GB1260798A - Method of improving the interfacial adhesion of inorganic fibre materials - Google Patents

Method of improving the interfacial adhesion of inorganic fibre materials

Info

Publication number
GB1260798A
GB1260798A GB31303/70A GB3130370A GB1260798A GB 1260798 A GB1260798 A GB 1260798A GB 31303/70 A GB31303/70 A GB 31303/70A GB 3130370 A GB3130370 A GB 3130370A GB 1260798 A GB1260798 A GB 1260798A
Authority
GB
United Kingdom
Prior art keywords
silane
dispersions
inorganic
fibre materials
resins
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB31303/70A
Inventor
Gottfried Wiedemann
Horst Frenzel
Margit Matzke
Ursula Renner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TECHNISCHES GLAS VEB K
Original Assignee
TECHNISCHES GLAS VEB K
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DD14118669A priority Critical patent/DD81191A3/xx
Priority to DE19702031592 priority patent/DE2031592A1/en
Application filed by TECHNISCHES GLAS VEB K filed Critical TECHNISCHES GLAS VEB K
Priority to GB31303/70A priority patent/GB1260798A/en
Priority to FR707025969A priority patent/FR2051736B1/fr
Publication of GB1260798A publication Critical patent/GB1260798A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
    • C03C25/10—Coating
    • C03C25/24—Coatings containing organic materials
    • C03C25/40—Organo-silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
    • C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
    • C08J5/08—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials glass fibres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C08K9/06—Ingredients treated with organic substances with silicon-containing compounds

Abstract

1,260,798. Laminates. VEB KOMBINAT TECHNISCHES GLAS ILMENAU. 29 June, 1970, No. 31303/70. Heading B5N. [Also in Division D1] Method for improving the interfacial adhesion of inorganic fibre materials, especially desized fabrics of glass fibre materials to resins, wherein inorganic fibre materials are treated with a solution of an epoxy silane and, for the production of composite materials, a resin specific coupling agent of the silane type, containing unsaturated radicals, is added to the resin. Vinyl or methacrylate silane is used as the silane in the case of the use of unsaturated polyester resins and epoxy-silane is used for epoxide or phenolic resins. The inorganic fibre materials may also be impregnated with a solution comprising an organo-silane, preferably containing unsaturated radicals, and a chromium salt of an organic and/or inorganic acid. To improve the wettability by the resin, the inorganic fibre materials are treated with coupling agents containing polymeric compounds and/or phenol derivatives and/or silicic acid compounds and/or inorganic pigments. It is possible to add, as polymeric compounds, water soluble and/or water dispersible polymers and as phenol derivatives dihydroxy-benzenes, and as silicic acid compounds aqueous dispersions of silicon dioxide and/or silicic acid ester dispersions and/or dispersions of condensed silicic acid esters, and as inorganic pigments titanium dioxide, calcium carbonate and antimony trioxide preferably in dispersed form. For the production of composite materials, the above treated inorganic fibre materials are impregnated with a resin either in pure form or modified with silane. Examples of polymeric compounds are polyvinyl pyrrolidone solutions, epoxide resin dispersions, dispersions of unsaturated polyester resins; examples of phenol derivatives are resorcinol, precondensates or condensates of resorcinol with formaldehyde as solutions or dispersions and examples of resins are thermosetting or thermoplastic resins and silicone resins or elastomers. The fabric of inorganic material is first desized, preferably thermally and then impregnated with mixtures of the described coupling agents and additives, whereupon it is dried and set at an elevated temperature.
GB31303/70A 1969-07-14 1970-06-29 Method of improving the interfacial adhesion of inorganic fibre materials Expired GB1260798A (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
DD14118669A DD81191A3 (en) 1969-07-14 1969-07-14
DE19702031592 DE2031592A1 (en) 1969-07-14 1970-06-26 Process for improving the interfacial adhesion for inorganic fiber materials, in particular desized flat structures made of glass fiber materials
GB31303/70A GB1260798A (en) 1969-07-14 1970-06-29 Method of improving the interfacial adhesion of inorganic fibre materials
FR707025969A FR2051736B1 (en) 1969-07-14 1970-07-15

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DD14118669A DD81191A3 (en) 1969-07-14 1969-07-14
GB31303/70A GB1260798A (en) 1969-07-14 1970-06-29 Method of improving the interfacial adhesion of inorganic fibre materials

Publications (1)

Publication Number Publication Date
GB1260798A true GB1260798A (en) 1972-01-19

Family

ID=25747258

Family Applications (1)

Application Number Title Priority Date Filing Date
GB31303/70A Expired GB1260798A (en) 1969-07-14 1970-06-29 Method of improving the interfacial adhesion of inorganic fibre materials

Country Status (4)

Country Link
DD (1) DD81191A3 (en)
DE (1) DE2031592A1 (en)
FR (1) FR2051736B1 (en)
GB (1) GB1260798A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001048073A1 (en) * 1999-12-28 2001-07-05 Dsm N.V. Reactive particles, curable composition comprising the same and cured products
CN103466964A (en) * 2013-09-10 2013-12-25 西安友基复合材料有限公司 Preparation method of wetting agent for E glass fishing rod gauze
CN107022119A (en) * 2017-05-15 2017-08-08 北京化工大学 A kind of preparation method of graphene/silicon dioxide/rubber composite
CN112941933A (en) * 2021-02-04 2021-06-11 郑州市娅丽达服饰有限公司 Fabric with visible and invisible patterns, garment designed and processed by fabric and processing method

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3603909A1 (en) * 1986-02-07 1987-08-13 Frenzelit Werke Gmbh & Co Kg Glass fibres having improved heat resistance, and process for the production thereof

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2931739A (en) * 1956-10-08 1960-04-05 Owens Corning Fiberglass Corp Plastics and laminates formed of glass fibers and epoxy resins
US2946701A (en) * 1957-11-12 1960-07-26 Dow Corning Method of treating glass with epoxysilanes and their epoxy-amine adducts, and the articles made thereby
NL243936A (en) * 1958-10-01 1900-01-01
US3217065A (en) * 1960-12-16 1965-11-09 Monsanto Co Laminated structures
FR1495136A (en) * 1966-09-23 1967-09-15 Owens Corning Fiberglass Corp Method and means for reinforcing elastomeric products with glass fibers
FR1356819A (en) * 1963-05-20 1964-03-27 B T R Ind Ltd Coating composition for glass fibers, its applications and resulting products
FR1460717A (en) * 1964-09-30 1966-03-04 Owens Corning Fiberglass Corp glass fiber reinforced elastomers
US3488310A (en) * 1967-02-24 1970-01-06 Owens Corning Fiberglass Corp Urea-melamine-formaldehyde resins
FR1527997A (en) * 1967-04-21 1968-06-07 Wimpfheimer & Bro A Composite and laminated glass and resin products

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001048073A1 (en) * 1999-12-28 2001-07-05 Dsm N.V. Reactive particles, curable composition comprising the same and cured products
US6686047B2 (en) 1999-12-28 2004-02-03 Dsm N.V. Reactive particles, curable composition comprising the same and cured products
CN103466964A (en) * 2013-09-10 2013-12-25 西安友基复合材料有限公司 Preparation method of wetting agent for E glass fishing rod gauze
CN103466964B (en) * 2013-09-10 2016-01-20 西安友基复合材料有限公司 The preparation method of E glass fishing rod cloth yarn treating compound
CN107022119A (en) * 2017-05-15 2017-08-08 北京化工大学 A kind of preparation method of graphene/silicon dioxide/rubber composite
CN112941933A (en) * 2021-02-04 2021-06-11 郑州市娅丽达服饰有限公司 Fabric with visible and invisible patterns, garment designed and processed by fabric and processing method
CN112941933B (en) * 2021-02-04 2023-04-11 郑州市娅丽达服饰有限公司 Fabric with visible and invisible patterns, garment designed and processed by fabric and processing method

Also Published As

Publication number Publication date
DE2031592A1 (en) 1971-03-25
FR2051736A1 (en) 1971-04-09
DD81191A3 (en) 1971-04-12
FR2051736B1 (en) 1973-05-25

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee