GB1329815A - Production of tertiary acetylenic glycols by reaction of acetylene with ketones - Google Patents
Production of tertiary acetylenic glycols by reaction of acetylene with ketonesInfo
- Publication number
- GB1329815A GB1329815A GB2255871A GB2255871A GB1329815A GB 1329815 A GB1329815 A GB 1329815A GB 2255871 A GB2255871 A GB 2255871A GB 2255871 A GB2255871 A GB 2255871A GB 1329815 A GB1329815 A GB 1329815A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acetylenic glycols
- acetylene
- ketones
- reaction
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002334 glycols Chemical class 0.000 title abstract 3
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 title abstract 2
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 title abstract 2
- 150000002576 ketones Chemical class 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract 1
- CUQOHAYJWVTKDE-UHFFFAOYSA-N potassium;butan-1-olate Chemical compound [K+].CCCC[O-] CUQOHAYJWVTKDE-UHFFFAOYSA-N 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
- C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D211/06—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members
- C07D211/36—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D211/40—Oxygen atoms
- C07D211/44—Oxygen atoms attached in position 4
- C07D211/46—Oxygen atoms attached in position 4 having a hydrogen atom as the second substituent in position 4
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
- C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
- C07C29/42—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones with compounds containing triple carbon-to-carbon bonds, e.g. with metal-alkynes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702008675 DE2008675A1 (de) | 1970-02-25 | 1970-02-25 | Verfahren zur Herstellung von tertiären Acetylenglykolen durch Umsetzung von Acetylen mit Ketonen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1329815A true GB1329815A (en) | 1973-09-12 |
Family
ID=5763272
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2255871A Expired GB1329815A (en) | 1970-02-25 | 1971-04-19 | Production of tertiary acetylenic glycols by reaction of acetylene with ketones |
Country Status (6)
| Country | Link |
|---|---|
| BE (1) | BE763306A (enExample) |
| CA (1) | CA942749A (enExample) |
| CH (1) | CH554822A (enExample) |
| DE (1) | DE2008675A1 (enExample) |
| FR (1) | FR2078998A5 (enExample) |
| GB (1) | GB1329815A (enExample) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4960959A (en) * | 1987-04-04 | 1990-10-02 | Huels Aktiengesellschaft | Process for the manufacture of alkynediols by reaction of ketones with acetylene |
| JP2001002607A (ja) * | 1999-05-26 | 2001-01-09 | Basf Ag | アルキンジオールの製造方法 |
| CN1083414C (zh) * | 1999-08-25 | 2002-04-24 | 成都惟精防水材料研究所 | 2,5-二甲基-2,5-己二醇一步合成法 |
| JP2002522516A (ja) * | 1998-08-17 | 2002-07-23 | ビーエーエスエフ アクチェンゲゼルシャフト | アルキンジオールの製造方法 |
| JP2002356451A (ja) * | 2001-05-29 | 2002-12-13 | Maruzen Petrochem Co Ltd | アセチレンジオール化合物の製造方法 |
| US6956141B1 (en) | 1999-02-22 | 2005-10-18 | Basf Aktiengesellschaft | Method for preparing acetylene alcohols and their secondary products |
| EP1808426A1 (en) * | 2006-01-16 | 2007-07-18 | DSMIP Assets B.V. | Process for the preparation of alkynediols |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4628092A (en) * | 1985-06-21 | 1986-12-09 | Air Products And Chemicals, Inc. | Triethylenediamine containing acetylenic alcohols as flow aids |
| DE19635703A1 (de) * | 1996-09-03 | 1998-03-05 | Basf Ag | Verfahren zur Herstellung von Alkindiolen oder Gemischen von Alkindiolen mit Alkinmonoolen |
| DE102005014984A1 (de) | 2005-04-01 | 2006-10-05 | Franz Haimer Maschinenbau Kg | Induktionsspulen-Baueinheit |
-
1970
- 1970-02-25 DE DE19702008675 patent/DE2008675A1/de active Pending
-
1971
- 1971-02-23 CA CA106,100A patent/CA942749A/en not_active Expired
- 1971-02-23 CH CH258971A patent/CH554822A/xx not_active IP Right Cessation
- 1971-02-23 BE BE763306A patent/BE763306A/xx unknown
- 1971-02-24 FR FR7106228A patent/FR2078998A5/fr not_active Expired
- 1971-04-19 GB GB2255871A patent/GB1329815A/en not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4960959A (en) * | 1987-04-04 | 1990-10-02 | Huels Aktiengesellschaft | Process for the manufacture of alkynediols by reaction of ketones with acetylene |
| JP2002522516A (ja) * | 1998-08-17 | 2002-07-23 | ビーエーエスエフ アクチェンゲゼルシャフト | アルキンジオールの製造方法 |
| RU2221768C2 (ru) * | 1998-08-17 | 2004-01-20 | Басф Акциенгезельшафт | Способ получения алкиндиолов, возможно, содержащих алкинмоноспирты |
| US6956141B1 (en) | 1999-02-22 | 2005-10-18 | Basf Aktiengesellschaft | Method for preparing acetylene alcohols and their secondary products |
| JP2001002607A (ja) * | 1999-05-26 | 2001-01-09 | Basf Ag | アルキンジオールの製造方法 |
| CN1083414C (zh) * | 1999-08-25 | 2002-04-24 | 成都惟精防水材料研究所 | 2,5-二甲基-2,5-己二醇一步合成法 |
| JP2002356451A (ja) * | 2001-05-29 | 2002-12-13 | Maruzen Petrochem Co Ltd | アセチレンジオール化合物の製造方法 |
| EP1808426A1 (en) * | 2006-01-16 | 2007-07-18 | DSMIP Assets B.V. | Process for the preparation of alkynediols |
| WO2007080103A3 (en) * | 2006-01-16 | 2007-11-01 | Dsm Ip Assets Bv | Process for the preparation of alkynediols |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2008675A1 (de) | 1971-09-09 |
| CA942749A (en) | 1974-02-26 |
| CH554822A (de) | 1974-10-15 |
| FR2078998A5 (enExample) | 1971-11-05 |
| BE763306A (fr) | 1971-07-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |