GB652462A - Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses - Google Patents
Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl cellulosesInfo
- Publication number
- GB652462A GB652462A GB2178948A GB2178948A GB652462A GB 652462 A GB652462 A GB 652462A GB 2178948 A GB2178948 A GB 2178948A GB 2178948 A GB2178948 A GB 2178948A GB 652462 A GB652462 A GB 652462A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sodium
- relating
- carboxyalkyl celluloses
- manufacture
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/02—Alkyl or cycloalkyl ethers
- C08B11/04—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals
- C08B11/10—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals
- C08B11/12—Alkyl or cycloalkyl ethers with substituted hydrocarbon radicals substituted with acid radicals substituted with carboxylic radicals, e.g. carboxymethylcellulose [CMC]
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Sodium salts of carboxyalkyl celluloses are made by treating a semi-moist mixture containing cellulose with the sodium salt of a chloro-fatty acid and an excess of sodium hydroxide, sufficient sodium bicarbonate being included in the mixture to convert the excess sodium hydroxide into sodium carbonate. The sodium bicarbonate is added before the etherification reaction has proceeded to any substantial extent. In one example, disintegrated sulphite woodpulp sheet is mixed with ethyl alcohol and sodium hydroxide solution, mono-chloracetic acid and then sodium bicarbonate are added, and mixing is continued for 30 minutes at 20-25 DEG C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2178948A GB652462A (en) | 1948-08-18 | 1948-08-18 | Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2178948A GB652462A (en) | 1948-08-18 | 1948-08-18 | Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses |
Publications (1)
Publication Number | Publication Date |
---|---|
GB652462A true GB652462A (en) | 1951-04-25 |
Family
ID=10168828
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2178948A Expired GB652462A (en) | 1948-08-18 | 1948-08-18 | Improvements in or relating to the manufacture of water-soluble salts of carboxyalkyl celluloses |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB652462A (en) |
-
1948
- 1948-08-18 GB GB2178948A patent/GB652462A/en not_active Expired
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