GB652462A - Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses - Google Patents

Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses

Info

Publication number
GB652462A
GB652462A GB2178948A GB2178948A GB652462A GB 652462 A GB652462 A GB 652462A GB 2178948 A GB2178948 A GB 2178948A GB 2178948 A GB2178948 A GB 2178948A GB 652462 A GB652462 A GB 652462A
Authority
GB
United Kingdom
Prior art keywords
sodium
relating
carboxyalkyl celluloses
manufacture
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2178948A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CALLUM ANGUS MACINNES
Imperial Chemical Industries Ltd
Original Assignee
CALLUM ANGUS MACINNES
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CALLUM ANGUS MACINNES, Imperial Chemical Industries Ltd filed Critical CALLUM ANGUS MACINNES
Priority to GB2178948A priority Critical patent/GB652462A/en
Publication of GB652462A publication Critical patent/GB652462A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00Preparation of cellulose ethers
    • C08B11/02Alkyl or cycloalkyl ethers
    • C08B11/04Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals
    • C08B11/10Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals
    • C08B11/12Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals substituted with carboxylic radicals, e.g. carboxymethylcellulose [CMC]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

Sodium salts of carboxyalkyl celluloses are made by treating a semi-moist mixture containing cellulose with the sodium salt of a chloro-fatty acid and an excess of sodium hydroxide, sufficient sodium bicarbonate being included in the mixture to convert the excess sodium hydroxide into sodium carbonate. The sodium bicarbonate is added before the etherification reaction has proceeded to any substantial extent. In one example, disintegrated sulphite woodpulp sheet is mixed with ethyl alcohol and sodium hydroxide solution, mono-chloracetic acid and then sodium bicarbonate are added, and mixing is continued for 30 minutes at 20-25 DEG C.
GB2178948A 1948-08-18 1948-08-18 Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses Expired GB652462A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2178948A GB652462A (en) 1948-08-18 1948-08-18 Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2178948A GB652462A (en) 1948-08-18 1948-08-18 Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses

Publications (1)

Publication Number Publication Date
GB652462A true GB652462A (en) 1951-04-25

Family

ID=10168828

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2178948A Expired GB652462A (en) 1948-08-18 1948-08-18 Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses

Country Status (1)

Country Link
GB (1) GB652462A (en)

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