GB1139507A - Preparation of peracids - Google Patents
Preparation of peracidsInfo
- Publication number
- GB1139507A GB1139507A GB1644665A GB1644665A GB1139507A GB 1139507 A GB1139507 A GB 1139507A GB 1644665 A GB1644665 A GB 1644665A GB 1644665 A GB1644665 A GB 1644665A GB 1139507 A GB1139507 A GB 1139507A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrogen peroxide
- liquid
- mono
- peracids
- miscible
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C409/00—Peroxy compounds
- C07C409/24—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids
- C07C409/30—Peroxy compounds the —O—O— group being bound between a >C=O group and hydrogen, i.e. peroxy acids a >C=O group being bound to a carbon atom of a six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrrole Compounds (AREA)
Abstract
1,139,507. Peracids. DISTILLERS CO. Ltd. 9 May, 1966 [20 April, 1965], No. 16446/65. Heading C2C. Mono-percarboxylic acids are prepared by reacting hydrogen peroxide with the anhydride of a dicarboxylic acid in the presence of a liquid which is miscible with hydrogen peroxide and which has a dielectric constant greater than 20, provided that said liquid does not comprise solely water or sulphuric acid. It is preferred to use substantially inert organic liquids, e.g. N,N-dialkyl formamides, N-alkyl pyrrolidones and formic acid. The reaction mixture may also include a high dielectric liquid which is not miscible with hydrogen peroxide, e.g., nitromethane and nitrobenzene, or a low dielectric liquid, e.g. chloroform. It is preferred to use aqueous hydrogen peroxide having a concentration greater than 80% w./w. and to effect the reaction at a temperature below 50‹ C. Examples relate to the preparation of mono-peracids from maleic, phthalic and succinic anhydrides. The mono-peracid may be used to oxidize cyclohexanone to caprolactone.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1644665A GB1139507A (en) | 1965-04-20 | 1965-04-20 | Preparation of peracids |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1644665A GB1139507A (en) | 1965-04-20 | 1965-04-20 | Preparation of peracids |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1139507A true GB1139507A (en) | 1969-01-08 |
Family
ID=10077469
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1644665A Expired GB1139507A (en) | 1965-04-20 | 1965-04-20 | Preparation of peracids |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1139507A (en) |
-
1965
- 1965-04-20 GB GB1644665A patent/GB1139507A/en not_active Expired
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