GB853769A - A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer - Google Patents

A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer

Info

Publication number
GB853769A
GB853769A GB2684957A GB2684957A GB853769A GB 853769 A GB853769 A GB 853769A GB 2684957 A GB2684957 A GB 2684957A GB 2684957 A GB2684957 A GB 2684957A GB 853769 A GB853769 A GB 853769A
Authority
GB
United Kingdom
Prior art keywords
washing
catalyst residues
catalyst
polymer
treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2684957A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bergwerksgesellschaft Hibernia AG
Original Assignee
Bergwerksgesellschaft Hibernia AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksgesellschaft Hibernia AG filed Critical Bergwerksgesellschaft Hibernia AG
Publication of GB853769A publication Critical patent/GB853769A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/02Neutralisation of the polymerisation mass, e.g. killing the catalyst also removal of catalyst residues

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Dilute solutions of alcohols in hydrocarbons which contain catalyst residues from their use in the washing of polymers, are treated with gaseous ammonia and the precipitated catalyst residues and any dissolved ammonia are subsequently separated whereby the alcohol/hydrocarbon solution is ready for re-use. The method is suitable for the removal of halogen containing aluminium and titanium compounds from washing solutions, such as 5% propanol in cyclohexane, which have been used in the purification of polyolefines obtained by Ziegler low pressure processes.ALSO:Dilute solutions of alcohols in hydrocarbons which contain catalyst residues from their use in the washing of polymers (e.g. polyolefines produced by Ziegler catalysts), are treated with gaseous ammonia to precipitate the catalyst residues.
GB2684957A 1956-09-25 1957-08-26 A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer Expired GB853769A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEB41881A DE1029152B (en) 1956-09-25 1956-09-25 Process for the processing of non-aqueous washing solutions, such as those obtained when cleaning low-pressure polyolefins produced by the Ziegler method using alcohols

Publications (1)

Publication Number Publication Date
GB853769A true GB853769A (en) 1960-11-09

Family

ID=6966566

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2684957A Expired GB853769A (en) 1956-09-25 1957-08-26 A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer

Country Status (6)

Country Link
BE (1) BE560278A (en)
DE (1) DE1029152B (en)
FR (1) FR1181686A (en)
GB (1) GB853769A (en)
LU (1) LU35414A1 (en)
NL (2) NL220612A (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE587490A (en) * 1959-02-12
DE1192824B (en) * 1959-09-23 1965-05-13 Exxon Research Engineering Co Process for the fractionation of a mixture of a hydrocarbon, methanol and water obtained in the polymerization of alpha-olefins

Also Published As

Publication number Publication date
NL102442C (en)
BE560278A (en)
LU35414A1 (en)
NL220612A (en)
FR1181686A (en) 1959-06-17
DE1029152B (en) 1958-04-30

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