GB957985A - Process for the preparation of 2:5-furandicarboxylic acid - Google Patents

Process for the preparation of 2:5-furandicarboxylic acid

Info

Publication number
GB957985A
GB957985A GB7698/62A GB769862A GB957985A GB 957985 A GB957985 A GB 957985A GB 7698/62 A GB7698/62 A GB 7698/62A GB 769862 A GB769862 A GB 769862A GB 957985 A GB957985 A GB 957985A
Authority
GB
United Kingdom
Prior art keywords
acid
water
sulphuric acid
eliminated
saccharic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB7698/62A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Schweiz AG
Original Assignee
Ciba AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba AG filed Critical Ciba AG
Publication of GB957985A publication Critical patent/GB957985A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/56—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/68—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Furan Compounds (AREA)

Abstract

2:5 Furandicarboxylic acid is prepared by heating a tetrahydroxy-butane-dicarboxylic acid HOOC-(CHOH)4-COOH, with concentrated sulphuric acid, first at 85 to 120 DEG C., until two molecular proportions of water have been eliminated and then at above 120 DEG C., preferably at 125-135 DEG C., until a third molecular proportion of water has been eliminated. Manno-saccharic, idosaccharic, talomucic, allomucic acids may be used or a reaction mixture obtained by mixing monopotassium saccharate with concentrated sulphuric acid which forms saccharic acid in situ. Sulphuric acid of at least 90%, preferably 100% strength, is used and zinc or aluminium sulphate may be added to the reaction. The product is washed with water and filtered and purified by way of its calcium or disodium salt.
GB7698/62A 1961-03-07 1962-02-27 Process for the preparation of 2:5-furandicarboxylic acid Expired GB957985A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH272761A CH387656A (en) 1961-03-07 1961-03-07 Process for the preparation of 2,5-furandicarboxylic acid

Publications (1)

Publication Number Publication Date
GB957985A true GB957985A (en) 1964-05-13

Family

ID=4240239

Family Applications (1)

Application Number Title Priority Date Filing Date
GB7698/62A Expired GB957985A (en) 1961-03-07 1962-02-27 Process for the preparation of 2:5-furandicarboxylic acid

Country Status (2)

Country Link
CH (1) CH387656A (en)
GB (1) GB957985A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9506090B2 (en) 2012-09-21 2016-11-29 Synthetic Genomics, Inc. Method for synthesizing FDCA and derivates thereof
US9528133B2 (en) 2012-09-21 2016-12-27 Synthetic Genomics, Inc. Compositions and methods for producing chemicals and derivatives thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9506090B2 (en) 2012-09-21 2016-11-29 Synthetic Genomics, Inc. Method for synthesizing FDCA and derivates thereof
US9528133B2 (en) 2012-09-21 2016-12-27 Synthetic Genomics, Inc. Compositions and methods for producing chemicals and derivatives thereof

Also Published As

Publication number Publication date
CH387656A (en) 1965-02-15

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