GB896766A - Improvements in and relating to nitriding aluminum - Google Patents

Improvements in and relating to nitriding aluminum

Info

Publication number
GB896766A
GB896766A GB21282/60A GB2128260A GB896766A GB 896766 A GB896766 A GB 896766A GB 21282/60 A GB21282/60 A GB 21282/60A GB 2128260 A GB2128260 A GB 2128260A GB 896766 A GB896766 A GB 896766A
Authority
GB
United Kingdom
Prior art keywords
aluminium
mixture
fluoride
temperature
nitride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB21282/60A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Union Carbide Corp
Original Assignee
Union Carbide Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Union Carbide Corp filed Critical Union Carbide Corp
Publication of GB896766A publication Critical patent/GB896766A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/072—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with aluminium
    • C01B21/0722—Preparation by direct nitridation of aluminium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Products (AREA)
  • Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)

Abstract

Aluminium nitride is made by forming a mixture of finely divided aluminium metal and aluminium nitride and/or aluminium fluoride, nitriding the mixture by passing nitrogen gas thereover at a temperature ranging from 800 DEG -1100 DEG C., raising the temperature of the mixture to 1900 DEG C., while passing a stream of inert gas thereover, cooling the mixture, and recovering aluminium nitride. Preferably the temperature of the mixture is raised from 800 DEG -1100 DEG C. to 1900 DEG C. at a rate of 450 DEG -550 DEG C. per hour. The aluminium metal may form 40-60% by weight of the mixture, which may contain 33% of aluminium nitride and 17% of aluminium fluoride or 41,5% of aluminium nitride and 17% of aluminium fluoride. When aluminium fluoride alone is admixed with aluminium metal the mixture may be heated to 825 DEG -850 DEG C. under nitrogen, the heating may be interrupted and resumed again when the temperature declines to below 825 DEG C. and the mixture may be subsequently heated in an inert atmosphere to 1400 DEG C. to cause sublimation of the aluminium fluoride from the reaction product. An example is given.
GB21282/60A 1959-06-24 1960-06-17 Improvements in and relating to nitriding aluminum Expired GB896766A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US896766XA 1959-06-24 1959-06-24

Publications (1)

Publication Number Publication Date
GB896766A true GB896766A (en) 1962-05-16

Family

ID=22218977

Family Applications (1)

Application Number Title Priority Date Filing Date
GB21282/60A Expired GB896766A (en) 1959-06-24 1960-06-17 Improvements in and relating to nitriding aluminum

Country Status (2)

Country Link
DE (1) DE1131195B (en)
GB (1) GB896766A (en)

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4713360A (en) * 1984-03-16 1987-12-15 Lanxide Technology Company, Lp Novel ceramic materials and methods for making same
US4859640A (en) * 1986-08-13 1989-08-22 Lanxide Technology Company, Lp Method of making ceramic composite articles with shape replicated surfaces
US4923832A (en) * 1986-05-08 1990-05-08 Lanxide Technology Company, Lp Method of making shaped ceramic composites with the use of a barrier
US5017526A (en) * 1986-05-08 1991-05-21 Lanxide Technology Company, Lp Methods of making shaped ceramic composites
US5077245A (en) * 1987-01-30 1991-12-31 Kyocera Corporation Aluminum nitride-based sintered body and process for the production thereof
US5154863A (en) * 1985-10-31 1992-10-13 Kyocera Corporation Aluminum nitride-based sintered body and process for the production thereof
US5212124A (en) * 1986-08-13 1993-05-18 Lanxide Technology Company, Lp Ceramic composite articles with shape replicated surfaces
US5236786A (en) * 1986-05-08 1993-08-17 Lanxide Technology Company, Lp Shaped ceramic composites with a barrier
US5306677A (en) * 1984-03-16 1994-04-26 Lanxide Technology Company, Lp Ceramic materials
US5306676A (en) * 1993-03-09 1994-04-26 Lanxide Technology Company, Lp Silicon carbide bodies and methods of making the same
US5314850A (en) * 1985-10-31 1994-05-24 Kyocera Corporation Aluminum nitride sintered body and production thereof
US5340655A (en) * 1986-05-08 1994-08-23 Lanxide Technology Company, Lp Method of making shaped ceramic composites with the use of a barrier and articles produced thereby
US5358914A (en) * 1986-05-08 1994-10-25 Lanxide Technology Company, Lp Methods of making shaped ceramic composites

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE360038C (en) * 1913-11-20 1922-09-29 Nitrures Soc Gen Des Process for the production of aluminum nitride or complex nitrides containing aluminum nitride

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4713360A (en) * 1984-03-16 1987-12-15 Lanxide Technology Company, Lp Novel ceramic materials and methods for making same
US5306677A (en) * 1984-03-16 1994-04-26 Lanxide Technology Company, Lp Ceramic materials
US5154863A (en) * 1985-10-31 1992-10-13 Kyocera Corporation Aluminum nitride-based sintered body and process for the production thereof
US5314850A (en) * 1985-10-31 1994-05-24 Kyocera Corporation Aluminum nitride sintered body and production thereof
US5356720A (en) * 1986-05-08 1994-10-18 Lanxide Technology Company, Lp Shaped self-supporting ceramic composite bodies comprising silicon nitrides
US5236786A (en) * 1986-05-08 1993-08-17 Lanxide Technology Company, Lp Shaped ceramic composites with a barrier
US5017526A (en) * 1986-05-08 1991-05-21 Lanxide Technology Company, Lp Methods of making shaped ceramic composites
US4923832A (en) * 1986-05-08 1990-05-08 Lanxide Technology Company, Lp Method of making shaped ceramic composites with the use of a barrier
US5340655A (en) * 1986-05-08 1994-08-23 Lanxide Technology Company, Lp Method of making shaped ceramic composites with the use of a barrier and articles produced thereby
US5358914A (en) * 1986-05-08 1994-10-25 Lanxide Technology Company, Lp Methods of making shaped ceramic composites
US5436209A (en) * 1986-05-08 1995-07-25 Lanxide Technology Company, Lp Set up for making shaped ceramic composites with the use of a barrier means and articles produced thereby
US5212124A (en) * 1986-08-13 1993-05-18 Lanxide Technology Company, Lp Ceramic composite articles with shape replicated surfaces
US4859640A (en) * 1986-08-13 1989-08-22 Lanxide Technology Company, Lp Method of making ceramic composite articles with shape replicated surfaces
US5077245A (en) * 1987-01-30 1991-12-31 Kyocera Corporation Aluminum nitride-based sintered body and process for the production thereof
US5306676A (en) * 1993-03-09 1994-04-26 Lanxide Technology Company, Lp Silicon carbide bodies and methods of making the same
US5436208A (en) * 1993-03-09 1995-07-25 Lanxide Technology Company, Lp Silicon carbide bodies and methods of making the same

Also Published As

Publication number Publication date
DE1131195B (en) 1962-06-14

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