GB1197410A - A Process for the Continuous Production of Aliphatic Titanic Acid Esters - Google Patents
A Process for the Continuous Production of Aliphatic Titanic Acid EstersInfo
- Publication number
- GB1197410A GB1197410A GB50084/68A GB5008468A GB1197410A GB 1197410 A GB1197410 A GB 1197410A GB 50084/68 A GB50084/68 A GB 50084/68A GB 5008468 A GB5008468 A GB 5008468A GB 1197410 A GB1197410 A GB 1197410A
- Authority
- GB
- United Kingdom
- Prior art keywords
- aliphatic
- mixture
- reaction
- hydrohalide
- acid esters
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 Aliphatic Titanic Acid Esters Chemical class 0.000 title abstract 2
- 238000010924 continuous production Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 abstract 2
- 239000003085 diluting agent Substances 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- KNIUHBNRWZGIQQ-UHFFFAOYSA-N 7-diethoxyphosphinothioyloxy-4-methylchromen-2-one Chemical compound CC1=CC(=O)OC2=CC(OP(=S)(OCC)OCC)=CC=C21 KNIUHBNRWZGIQQ-UHFFFAOYSA-N 0.000 abstract 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 239000003701 inert diluent Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 1
- 239000003208 petroleum Substances 0.000 abstract 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/003—Compounds containing elements of Groups 4 or 14 of the Periodic Table without C-Metal linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,197,410. Aliphatic titanates. FARBENFABRIKEN BAYER A.G. 22 Oct., 1968 [18 Nov., 1967], No. 50084/68. Heading C2C. A continuous process for producing aliphatic titanate esters comprises continuously mixing a titanium tetrahalide and an aliphatic alcohol, optionally in the presence of an inert diluent, dissipating the heat generated during mixing, passing the mixture through one or more reaction zones under anhydrous conditions at a temperature of not more than 220‹ C., into which zone(s) a nitrogen-containing base which forms a hydrohalide insoluble in the reaction mixture is introduced continuously or in stages in such a quantity that on completion of the reaction the mixture has a pH of about 8, and separating the resulting ester from the hydrohalide of the base and from the diluent if used. Suitable alcohols include straight- or branched chain primary and secondary alkanols with 2-9 carbons in the straight chain; suitable bases include gaseous or liquid NH 3 and pyridine; and suitable diluents include petroleum ether, cyclohexane and benzene.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0054073 | 1967-11-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1197410A true GB1197410A (en) | 1970-07-01 |
Family
ID=7106814
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB50084/68A Expired GB1197410A (en) | 1967-11-18 | 1968-10-22 | A Process for the Continuous Production of Aliphatic Titanic Acid Esters |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE724045A (en) |
| DE (1) | DE1668042A1 (en) |
| FR (1) | FR1592031A (en) |
| GB (1) | GB1197410A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322219A (en) * | 2022-08-22 | 2022-11-11 | 青岛科技大学 | Continuous production system and method for isopropyl titanate |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3739577C1 (en) * | 1987-11-23 | 1988-10-13 | Huels Troisdorf | Process for the continuous production of titanium orthoesters |
-
1967
- 1967-11-18 DE DE19671668042 patent/DE1668042A1/en active Pending
-
1968
- 1968-10-22 GB GB50084/68A patent/GB1197410A/en not_active Expired
- 1968-11-18 FR FR1592031D patent/FR1592031A/fr not_active Expired
- 1968-11-18 BE BE724045D patent/BE724045A/xx unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115322219A (en) * | 2022-08-22 | 2022-11-11 | 青岛科技大学 | Continuous production system and method for isopropyl titanate |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1668042A1 (en) | 1971-06-09 |
| FR1592031A (en) | 1970-05-04 |
| BE724045A (en) | 1969-05-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES2088973T3 (en) | IMPROVED 6-ESTER CHLORINATION OF SACAROSA. | |
| GB1395926A (en) | Process for the production of isoprene by the chlorination/ dehydrochlorination of 2-methylbutene-2 | |
| GB1197410A (en) | A Process for the Continuous Production of Aliphatic Titanic Acid Esters | |
| GB1151059A (en) | Method of Producing Hexabromocyclododecane. | |
| ATE7881T1 (en) | PROCESS FOR GENERATING CHLORINE DIOXIDE. | |
| GB1301819A (en) | ||
| GB1155023A (en) | Azetidino-Thiazolidinemethane Carboxylic Acid Derivatives and process for their Manufacture | |
| GB1410474A (en) | Distillation of halogen containing aromatic compounds | |
| GB915804A (en) | Process for the production of basically substituted carboxylic acid amides | |
| GB1346013A (en) | Process and apparatus for chlorinating methylchlorosilanes | |
| GB1190303A (en) | Process for the production of neopentylglycol-carboxylic acid-carbonic acid mixed esters | |
| US2421233A (en) | Ureido acid esters and method of making the same | |
| GB1335363A (en) | Substituted benzamidoacetohydroxamic acids | |
| IE32440L (en) | Penicillin esters | |
| GB1442920A (en) | Process for the manufacutre of 6-d- - x-aminophenylacetamido- pencillanic acid | |
| GB1249613A (en) | PROCESS OF PREPARING gamma-CYANOBUTYRALDIMINES | |
| ES465382A1 (en) | Manufacture of a titanium-containing component for catalysts of the Ziegler-Natta type | |
| GB1340130A (en) | Continuous process for producing dialkyl phosphorochlorido thionates | |
| GB1181775A (en) | A Process for the Production of N-Cyclohexyl Amidosulphonic Acid | |
| GB1396489A (en) | Process for the dehydration of maleic acid | |
| GB1257932A (en) | ||
| GB1156443A (en) | Method of preparing beta-Ionone | |
| GB1182557A (en) | Alkoxycarbonylamino Propanes and Process for Preparing Them | |
| GB1328035A (en) | Preparation of aromatic carboxylic acid isomeric sulphonates | |
| GB1210827A (en) | A process for preparing substituted alkylmercaptophenols |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |