GB977686A - Process for concentrating a multi-component liquid material and apparatus therefor - Google Patents

Process for concentrating a multi-component liquid material and apparatus therefor

Info

Publication number
GB977686A
GB977686A GB15032/63A GB1503263A GB977686A GB 977686 A GB977686 A GB 977686A GB 15032/63 A GB15032/63 A GB 15032/63A GB 1503263 A GB1503263 A GB 1503263A GB 977686 A GB977686 A GB 977686A
Authority
GB
United Kingdom
Prior art keywords
chiller
crystals
drum
via valve
liquor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB15032/63A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Phillips Petroleum Co
Original Assignee
Phillips Petroleum Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Phillips Petroleum Co filed Critical Phillips Petroleum Co
Publication of GB977686A publication Critical patent/GB977686A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
    • A23C1/00—Concentration, evaporation or drying
    • A23C1/06—Concentration by freezing out the water
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
    • A23L2/08—Concentrating or drying of juices
    • A23L2/12—Concentrating or drying of juices by freezing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
    • C12H6/04—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by freezing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Organic Chemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Zoology (AREA)
  • General Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Wood Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Genetics & Genomics (AREA)
  • General Health & Medical Sciences (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Tea And Coffee (AREA)

Abstract

977,686. Concentrating liquids by freezing. PHILLIPS PETROLEUM CO. April 17, 1963 [May 14, 19621, No. 15032/63. Heading F4H. In a process for concentrating solutions by freezing, one component of the solution is partly crystallized in a chiller and the crystals are then passed to a storage zone in which the crystals are allowed to grow before being passed to a purification column. As shown, beer is passed through a line 11 to a jacketed chiller 13 having a scraper 15, the resultant ice crystals and mother liquor being then forwarded to a storage vessel 19 containing an agitator 20. The crystals remain from one to ten hours in vessel 19 during which time they increase in size, and are then passed to a purification column 22. In the latter the crystals move as a compact mass towards a heater 24 which melts the crystals, part of the melt water being forced back through the crystal mass by a pulse unit 28 to remove occluded liquor therefrom and the remainder of the melt being extracted through line 25. The mother liquor is extracted from the purification column through a filter 23 and is collected in a drum 27, whence it is supplied, via line 32, to the inlet of a second chiller 13a in which the process is repeated. A third stage 13b, 19b, 22b and 25b is provided and receives mother liquor from the drum 27a of the second stage. Liquor from drum 27 may be recycled to the inlet of chiller 13 via valve 51 while liquor from drum 27a may be recycled to chiller 13 via valve 55 or to chiller 13a via valve 53. Similarly, liquor from drum 27b may be returned to chiller 13 via valve 61, chiller 13a via valve 59 and chiller 13b via valve 57. The chillers 13, 13a and 13b receive and return refrigerant from and to respective receivers 39, 39a and 39b having connections with a refrigeration unit 37. The process may be used for milk, fruit juices, vegetable juices, vinegar, coffee, tea and wine or to separate mixtures of organic materials. Specification 807,100 is referred to.
GB15032/63A 1962-05-14 1963-04-17 Process for concentrating a multi-component liquid material and apparatus therefor Expired GB977686A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US19447262A 1962-05-14 1962-05-14
NL6400608A NL6400608A (en) 1962-05-14 1964-01-27

Publications (1)

Publication Number Publication Date
GB977686A true GB977686A (en) 1964-12-09

Family

ID=26643712

Family Applications (1)

Application Number Title Priority Date Filing Date
GB15032/63A Expired GB977686A (en) 1962-05-14 1963-04-17 Process for concentrating a multi-component liquid material and apparatus therefor

Country Status (6)

Country Link
BR (1) BR6348678D0 (en)
CH (1) CH410862A (en)
DE (1) DE1286507B (en)
FR (1) FR1365366A (en)
GB (1) GB977686A (en)
NL (1) NL6400608A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0084895A2 (en) * 1982-01-11 1983-08-03 Nederlandse Organisatie voor toegepast-natuurwetenschappelijk onderzoek TNO A process for the continuous partial crystallization and the separation of a liquid mixture and a device for carrying out this process
FR2738754A1 (en) * 1995-09-18 1997-03-21 Renault Soln. crystallisation and filtration using large seed quantity
FR2815701A1 (en) * 2000-10-19 2002-04-26 Pierre Bertaud Extraction procedure and plant for frozen substance such as pure water from sea water uses two vessels with coils for circulating refrigerant

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL35793A (en) * 1969-12-12 1973-10-25 Stamicarbon Continuous process for crystallization
JPH0738921B2 (en) * 1983-12-27 1995-05-01 チエング，シング−ワング Fractional solidification method and equipment used therefor
US4787985A (en) * 1987-08-25 1988-11-29 Grenco Process Technology B.V. Multi-stage purification unit process
AT389122B (en) * 1988-05-17 1989-10-25 METHOD FOR PRODUCING CONCENTRATES FROM WATER-LIQUID

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE968452C (en) * 1951-11-16 1958-02-20 Dr Heinrich Ratte Process for the separation of liquids or substances by crystallization
DE1192155B (en) * 1955-03-17 1965-05-06 Phillips Petroleum Company, Bartlesville, OkIa. (V. St. A.) Process for the continuous purification of crystal suspensions
US2881230A (en) * 1955-09-26 1959-04-07 Phillips Petroleum Co Fractional crystallization process

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0084895A2 (en) * 1982-01-11 1983-08-03 Nederlandse Organisatie voor toegepast-natuurwetenschappelijk onderzoek TNO A process for the continuous partial crystallization and the separation of a liquid mixture and a device for carrying out this process
EP0084895A3 (en) * 1982-01-11 1983-08-10 Nederlandse Centrale Organisatie Voor Toegepast-Natuurwetenschappelijk Onderzoek A process for the continuous partial crystallization and the separation of a liquid mixture and a device for carrying out this process
FR2738754A1 (en) * 1995-09-18 1997-03-21 Renault Soln. crystallisation and filtration using large seed quantity
FR2815701A1 (en) * 2000-10-19 2002-04-26 Pierre Bertaud Extraction procedure and plant for frozen substance such as pure water from sea water uses two vessels with coils for circulating refrigerant

Also Published As

Publication number Publication date
CH410862A (en) 1966-04-15
BR6348678D0 (en) 1973-08-14
NL6400608A (en) 1965-07-28
DE1286507B (en) 1969-01-09
FR1365366A (en) 1964-07-03

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