may be regulated by varying the intensity of the radiant flux and may be carried out by dividing the reaction zone into a plurality of sections, each section having a different temperature and each section maintained at that temperature by means of temperature-controlled light sources, each of which is independent from the other light sources. In the examples, the chloroethane added is 1 : 2-dichloroethane and the products include 1 : 1 : 2 : 2-tetrachloroethane.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE1961F0033511 DE1146044B (en) | 1961-04-25 | 1961-04-25 | Process for the production of 1, 1, 2-trichloroethane |
Publications (1)
Publication Number | Publication Date |
---|---|
GB996306A true GB996306A (en) | 1965-06-23 |
Family
ID=7095123
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1048662A Expired GB996306A (en) | 1961-04-25 | 1962-03-19 | Process for the manufacture of 1:1:2-trichloroethane |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE1146044B (en) |
GB (1) | GB996306A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3629085A (en) * | 1967-12-19 | 1971-12-21 | Solvay | Photochemical purification of 1,2-dichlorethane |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE529524C (en) * | 1927-04-29 | 1931-07-14 | Albert Maier | Process for the production of ethylene chloride from ethylene or gases containing ethylene and chlorine |
DE522959C (en) * | 1927-08-26 | 1931-04-20 | Albert Maier | Process for the production of chlorinated ethanes, especially 1: 1: 2 trichloroethane |
-
1961
- 1961-04-25 DE DE1961F0033511 patent/DE1146044B/en active Pending
-
1962
- 1962-03-19 GB GB1048662A patent/GB996306A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3629085A (en) * | 1967-12-19 | 1971-12-21 | Solvay | Photochemical purification of 1,2-dichlorethane |
Also Published As
Publication number | Publication date |
---|---|
DE1146044B (en) | 1963-03-28 |
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