GB1447656A - Breaking-up of emulsions - Google Patents

Breaking-up of emulsions

Info

Publication number
GB1447656A
GB1447656A GB5885473A GB5885473A GB1447656A GB 1447656 A GB1447656 A GB 1447656A GB 5885473 A GB5885473 A GB 5885473A GB 5885473 A GB5885473 A GB 5885473A GB 1447656 A GB1447656 A GB 1447656A
Authority
GB
United Kingdom
Prior art keywords
emulsion
oil
heating
mixture
iron
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB5885473A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fried Krupp Huettenwerke AG
Original Assignee
Fried Krupp Huettenwerke AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fried Krupp Huettenwerke AG filed Critical Fried Krupp Huettenwerke AG
Publication of GB1447656A publication Critical patent/GB1447656A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M175/00Working-up used lubricants to recover useful products ; Cleaning
    • C10M175/04Working-up used lubricants to recover useful products ; Cleaning aqueous emulsion based
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/042Breaking emulsions by changing the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/047Breaking emulsions with separation aids
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Colloid Chemistry (AREA)
  • Separation Of Suspended Particles By Flocculating Agents (AREA)
  • Lubricants (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Edible Oils And Fats (AREA)

Abstract

1447656 Breaking oil-in-water emulsions FRIED KRUPP HUTTENWERKE AG 19 Dec 1973 [18 Jan 1973 15 Sept 1973] 58854/73 Heading C5E Spent oil-in-water emulsion containing a non- ionic emulsifier and an anion active emulsifier is broken by adding an aqueous solution, at pH 4-9, of an electrolyte consisting of at least one Group Ia and/or Group IIa metal salt, heating the emulsion to boiling, adding before or during the heating an iron or aluminium salt, blowing air through the mixture until the emulsifiers are destroyed, and allowing the mixture to stand and separate into oil and water phases. 1-20 kg. of sodium chloride or of magnesium chloride and 0À2-2 kg. of ferrous sulphate heptahydrate can be added per cubic metre of emulsion. A spent emulsion, from the cold rolling of pickled metal and containing 1-10 wt. per cent oil, can be treated by heating at its boiling point with steam for 3 hours, blowing in air to oxidize divalent iron to trivalent iron, and leaving the mixture to stand.
GB5885473A 1973-01-18 1973-12-19 Breaking-up of emulsions Expired GB1447656A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE2302369A DE2302369C2 (en) 1973-01-18 1973-01-18 Process for the splitting of used cold-rolling emulsions and other oil-in-water emulsion systems with non-ionogenic, anion-active emulsifiers
DE2346604A DE2346604C3 (en) 1973-01-18 1973-09-15 Process for splitting used cold-rolling emulsions and other oil-in-water emulsions with non-ionic and anion-active emulsifiers

Publications (1)

Publication Number Publication Date
GB1447656A true GB1447656A (en) 1976-08-25

Family

ID=25764543

Family Applications (1)

Application Number Title Priority Date Filing Date
GB5885473A Expired GB1447656A (en) 1973-01-18 1973-12-19 Breaking-up of emulsions

Country Status (13)

Country Link
JP (1) JPS49102579A (en)
AT (1) AT330683B (en)
BE (1) BE807972A (en)
CA (1) CA1021220A (en)
CH (1) CH583057A5 (en)
DE (2) DE2302369C2 (en)
ES (1) ES420575A1 (en)
FR (1) FR2214744A1 (en)
GB (1) GB1447656A (en)
IT (1) IT1012120B (en)
LU (1) LU69165A1 (en)
NL (1) NL156061B (en)
SE (1) SE402406B (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5320413Y2 (en) * 1974-08-26 1978-05-30
JPS5129019U (en) * 1974-08-26 1976-03-02
DE4228096A1 (en) * 1992-08-26 1994-03-03 Gfr Ges Fuer Recycling Mbh Sepn. of emulsified oil from bath waste water - uses activator and additive to float emulsified oil mixt. for removal and disposal with recycling of cleaned water.
DE9407292U1 (en) * 1994-05-02 1994-07-14 Rietbergwerke GmbH & Co KG, 33397 Rietberg Device for the maintenance of cooling lubricants

Also Published As

Publication number Publication date
ES420575A1 (en) 1976-07-01
JPS49102579A (en) 1974-09-27
DE2302369B1 (en) 1974-05-02
BE807972A (en) 1974-03-15
DE2346604C3 (en) 1984-04-05
SE402406B (en) 1978-07-03
DE2302369C2 (en) 1975-01-23
ATA37174A (en) 1975-09-15
LU69165A1 (en) 1974-04-08
CH583057A5 (en) 1976-12-31
NL7315126A (en) 1974-07-22
DE2346604B2 (en) 1977-05-18
DE2346604A1 (en) 1975-04-24
AT330683B (en) 1976-07-12
FR2214744A1 (en) 1974-08-19
CA1021220A (en) 1977-11-22
IT1012120B (en) 1977-03-10
NL156061B (en) 1978-03-15

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Legal Events

Date Code Title Description
PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee