GB914428A - Process for the production of ª-, ª--dichloropropionic acid - Google Patents

Process for the production of ª-, ª--dichloropropionic acid

Info

Publication number
GB914428A
GB914428A GB3295161A GB3295161A GB914428A GB 914428 A GB914428 A GB 914428A GB 3295161 A GB3295161 A GB 3295161A GB 3295161 A GB3295161 A GB 3295161A GB 914428 A GB914428 A GB 914428A
Authority
GB
United Kingdom
Prior art keywords
acid
chlorinating
dichloropropionic
production
dichloropropionic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB3295161A
Inventor
Helmut Schlecht
Hans Albers
Robert Aurnhammer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB914428A publication Critical patent/GB914428A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0231—Halogen-containing compounds
    • B01J31/0232—Halogen-containing compounds also containing elements or functional groups covered by B01J31/0201 - B01J31/0228
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0215—Sulfur-containing compounds
    • B01J31/0222—Sulfur-containing compounds comprising sulfonyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0237—Amines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0271—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds also containing elements or functional groups covered by B01J31/0201 - B01J31/0231
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/363—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/15—Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen containing halogen
    • C07C53/19—Acids containing three or more carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

a ,a -Dichloropropionic acid is prepared by chlorinating a -chloropropionic acid at 160 DEG -180 DEG C., or chlorinating propionic acid at about 120 DEG C. to form a -chloropropionic acid and further chlorinating as above, in the presence of a compound RNHSO2X, where R is hydrogen or alkyl and X is hydroxy, alkoxy or a halogen. Specified catalysts are sulphamic acid, its acid chloride and its esters, e.g. H2NSO3CH3 and C2H5NHSO2Cl; these may be formed in situ, e.g. the last from ethylamine and sulphuryl chloride. Other organic additives which boil above a ,a -dichloropropionic acid and are soluble in the chlorination mixture may be present, e.g. aliphatic or aromatic sulphochlorides.
GB3295161A 1960-09-23 1961-09-14 Process for the production of ª-, ª--dichloropropionic acid Expired GB914428A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEB59488A DE1133710B (en) 1960-09-23 1960-09-23 Process for the production of ª ‡, ª ‡ -Dichloropropionic acid

Publications (1)

Publication Number Publication Date
GB914428A true GB914428A (en) 1963-01-02

Family

ID=6972478

Family Applications (1)

Application Number Title Priority Date Filing Date
GB3295161A Expired GB914428A (en) 1960-09-23 1961-09-14 Process for the production of ª-, ª--dichloropropionic acid

Country Status (2)

Country Link
DE (1) DE1133710B (en)
GB (1) GB914428A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3452089A (en) * 1966-06-09 1969-06-24 Michigan Chem Corp Production of alpha,alpha-dihalo-aliphatic acids

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3452089A (en) * 1966-06-09 1969-06-24 Michigan Chem Corp Production of alpha,alpha-dihalo-aliphatic acids

Also Published As

Publication number Publication date
DE1133710B (en) 1962-07-26

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