GB822871A - Heterocyclic bis-sulphonamides - Google Patents
Heterocyclic bis-sulphonamidesInfo
- Publication number
- GB822871A GB822871A GB239/58A GB23958A GB822871A GB 822871 A GB822871 A GB 822871A GB 239/58 A GB239/58 A GB 239/58A GB 23958 A GB23958 A GB 23958A GB 822871 A GB822871 A GB 822871A
- Authority
- GB
- United Kingdom
- Prior art keywords
- treating
- compound
- carbon atoms
- sulphide
- give
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/62—Oxygen or sulfur atoms
- C07D213/70—Sulfur atoms
- C07D213/71—Sulfur atoms to which a second hetero atom is attached
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
The invention comprises compounds of the formula <FORM:0822871/IV (a)/1> wherein X is an oxygen or sulphur atom, a carbonyl group or a straight or branched saturated or unsaturated alkylene radical of 1-5 carbon atoms and their preparation either by treating the corresponding bis sulphonyl halide with ammonia, an ammonium salt, e.g. ammonium carbonate or bicarbonate, or a compound which splits off ammonia, e.g. hexamethylene tetramine, preferably in aqueous, alcoholic or aqueous-alcoholic solution, or by treating a pyridyl sulphonamide of the formula <FORM:0822871/IV (a)/2> in which R is a halogen atom with an alkalimetal sulphide or with a hydroxy- or mercaptopyridine sulphonamide to give compounds wherein X = O or S, or treating a compound of the above formula wherein R is halo-alkyl radical of 1 or 2 carbon atoms with an alkalimetal to give a compound wherein X is an alkylene radical of 2 or 4 carbon atoms, or treating a compound wherein R is a carboxy-halide group or a halo-acyl radical of 1-5 carbon atoms with a similar compound wherein R is hydrogen to give a product in which X is a -CO- bridge or an alkylene radical. Examples describe the preparation of 2 : 21-dipyridyl sulphide-5 : 51-disulphonamide. 2 : 21 - Dipyridylsulphide - 5 : 51 - disulphonyl chloride is made by diazotizing 5 : 51-diamino-2 : 21-dipyridyl sulphide and treating the product with sulphur dioxide and cuprous chloride in acetic acid.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE822871X | 1957-01-02 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB822871A true GB822871A (en) | 1959-11-04 |
Family
ID=6744509
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB239/58A Expired GB822871A (en) | 1957-01-02 | 1958-01-02 | Heterocyclic bis-sulphonamides |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB822871A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5110937A (en) * | 1989-08-30 | 1992-05-05 | Eastman Kodak Company | Preparation of di-cation ethers |
-
1958
- 1958-01-02 GB GB239/58A patent/GB822871A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5110937A (en) * | 1989-08-30 | 1992-05-05 | Eastman Kodak Company | Preparation of di-cation ethers |
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