GB853769A - A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer - Google Patents
A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymerInfo
- Publication number
- GB853769A GB853769A GB2684957A GB2684957A GB853769A GB 853769 A GB853769 A GB 853769A GB 2684957 A GB2684957 A GB 2684957A GB 2684957 A GB2684957 A GB 2684957A GB 853769 A GB853769 A GB 853769A
- Authority
- GB
- United Kingdom
- Prior art keywords
- washing
- catalyst residues
- catalyst
- polymer
- treatment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/02—Neutralisation of the polymerisation mass, e.g. killing the catalyst also removal of catalyst residues
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Cleaning By Liquid Or Steam (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Dilute solutions of alcohols in hydrocarbons which contain catalyst residues from their use in the washing of polymers, are treated with gaseous ammonia and the precipitated catalyst residues and any dissolved ammonia are subsequently separated whereby the alcohol/hydrocarbon solution is ready for re-use. The method is suitable for the removal of halogen containing aluminium and titanium compounds from washing solutions, such as 5% propanol in cyclohexane, which have been used in the purification of polyolefines obtained by Ziegler low pressure processes.ALSO:Dilute solutions of alcohols in hydrocarbons which contain catalyst residues from their use in the washing of polymers (e.g. polyolefines produced by Ziegler catalysts), are treated with gaseous ammonia to precipitate the catalyst residues.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEB41881A DE1029152B (en) | 1956-09-25 | 1956-09-25 | Process for the processing of non-aqueous washing solutions, such as those obtained when cleaning low-pressure polyolefins produced by the Ziegler method using alcohols |
Publications (1)
Publication Number | Publication Date |
---|---|
GB853769A true GB853769A (en) | 1960-11-09 |
Family
ID=6966566
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2684957A Expired GB853769A (en) | 1956-09-25 | 1957-08-26 | A method for the treatment of catalyst-containing non-aqueous washing solutions obtained from the washing of a polymer |
Country Status (6)
Country | Link |
---|---|
BE (1) | BE560278A (en) |
DE (1) | DE1029152B (en) |
FR (1) | FR1181686A (en) |
GB (1) | GB853769A (en) |
LU (1) | LU35414A1 (en) |
NL (2) | NL220612A (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE587490A (en) * | 1959-02-12 | |||
DE1192824B (en) * | 1959-09-23 | 1965-05-13 | Exxon Research Engineering Co | Process for the fractionation of a mixture of a hydrocarbon, methanol and water obtained in the polymerization of alpha-olefins |
-
0
- BE BE560278D patent/BE560278A/xx unknown
- NL NL102442D patent/NL102442C/xx active
- LU LU35414D patent/LU35414A1/xx unknown
- NL NL220612D patent/NL220612A/xx unknown
-
1956
- 1956-09-25 DE DEB41881A patent/DE1029152B/en active Pending
-
1957
- 1957-08-26 GB GB2684957A patent/GB853769A/en not_active Expired
- 1957-08-27 FR FR1181686D patent/FR1181686A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
NL102442C (en) | |
BE560278A (en) | |
LU35414A1 (en) | |
NL220612A (en) | |
FR1181686A (en) | 1959-06-17 |
DE1029152B (en) | 1958-04-30 |
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