GB927450A - Process for the manufacture of succinic acid and the alkali-metal salts thereof - Google Patents

Process for the manufacture of succinic acid and the alkali-metal salts thereof

Info

Publication number
GB927450A
GB927450A GB2996561A GB2996561A GB927450A GB 927450 A GB927450 A GB 927450A GB 2996561 A GB2996561 A GB 2996561A GB 2996561 A GB2996561 A GB 2996561A GB 927450 A GB927450 A GB 927450A
Authority
GB
United Kingdom
Prior art keywords
succinic acid
alkali metal
acid
metal salts
sulphate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2996561A
Inventor
Walter Voss
Rainer Knopp
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Filmfabrik Wolfen VEB
Original Assignee
Filmfabrik Wolfen VEB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Filmfabrik Wolfen VEB filed Critical Filmfabrik Wolfen VEB
Publication of GB927450A publication Critical patent/GB927450A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/29Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with halogen-containing compounds which may be formed in situ

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Succinic acid, or its alkali metal salt, is prepared by the oxidation of an alkali metal salt of a -hydroxy-glutonic acid or of 2:21-dihydroxy-adipic acid, or a mixture of alkali metal salts of these acids, by alkali metal hypochlorite in a alkaline or neutral aqueous solution in the presence of a catalyst, known to be capable of promoting the decomposition of hypochlorites accompanied by the evaluation of oxygen, and the salt of succinic acid obtained converted, if desired, into the free acid. Specific catalysts are cobaltous nitrate, nickelous sulphate or a mixture of nickelous sulphate and cupric sulphate. Excess of hypochlorite is advantageous. On completion of the reaction and removal of the catalyst the solution may be acidified with hydrochloric acid, evaporated to dryness and the succinic acid extracted with acetone. Examples are given.
GB2996561A 1960-12-22 1961-08-18 Process for the manufacture of succinic acid and the alkali-metal salts thereof Expired GB927450A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DD7135360 1960-12-22

Publications (1)

Publication Number Publication Date
GB927450A true GB927450A (en) 1963-05-29

Family

ID=5477577

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2996561A Expired GB927450A (en) 1960-12-22 1961-08-18 Process for the manufacture of succinic acid and the alkali-metal salts thereof

Country Status (4)

Country Link
CH (1) CH406180A (en)
DE (1) DE1171416B (en)
FR (1) FR1297380A (en)
GB (1) GB927450A (en)

Also Published As

Publication number Publication date
DE1171416B (en) 1964-06-04
CH406180A (en) 1966-01-31
FR1297380A (en) 1962-06-29

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