GB901879A - Process for recovering adipic acid from the reaction products of the air-oxidation of cyclohexane - Google Patents
Process for recovering adipic acid from the reaction products of the air-oxidation of cyclohexaneInfo
- Publication number
- GB901879A GB901879A GB29305/60A GB2930560A GB901879A GB 901879 A GB901879 A GB 901879A GB 29305/60 A GB29305/60 A GB 29305/60A GB 2930560 A GB2930560 A GB 2930560A GB 901879 A GB901879 A GB 901879A
- Authority
- GB
- United Kingdom
- Prior art keywords
- adipic acid
- water
- cyclohexane
- oxidation
- aqueous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 title abstract 12
- 235000011037 adipic acid Nutrition 0.000 title abstract 6
- 239000001361 adipic acid Substances 0.000 title abstract 6
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 title abstract 3
- 239000007795 chemical reaction product Substances 0.000 title abstract 3
- 238000007254 oxidation reaction Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- 150000001279 adipic acids Chemical class 0.000 abstract 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract 2
- 239000000284 extract Substances 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- JSZOAYXJRCEYSX-UHFFFAOYSA-N 1-nitropropane Chemical compound CCC[N+]([O-])=O JSZOAYXJRCEYSX-UHFFFAOYSA-N 0.000 abstract 1
- FGLBSLMDCBOPQK-UHFFFAOYSA-N 2-nitropropane Chemical compound CC(C)[N+]([O-])=O FGLBSLMDCBOPQK-UHFFFAOYSA-N 0.000 abstract 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000006286 aqueous extract Substances 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- HPXRVTGHNJAIIH-UHFFFAOYSA-N cyclohexanol Chemical compound OC1CCCCC1 HPXRVTGHNJAIIH-UHFFFAOYSA-N 0.000 abstract 1
- 229910001882 dioxygen Inorganic materials 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- MCSAJNNLRCFZED-UHFFFAOYSA-N nitroethane Chemical compound CC[N+]([O-])=O MCSAJNNLRCFZED-UHFFFAOYSA-N 0.000 abstract 1
- LYGJENNIWJXYER-UHFFFAOYSA-N nitromethane Chemical compound C[N+]([O-])=O LYGJENNIWJXYER-UHFFFAOYSA-N 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
- C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
- C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
- C07C51/316—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with oxides of nitrogen or nitrogen-containing mineral acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US838629A US3023238A (en) | 1959-09-08 | 1959-09-08 | Process for recovering adipic acid from the reaction products of the air-oxidation of cyclohexane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB901879A true GB901879A (en) | 1962-07-25 |
Family
ID=25277636
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB29305/60A Expired GB901879A (en) | 1959-09-08 | 1960-08-24 | Process for recovering adipic acid from the reaction products of the air-oxidation of cyclohexane |
Country Status (8)
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1044446A (en) * | 1963-03-30 | 1966-09-28 | Inst Chemii Ogolnej | Improvements in or relating to a method of distilling chemical substances |
| FR1584849A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 1968-09-30 | 1970-01-02 | ||
| US4450291A (en) * | 1983-05-02 | 1984-05-22 | Monsanto Company | Decontamination of KA oil refinement waste stream |
| US5104492A (en) * | 1990-07-11 | 1992-04-14 | The Regents Of The University Of California | Recovery of carboxylic acids from water by precipitation from organic solutions |
| FR2697247B1 (fr) * | 1992-10-22 | 1994-12-02 | Rhone Poulenc Chimie | Procédé d'hydroxycarbonylation d'acides penténoiques. |
| TW460452B (en) * | 1998-09-14 | 2001-10-21 | Rhodia Fiber & Amp Resin Inter | Process for the crystallization of carboxylic acid and process for manufacturing crystalline carboxylic acid |
| FR2795720B1 (fr) * | 1999-06-29 | 2003-05-02 | Rhone Poulenc Fibres | Procede de cristallisation d'acide carboxylique et procede de fabrication d'acide carboxylique cristallise |
| EP1198444A1 (en) * | 1999-07-23 | 2002-04-24 | Chemintel (India) Private Limited | Process for crystallization of dicarboxylic acids |
| CN103732569B (zh) * | 2011-06-17 | 2016-06-29 | 英威达技术有限责任公司 | 使用水解酶来增加废物流中的单体含量 |
| US9650653B2 (en) | 2011-06-30 | 2017-05-16 | Invista North America S.A.R.L. | Bioconversion process for producing nylon-7, nylon-7,7 and polyesters |
| US9102958B2 (en) | 2011-12-16 | 2015-08-11 | Invista North America S.á.r.l. | Methods of producing 6-carbon chemicals via CoA-dependent carbon chain elongation associated with carbon storage |
| US9102960B2 (en) | 2011-12-16 | 2015-08-11 | Invista North America S.á.r.l. | Methods of producing 6-carbon chemicals via CoA-dependent carbon chain elongation associated with carbon storage |
| BR112015013413A2 (pt) | 2012-12-14 | 2017-11-14 | Invista Tech Sarl | método para biosintetizar um produto e hospedeiro recombinante |
| WO2014105797A2 (en) | 2012-12-31 | 2014-07-03 | Invista North America S.A.R.L. | Methods of producing 7-carbon chemicals via pyruvate and succinate semialdehyde aldol condensation |
| CN105189764A (zh) | 2012-12-31 | 2015-12-23 | 英威达技术有限责任公司 | 通过与辅酶b合成相关的c1碳链延伸生产7-碳化学物的方法 |
| EP2938734A2 (en) | 2012-12-31 | 2015-11-04 | Invista Technologies S.A R.L. | Methods of producing 7-carbon chemicals via aromatic compounds |
| EP2938731A2 (en) | 2012-12-31 | 2015-11-04 | Invista Technologies S.A R.L. | Methods of producing 7-carbon chemicals via carbon chain elongation associated with cyclohexane carboxylate synthesis |
| EP2938730A2 (en) | 2012-12-31 | 2015-11-04 | Invista Technologies S.A R.L. | Methods of producing 6-carbon chemicals via methyl-ester shielded carbon chain elongation |
| EP2938732A1 (en) | 2012-12-31 | 2015-11-04 | Invista Technologies S.à.r.l. | Methods of producing 7-carbon chemicals from long chain fatty acids via oxidative cleavage |
| WO2014105794A2 (en) | 2012-12-31 | 2014-07-03 | Invista North America S.A.R.L. | Methods of producing 7-carbon chemicals via methyl-ester shielded carbon chain elongation |
| CN106574283A (zh) | 2014-05-15 | 2017-04-19 | 英威达技术有限责任公司 | 使用2,6‑二氨基庚二酸作为2‑氨基庚二酸的前体生产6‑碳化学品的方法 |
| US9988654B2 (en) | 2014-06-16 | 2018-06-05 | Invista North America S.A.R.L. | Methods, reagents and cells for biosynthesizing compounds |
| BR112016029375A2 (pt) | 2014-06-16 | 2017-10-17 | Invista Tech Sarl | métodos, reagentes e células para biossintetizar compostos |
| CN106795535A (zh) | 2014-06-16 | 2017-05-31 | 英威达技术有限责任公司 | 用于生物合成化合物的方法，试剂和细胞 |
| US9938543B2 (en) | 2014-06-16 | 2018-04-10 | Invista North America S.A.R.L. | Methods, reagents and cells for biosynthesizing glutarate methyl ester |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2675407A (en) * | 1952-04-10 | 1954-04-13 | Standard Oil Dev Co | Air oxidation of cycloalkanes |
| US2870203A (en) * | 1955-05-19 | 1959-01-20 | Du Pont | Chloroform extraction process for improving recovery of adipic acid |
-
0
- NL NL255708D patent/NL255708A/xx unknown
-
1959
- 1959-09-08 US US838629A patent/US3023238A/en not_active Expired - Lifetime
-
1960
- 1960-08-24 GB GB29305/60A patent/GB901879A/en not_active Expired
- 1960-09-07 DE DE19601418702 patent/DE1418702A1/de active Pending
- 1960-09-07 SE SE8551/60A patent/SE302299B/xx unknown
- 1960-09-07 BE BE594819A patent/BE594819A/fr unknown
- 1960-09-07 DK DK354560AA patent/DK106607C/da active
- 1960-09-08 CH CH1016760A patent/CH400116A/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NL255708A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | |
| DK106607C (da) | 1967-02-27 |
| US3023238A (en) | 1962-02-27 |
| BE594819A (fr) | 1961-03-07 |
| CH400116A (fr) | 1965-10-15 |
| SE302299B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1968-07-15 |
| DE1418702A1 (de) | 1968-12-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB901879A (en) | Process for recovering adipic acid from the reaction products of the air-oxidation of cyclohexane | |
| GB963368A (en) | Process for the recovery of constituent diamines and diacids from nylon | |
| US2789136A (en) | Recovery of nitrocyclohexane and adipic acid | |
| US3726917A (en) | Process for preparing adipic acid | |
| GB841323A (en) | Improvements in or relating to the manufacture of hydrogen peroxide | |
| US2223797A (en) | Recovery of lactic acids from crude solutions thereof | |
| GB1109543A (en) | A method of processing the reaction mixture from the oxidation of cyclohexane | |
| GB1004131A (en) | Reclamation of succinic and/or glutaric acid from chemical process streams | |
| GB928783A (en) | Purification of solutions obtained in the production of hydrogen peroxide | |
| GB841653A (en) | Process for the production of dibasic and monobasic acids | |
| US2870203A (en) | Chloroform extraction process for improving recovery of adipic acid | |
| GB823507A (en) | Improvements in or relating to the purification of tetrachlorophthalic acid and its anhydride | |
| GB1019544A (en) | Improvements in and relating to methods of preparing cycloalkanone-oximes and lactams in a concentrated acid medium | |
| GB1015828A (en) | Production of adipic acid | |
| GB950543A (en) | Recovery of by-product adipic acid | |
| GB963359A (en) | Chemical process for recovery of vanadium and copper catalysts | |
| US3350444A (en) | Process for separating cyclohexane oxidation products | |
| GB870105A (en) | Improvements in the recovery of adipic acid from oxidation products of cyclohexane | |
| GB1121478A (en) | Improvements in the purification of pyromellitic dianhydride and/or acid | |
| GB982751A (en) | Separation of dibasic acids | |
| GB855751A (en) | A process for the preparation of aromatic dicarboxylic acids | |
| GB1002973A (en) | Improvements in or relating to the production of adipic acid | |
| GB797797A (en) | Process for recovering pure isophthalic and terephthalic acid | |
| GB804686A (en) | Improvements relating to the purification of lactams | |
| GB1359879A (en) | Preparation of organic acids and esters |