GB678715A - Improvements in or relating to the formation of electrically insulating surfaces on ferrous metal laminations - Google Patents

Improvements in or relating to the formation of electrically insulating surfaces on ferrous metal laminations

Info

Publication number
GB678715A
GB678715A GB188/49A GB18849A GB678715A GB 678715 A GB678715 A GB 678715A GB 188/49 A GB188/49 A GB 188/49A GB 18849 A GB18849 A GB 18849A GB 678715 A GB678715 A GB 678715A
Authority
GB
United Kingdom
Prior art keywords
per cent
atmosphere
water
laminations
oxide film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB188/49A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Westinghouse Electric International Co
Original Assignee
Westinghouse Electric International Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Westinghouse Electric International Co filed Critical Westinghouse Electric International Co
Publication of GB678715A publication Critical patent/GB678715A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/74Methods of treatment in inert gas, controlled atmosphere, vacuum or pulverulent material
    • C21D1/76Adjusting the composition of the atmosphere
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/02Pretreatment of the material to be coated

Abstract

In a method of heat-treating porous metal laminations to remove stresses and provide a highly insulating oxide film thereon, the laminations are heated to above 570 DEG C in a reducing atmosphere to reduce any surface oxides present and relieve stresses, cooled in a reducing atmosphere and, while in the range 450-550 DEG C subjected to an atmosphere composed of at least 20 per cent of water or a mixture of water and carbon dioxide, the balance comprising at least one gas from the group consisting of hydrogen, carbon monoxide, and nitrogen, the volume ratio H2O to O2 being greater than 0.25, the volume ratio CO2 to CO being greater than 1.2 when both are present, and the free oxygen being less than 1/2 of 1 per cent, the time of treating at 450-550 DEG C being sufficient to produce a film of Fe3O4. The initial atmosphere may be water vapour, or an atmosphere of a combusted gas analyzing 15 per cent water, 12 per cent carbon dioxide, 5.4 per cent carbon monoxide, 3 per cent hydrogen, and the balance nitrogen may be used. The time of treatment may be four hours. The laminations may be removed from the furnace, which may be of the batch or of the continuous type, at a temperature between 300 DEG C and 100 DEG C and cooled in air. The Specification as open to inspection under Sect. 91, relates also to the formation of an oxide film when the original surface is not contaminated with any other oxide film. It also refers to a temperature range of 400-570 DEG C. This subject-matter does not appear in the Specification as accepted.
GB188/49A 1948-01-15 1949-01-04 Improvements in or relating to the formation of electrically insulating surfaces on ferrous metal laminations Expired GB678715A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US678715XA 1948-01-15 1948-01-15

Publications (1)

Publication Number Publication Date
GB678715A true GB678715A (en) 1952-09-10

Family

ID=22078973

Family Applications (1)

Application Number Title Priority Date Filing Date
GB188/49A Expired GB678715A (en) 1948-01-15 1949-01-04 Improvements in or relating to the formation of electrically insulating surfaces on ferrous metal laminations

Country Status (1)

Country Link
GB (1) GB678715A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2123443A (en) * 1982-07-06 1984-02-01 Xerox Corp Oxidized steel carrier particles for electrostatographic developer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2123443A (en) * 1982-07-06 1984-02-01 Xerox Corp Oxidized steel carrier particles for electrostatographic developer

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