GB885575A - Improvements in or relating to amino-guanidine preparation - Google Patents
Improvements in or relating to amino-guanidine preparationInfo
- Publication number
- GB885575A GB885575A GB19085/60A GB1908560A GB885575A GB 885575 A GB885575 A GB 885575A GB 19085/60 A GB19085/60 A GB 19085/60A GB 1908560 A GB1908560 A GB 1908560A GB 885575 A GB885575 A GB 885575A
- Authority
- GB
- United Kingdom
- Prior art keywords
- amino
- guanidine
- relating
- reaction mixture
- guanidine preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- HAMNKKUPIHEESI-UHFFFAOYSA-N aminoguanidine Chemical compound NNC(N)=N HAMNKKUPIHEESI-UHFFFAOYSA-N 0.000 title abstract 3
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- MVXMNHYVCLMLDD-UHFFFAOYSA-N 4-methoxynaphthalene-1-carbaldehyde Chemical compound C1=CC=C2C(OC)=CC=C(C=O)C2=C1 MVXMNHYVCLMLDD-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C281/00—Derivatives of carbonic acid containing functional groups covered by groups C07C269/00 - C07C279/00 in which at least one nitrogen atom of these functional groups is further bound to another nitrogen atom not being part of a nitro or nitroso group
- C07C281/16—Compounds containing any of the groups, e.g. aminoguanidine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Amino-guanidine is prepared by reacting an aqueous solution of hydrazine having a concentration of from 1% to 6% by weight with calcium cyanamide at ambient temperatures, filtering the reaction mixture so produced, adjusting its pH to a value of from 3 to 5, heating the reaction mixture to a temperature of at least 75 DEG C. for at least one hour and thereafter precipitating and recovering the amino-guanidine so formed.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR885575X | 1959-07-10 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB885575A true GB885575A (en) | 1961-12-28 |
Family
ID=9375517
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB19085/60A Expired GB885575A (en) | 1959-07-10 | 1960-05-30 | Improvements in or relating to amino-guanidine preparation |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB885575A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1518197B1 (en) * | 1963-10-12 | 1969-09-11 | Wasagchemie Ag | Process for the production of triamino guanidine nitrate |
US3673253A (en) * | 1967-02-24 | 1972-06-27 | Bayer Ag | Process for the production of aminoguanidine bicarbonate |
US4906778A (en) * | 1988-08-29 | 1990-03-06 | Amoco Corporation | Process for the production of aminoguanidine bicarbonate |
US5559243A (en) * | 1994-12-13 | 1996-09-24 | Nippon Carbide Kogyo Kabushiki Kaisha | Processes for producing a salt of N-guanidino thiourea and 3-amino-5-mercapto-1,2,4-triazole |
-
1960
- 1960-05-30 GB GB19085/60A patent/GB885575A/en not_active Expired
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1518197B1 (en) * | 1963-10-12 | 1969-09-11 | Wasagchemie Ag | Process for the production of triamino guanidine nitrate |
US3673253A (en) * | 1967-02-24 | 1972-06-27 | Bayer Ag | Process for the production of aminoguanidine bicarbonate |
US4906778A (en) * | 1988-08-29 | 1990-03-06 | Amoco Corporation | Process for the production of aminoguanidine bicarbonate |
US5559243A (en) * | 1994-12-13 | 1996-09-24 | Nippon Carbide Kogyo Kabushiki Kaisha | Processes for producing a salt of N-guanidino thiourea and 3-amino-5-mercapto-1,2,4-triazole |
US5714617A (en) * | 1994-12-13 | 1998-02-03 | Nippon Carbide Kogyo Kabushiki Kaisha | Processes for producing a salt of N-guanidino thiourea and 3-amino-5-mercapto-1,2,4-triazole |
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