GB1351047A - Manufacture of 1-nitroanthraquinone - Google Patents
Manufacture of 1-nitroanthraquinoneInfo
- Publication number
- GB1351047A GB1351047A GB3746571A GB3746571A GB1351047A GB 1351047 A GB1351047 A GB 1351047A GB 3746571 A GB3746571 A GB 3746571A GB 3746571 A GB3746571 A GB 3746571A GB 1351047 A GB1351047 A GB 1351047A
- Authority
- GB
- United Kingdom
- Prior art keywords
- anthraquinone
- nitro
- formamide
- nitration
- aug
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YCANAXVBJKNANM-UHFFFAOYSA-N 1-nitroanthracene-9,10-dione Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2[N+](=O)[O-] YCANAXVBJKNANM-UHFFFAOYSA-N 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 abstract 3
- 150000004056 anthraquinones Chemical class 0.000 abstract 3
- FEWLNYSYJNLUOO-UHFFFAOYSA-N 1-Piperidinecarboxaldehyde Chemical compound O=CN1CCCCC1 FEWLNYSYJNLUOO-UHFFFAOYSA-N 0.000 abstract 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 abstract 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- LCEDQNDDFOCWGG-UHFFFAOYSA-N morpholine-4-carbaldehyde Chemical compound O=CN1CCOCC1 LCEDQNDDFOCWGG-UHFFFAOYSA-N 0.000 abstract 2
- 238000006396 nitration reaction Methods 0.000 abstract 2
- 239000011541 reaction mixture Substances 0.000 abstract 2
- 238000005406 washing Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 abstract 1
- SUAKHGWARZSWIH-UHFFFAOYSA-N N,N‐diethylformamide Chemical compound CCN(CC)C=O SUAKHGWARZSWIH-UHFFFAOYSA-N 0.000 abstract 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 150000003857 carboxamides Chemical class 0.000 abstract 1
- MBHINSULENHCMF-UHFFFAOYSA-N n,n-dimethylpropanamide Chemical compound CCC(=O)N(C)C MBHINSULENHCMF-UHFFFAOYSA-N 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
- C07C205/45—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by at least one doubly—bound oxygen atom, not being part of a —CHO group
- C07C205/46—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by at least one doubly—bound oxygen atom, not being part of a —CHO group the carbon skeleton containing carbon atoms of quinone rings
- C07C205/47—Anthraquinones containing nitro groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/02—Ortho- or ortho- and peri-condensed systems
- C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
- C07C2603/22—Ortho- or ortho- and peri-condensed systems containing three rings containing only six-membered rings
- C07C2603/24—Anthracenes; Hydrogenated anthracenes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2039822A DE2039822B2 (de) | 1970-08-11 | 1970-08-11 | Verfahren zur Herstellung von 1-Nitroanthrachinon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1351047A true GB1351047A (en) | 1974-04-24 |
Family
ID=5779415
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3746571A Expired GB1351047A (en) | 1970-08-11 | 1971-08-10 | Manufacture of 1-nitroanthraquinone |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3766222A (enExample) |
| CH (1) | CH556320A (enExample) |
| DE (1) | DE2039822B2 (enExample) |
| FR (1) | FR2104225A5 (enExample) |
| GB (1) | GB1351047A (enExample) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4840749A (en) * | 1986-06-17 | 1989-06-20 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for production of 1-aminoanthraquinone |
| US5149848A (en) * | 1988-02-29 | 1992-09-22 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for producing 1-aminoanthraquinones |
| US5387704A (en) * | 1992-11-11 | 1995-02-07 | Basf Aktiengesellschaft | Preparation of anthraquinones |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE794823A (fr) * | 1972-02-01 | 1973-07-31 | Sandoz Sa | Procede de purification de la 1-nitroanthraquinone |
| DE2232446C3 (de) * | 1972-07-01 | 1979-05-03 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von reinem 1-Nitroanthrachinon |
| DE2253276C2 (de) * | 1972-10-31 | 1981-11-26 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von reinem 1-Nitroanthrachinon |
| DE2237904C3 (de) * | 1972-08-02 | 1981-02-12 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von reinem 1-Nitroanthrachinon |
| DE2256644C2 (de) * | 1972-11-18 | 1983-10-20 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von reinem 1-Nitro-anthrachinon |
| DE2259074C3 (de) * | 1972-12-02 | 1982-04-22 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von praktisch 1,5-Dinitro-anthrachinon-freiem 1-Nitro-anthrachinon |
| US3959317A (en) * | 1973-01-13 | 1976-05-25 | Bayer Aktiengesellschaft | Process for the preparation of 1-nitroanthraquinone |
| DE2334713C3 (de) * | 1973-07-07 | 1980-07-10 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Isolierung von 13-Dinitroanthrachinon |
| DE2400253A1 (de) * | 1974-01-04 | 1975-07-17 | Bayer Ag | Verfahren zur herstellung von praktisch anthrachinon- und 2-nitroanthrachinonfreiem 1-nitroanthrachinon |
| JPS5387345A (en) * | 1977-01-06 | 1978-08-01 | Sumitomo Chem Co Ltd | Method of preparing 1-nitroanthraquinone |
| US4394369A (en) * | 1982-05-24 | 1983-07-19 | Fmc Corporation | Hydrogen peroxide process |
-
1970
- 1970-08-11 DE DE2039822A patent/DE2039822B2/de not_active Ceased
-
1971
- 1971-07-20 CH CH1069671A patent/CH556320A/xx not_active IP Right Cessation
- 1971-08-09 US US00170222A patent/US3766222A/en not_active Expired - Lifetime
- 1971-08-10 GB GB3746571A patent/GB1351047A/en not_active Expired
- 1971-08-11 FR FR7129353A patent/FR2104225A5/fr not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4840749A (en) * | 1986-06-17 | 1989-06-20 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for production of 1-aminoanthraquinone |
| US5149848A (en) * | 1988-02-29 | 1992-09-22 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for producing 1-aminoanthraquinones |
| US5387704A (en) * | 1992-11-11 | 1995-02-07 | Basf Aktiengesellschaft | Preparation of anthraquinones |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2104225A5 (enExample) | 1972-04-14 |
| DE2039822B2 (de) | 1974-12-19 |
| US3766222A (en) | 1973-10-16 |
| CH556320A (de) | 1974-11-29 |
| DE2039822A1 (de) | 1972-02-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |