GB595777A - Improvements in or relating to the preparation of arylsulphonylthioureas - Google Patents
Improvements in or relating to the preparation of arylsulphonylthioureasInfo
- Publication number
- GB595777A GB595777A GB12488/45A GB1248845A GB595777A GB 595777 A GB595777 A GB 595777A GB 12488/45 A GB12488/45 A GB 12488/45A GB 1248845 A GB1248845 A GB 1248845A GB 595777 A GB595777 A GB 595777A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sulphur
- sodium
- anhydrous
- hydrogen
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The process of obtaining nuclearly substituted or unsubstituted N - arylsulphonylthioureas which is described in Specification 595,771 and which comprises the addition of hydrogen sulphide to the corresponding arylsulphonylcyanamides, is carried out in an anhydrous medium and in the presence of anhydrous ammonia or of an anhydrous organic base or of a substance capable of generating nacent sulphur under the conditions of the reaction. Specified substances for this purpose are flowers of sulphur, sodium polysulphide, sodium thioantimonate, the disulphide of tetramethylthiouram, thionyl chloride and the peroxides such as hydrogen, sodium or benzoyl peroxides. In examples: (1) an absolute alcoholic solution of diethylamine, p - aminobenzenesulphonyl - cyanide and the disulphide of tetramethylthiouram is saturated with hydrogen sulphide to form N-(p-aminobenzenesulphonyl)-thiourea; (2) as in example (1), but using ammonia as the base and thionyl chloride as the sulphur yielding compound. A sample has been furnished under Sect. 2 (5) prepared by saturating with H2S an alcohol solution of p-aminobenzenesulphonylcyanamide containing anhydrous ammonia and hydrogen peroxide. The product is worked up as in example (1).
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR595777X | 1943-10-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB595777A true GB595777A (en) | 1947-12-16 |
Family
ID=8967095
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB12488/45A Expired GB595777A (en) | 1943-10-19 | 1945-05-17 | Improvements in or relating to the preparation of arylsulphonylthioureas |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB595777A (en) |
-
1945
- 1945-05-17 GB GB12488/45A patent/GB595777A/en not_active Expired
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