GB255811A - A process for the production of 2-hydrazino-5-nitropyridine - Google Patents

A process for the production of 2-hydrazino-5-nitropyridine

Info

Publication number
GB255811A
GB255811A GB4119/26A GB411926A GB255811A GB 255811 A GB255811 A GB 255811A GB 4119/26 A GB4119/26 A GB 4119/26A GB 411926 A GB411926 A GB 411926A GB 255811 A GB255811 A GB 255811A
Authority
GB
United Kingdom
Prior art keywords
nitropyridine
hydrazino
solvent
prepared
hydrazine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4119/26A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Evonik Operations GmbH
Original Assignee
Degussa GmbH
Deutsche Gold und Silber Scheideanstalt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa GmbH, Deutsche Gold und Silber Scheideanstalt filed Critical Degussa GmbH
Publication of GB255811A publication Critical patent/GB255811A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/72Nitrogen atoms
    • C07D213/76Nitrogen atoms to which a second hetero atom is attached
    • C07D213/77Hydrazine radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)

Abstract

255,811. Deutsche Gold-und Silber- Scheideanstalt vorm. Roessler. July 22, 1925, [Convention date]. 2-Hydrazino-5-nitropyridine is prepared by treating a 2-halogen-5-nitropyridine with hydrazinc hydrate. Preferably the reaction is effected with cooling in the presence of a solvent such as water. According to the examples, 2-hydrazino- 5-nitropyridine is obtained by (1) adding powdered 2-chlor-5-nitropyridine to hydrazine hydrate, and (2) suffusing 2-chloro-5-nitropyridine with a 50 per cent aqueous solution of hydrazine. The Specification as open to inspection under Sect. 91 (3) (a) refers also to the use of alcohol as a solvent. This subject-matter does not appear in the Specification as accepted. 2-Bromo. and 2-iodo-5-nitropyridine are prepared by diazotizing 2-amino-5-nitropyridine in the presence of concentrated hydrobromic and hydriodic acid respectively.
GB4119/26A 1925-07-22 1926-02-12 A process for the production of 2-hydrazino-5-nitropyridine Expired GB255811A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT255811X 1925-07-22

Publications (1)

Publication Number Publication Date
GB255811A true GB255811A (en) 1926-10-21

Family

ID=3670209

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4119/26A Expired GB255811A (en) 1925-07-22 1926-02-12 A process for the production of 2-hydrazino-5-nitropyridine

Country Status (1)

Country Link
GB (1) GB255811A (en)

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