GB1500466A - Preparation of di(aminophenyl)methane - Google Patents
Preparation of di(aminophenyl)methaneInfo
- Publication number
- GB1500466A GB1500466A GB20886/76A GB2088676A GB1500466A GB 1500466 A GB1500466 A GB 1500466A GB 20886/76 A GB20886/76 A GB 20886/76A GB 2088676 A GB2088676 A GB 2088676A GB 1500466 A GB1500466 A GB 1500466A
- Authority
- GB
- United Kingdom
- Prior art keywords
- mixture
- weight
- aminophenyl
- until
- earth
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OHKOAJUTRVTYSW-UHFFFAOYSA-N 2-[(2-aminophenyl)methyl]aniline Chemical compound NC1=CC=CC=C1CC1=CC=CC=C1N OHKOAJUTRVTYSW-UHFFFAOYSA-N 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 abstract 5
- -1 poly(aminophenyl)methylenes Polymers 0.000 abstract 5
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- 150000003939 benzylamines Chemical class 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 229920000768 polyamine Polymers 0.000 abstract 2
- 229920006389 polyphenyl polymer Polymers 0.000 abstract 2
- 239000010457 zeolite Substances 0.000 abstract 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 abstract 1
- 239000005995 Aluminium silicate Substances 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- 235000012211 aluminium silicate Nutrition 0.000 abstract 1
- IXWIAFSBWGYQOE-UHFFFAOYSA-M aluminum;magnesium;oxygen(2-);silicon(4+);hydroxide;tetrahydrate Chemical compound O.O.O.O.[OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Mg+2].[Al+3].[Si+4].[Si+4].[Si+4].[Si+4] IXWIAFSBWGYQOE-UHFFFAOYSA-M 0.000 abstract 1
- 150000007854 aminals Chemical class 0.000 abstract 1
- 150000004982 aromatic amines Chemical class 0.000 abstract 1
- 239000000440 bentonite Substances 0.000 abstract 1
- 229910000278 bentonite Inorganic materials 0.000 abstract 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 abstract 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 abstract 1
- 150000004985 diamines Chemical class 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 abstract 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 abstract 1
- 229910052901 montmorillonite Inorganic materials 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/24—Preparation of compounds containing amino groups bound to a carbon skeleton by reductive alkylation of ammonia, amines or compounds having groups reducible to amino groups, with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/54—Preparation of compounds containing amino groups bound to a carbon skeleton by rearrangement reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/06—Amines
- C08G12/08—Amines aromatic
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Phenolic Resins Or Amino Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/590,801 US4039581A (en) | 1975-06-27 | 1975-06-27 | Process for the preparation of di(amino phenyl)methanes |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1500466A true GB1500466A (en) | 1978-02-08 |
Family
ID=24363778
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB20886/76A Expired GB1500466A (en) | 1975-06-27 | 1976-05-20 | Preparation of di(aminophenyl)methane |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4039581A (https=) |
| JP (1) | JPS527943A (https=) |
| BE (1) | BE843441A (https=) |
| BR (1) | BR7603973A (https=) |
| DD (1) | DD125493A5 (https=) |
| DE (1) | DE2623681C2 (https=) |
| ES (1) | ES448668A1 (https=) |
| FR (1) | FR2317334A1 (https=) |
| GB (1) | GB1500466A (https=) |
| IT (1) | IT1062037B (https=) |
| MX (1) | MX3356E (https=) |
| NL (1) | NL171263C (https=) |
| SU (1) | SU691080A3 (https=) |
Families Citing this family (32)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2928182A1 (de) * | 1979-07-12 | 1981-01-29 | Bayer Ag | Verfahren zur herstellung von elastischen, gegebenenfalls zellfoermigen, polyurethanharnstoffen |
| US4294987A (en) * | 1979-12-31 | 1981-10-13 | The Upjohn Company | Process for preparing methylene dianilines |
| US4554378A (en) * | 1983-02-22 | 1985-11-19 | The Dow Chemical Company | Process for preparing polyamines with ion exchange resin catalysts |
| JPS6153514A (ja) * | 1984-08-23 | 1986-03-17 | Yokogawa Hokushin Electric Corp | ジヤイロコンパス |
| EP0245244B1 (en) * | 1985-11-12 | 1992-03-11 | The Dow Chemical Company | A process for continuously preparing aromatic polyamines with ion exchange resin catalysts |
| US5241119A (en) * | 1986-10-22 | 1993-08-31 | Eniricerche S.P.A. | Process for the preparation of 4,4'-diaminodiphenyl-methane and its derivatives |
| EP0264744B1 (en) * | 1986-10-22 | 1992-12-23 | ENIRICERCHE S.p.A. | Process for the preparation of 4,4'-diaminodiphenylmethane and its derivatives |
| EP0329367A3 (en) * | 1988-02-15 | 1990-10-31 | Mitsui Petrochemical Industries, Ltd. | Method of preparing 4,4'-methylenedianiline |
| DE19707255A1 (de) * | 1997-02-24 | 1998-08-27 | Basf Ag | Verfahren zur Herstellung von aromatischen Polyamingemischen |
| CZ296966B6 (cs) | 1997-02-24 | 2006-08-16 | Boehringer Ingelheim Pharma Gmbh & Co. Kg. | Farmaceutický prostredek |
| DE10006452A1 (de) * | 2000-02-14 | 2001-08-16 | Bayer Ag | Verfahren zur Herstellung von Diaminodiphenylmethanen |
| IT1318437B1 (it) | 2000-03-31 | 2003-08-25 | Eni Spa | Procedimento per la preparazione di miscele di metilendianilina e suoi omologhi superiori. |
| IT1318686B1 (it) * | 2000-09-07 | 2003-08-27 | Eni Spa | Procedimento per la sintesi di miscele di metilendianilina e suoiomologhi superiori con distribuzione controllata degli isomeri. |
| RU2330016C2 (ru) * | 2002-03-28 | 2008-07-27 | Хантсмэн Интернэшнл Ллс | Способ получения диаминодифенилметана и его высших гомологов |
| US7238840B2 (en) * | 2002-03-28 | 2007-07-03 | Huntsman International Llc | Process for the production of diaminodiphenylmethane and its higher homologues |
| JP4434716B2 (ja) * | 2003-12-17 | 2010-03-17 | 三菱瓦斯化学株式会社 | アミノ組成物の製造方法 |
| DE102005014847A1 (de) * | 2005-03-30 | 2006-10-05 | Basf Ag | MMDI und PMDI Herstellung mittels Gasphasenphosegenierung |
| US7943724B2 (en) * | 2005-12-08 | 2011-05-17 | Huntsman International Llc | Process for preparing diaminodiphenylmethanes |
| EP2014641A3 (en) * | 2007-06-06 | 2009-03-18 | Huntsman International Llc | Process for preparing mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates |
| EP2039676A1 (en) | 2007-09-19 | 2009-03-25 | Huntsman International Llc | Process for the production of di-and polyamines of the diphenylmethane series |
| EP2062869A1 (en) * | 2007-09-19 | 2009-05-27 | Huntsman International Llc | Process for the production of di-and polyamines of the diphenylmethane series |
| DE102008012037A1 (de) | 2008-03-01 | 2009-09-03 | Bayer Materialscience Ag | Verfahren zur Herstellung von Methylen-diphenyl-diisocyanaten |
| US20110021741A1 (en) * | 2008-04-16 | 2011-01-27 | Dow Global Technologies Inc. | Process for making polyaminopolyphenyl methanes using a mixed solid acid catalyst system |
| DE102008001469A1 (de) | 2008-04-30 | 2009-11-05 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Diaminodiphenylalkanen |
| DE102008001492A1 (de) | 2008-04-30 | 2009-11-05 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Diaminodiphenylalkanen |
| DE102008002002A1 (de) | 2008-05-27 | 2009-12-03 | Evonik Degussa Gmbh | Chlor armes mehrstufiges Verfahren zur Herstellung von cycloaliphatischen Diisocyanaten |
| PT2379486E (pt) * | 2008-12-22 | 2013-10-17 | Huntsman Int Llc | Processo para a produção de polifenilpoliaminas com pontes de metileno |
| US9656239B2 (en) | 2014-06-16 | 2017-05-23 | International Business Machines Corporation | Apparatus for controlling metals in liquids |
| HUE037918T2 (hu) | 2014-07-07 | 2018-09-28 | Covestro Deutschland Ag | Eljárás a difenilmetán sorozat di- és poliaminjainak elõállítására |
| US10538480B2 (en) | 2016-06-30 | 2020-01-21 | Covestro Deutschland Ag | Process for the production of di- and polyamines of the diphenylmethane series |
| WO2025128774A1 (en) | 2023-12-13 | 2025-06-19 | Dow Global Technologies Llc | Method for making methylene dianiline and polymethylene polyanilines |
| WO2025128775A1 (en) | 2023-12-13 | 2025-06-19 | Dow Global Technologies Llc | Method for making polymethylene polyanilines using lewis acid-modified clay catalysts |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH408038A (de) * | 1961-12-22 | 1966-02-28 | Bayer Ag | Verfahren zur Herstellung neuer aromatischer Aminoverbindungen |
| GB991157A (en) * | 1962-12-10 | 1965-05-05 | Jefferson Chem Co Inc | Polyamine preparation |
| DE1179945B (de) * | 1962-12-11 | 1964-10-22 | Basf Ag | Verfahren zur Herstellung von 4, 4'-Diaminodiphenylmethanen |
| DE1210872C2 (de) * | 1963-09-28 | 1973-01-25 | Basf Ag | Verfahren zur Herstellung von 4, 4'-Diaminodiphenylmethanen |
| US3362979A (en) * | 1964-01-02 | 1968-01-09 | Jefferson Chem Co Inc | Mixtures of methylene-bridged polyphenyl polyisocyanates |
| FR1448359A (fr) * | 1964-08-24 | 1966-08-05 | Allied Chem | Procédé de préparation de diamines et de diisocyanates et de nouveaux mélanges de bis (aminoaryl) méthanes et de méthylènebis (arylisocyanates) isomères par phosgénation |
| DE1543611A1 (de) * | 1966-09-08 | 1969-07-31 | Bayer Ag | Verfahren zur Herstellung von Polyarylmethylenpolyaminen bzw. deren Gemischen |
| US3676497A (en) * | 1968-08-06 | 1972-07-11 | Upjohn Co | Process for preparing di(aminophenyl)-methanes |
| GB1234144A (https=) * | 1969-04-15 | 1971-06-03 | ||
| US3857890A (en) * | 1969-07-25 | 1974-12-31 | Upjohn Co | Process for preparing methylene-di-anilines |
| DD109615A1 (https=) * | 1972-08-14 | 1974-11-12 |
-
1975
- 1975-06-27 US US05/590,801 patent/US4039581A/en not_active Expired - Lifetime
-
1976
- 1976-05-20 GB GB20886/76A patent/GB1500466A/en not_active Expired
- 1976-05-26 DE DE2623681A patent/DE2623681C2/de not_active Expired
- 1976-06-08 ES ES448668A patent/ES448668A1/es not_active Expired
- 1976-06-10 MX MX000299U patent/MX3356E/es unknown
- 1976-06-18 NL NLAANVRAGE7606632,A patent/NL171263C/xx not_active IP Right Cessation
- 1976-06-21 BR BR7603973A patent/BR7603973A/pt unknown
- 1976-06-24 DD DD193547A patent/DD125493A5/xx unknown
- 1976-06-24 IT IT50130/76A patent/IT1062037B/it active
- 1976-06-25 FR FR7619325A patent/FR2317334A1/fr active Granted
- 1976-06-25 SU SU762378056A patent/SU691080A3/ru active
- 1976-06-25 BE BE168343A patent/BE843441A/xx not_active IP Right Cessation
- 1976-06-25 JP JP51075381A patent/JPS527943A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2317334B1 (https=) | 1980-04-30 |
| DD125493A5 (https=) | 1977-04-20 |
| DE2623681C2 (de) | 1982-09-16 |
| DE2623681A1 (de) | 1977-01-20 |
| JPS527943A (en) | 1977-01-21 |
| US4039581A (en) | 1977-08-02 |
| SU691080A3 (ru) | 1979-10-05 |
| FR2317334A1 (fr) | 1977-02-04 |
| NL171263B (nl) | 1982-10-01 |
| ES448668A1 (es) | 1977-07-01 |
| JPS5534138B2 (https=) | 1980-09-04 |
| MX3356E (es) | 1980-10-13 |
| NL171263C (nl) | 1983-03-01 |
| BR7603973A (pt) | 1977-03-22 |
| IT1062037B (it) | 1983-06-25 |
| NL7606632A (nl) | 1976-12-29 |
| BE843441A (fr) | 1976-12-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| 732 | Registration of transactions, instruments or events in the register (sect. 32/1977) | ||
| PE20 | Patent expired after termination of 20 years |
Effective date: 19960519 |