GB1077648A - A process for the preparation of 5h-dibenzo-(b,f) azepine - Google Patents
A process for the preparation of 5h-dibenzo-(b,f) azepineInfo
- Publication number
- GB1077648A GB1077648A GB20939/66A GB2093966A GB1077648A GB 1077648 A GB1077648 A GB 1077648A GB 20939/66 A GB20939/66 A GB 20939/66A GB 2093966 A GB2093966 A GB 2093966A GB 1077648 A GB1077648 A GB 1077648A
- Authority
- GB
- United Kingdom
- Prior art keywords
- azepine
- dibenzo
- preparation
- iminostilbene
- iminodibenzyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- LCGTWRLJTMHIQZ-UHFFFAOYSA-N 5H-dibenzo[b,f]azepine Chemical compound C1=CC2=CC=CC=C2NC2=CC=CC=C21 LCGTWRLJTMHIQZ-UHFFFAOYSA-N 0.000 title 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- MIMHGLQRWAZOSE-UHFFFAOYSA-N 11H-benzo[b][1]benzazepine 6-(2-phenylethenyl)cyclohexa-2,4-dien-1-imine Chemical compound N=C1C=CC=CC1C=CC1=CC=CC=C1.C1=CC2=CC=CC=C2NC2=CC=CC=C21 MIMHGLQRWAZOSE-UHFFFAOYSA-N 0.000 abstract 1
- ZSMRRZONCYIFNB-UHFFFAOYSA-N 6,11-dihydro-5h-benzo[b][1]benzazepine Chemical compound C1CC2=CC=CC=C2NC2=CC=CC=C12 ZSMRRZONCYIFNB-UHFFFAOYSA-N 0.000 abstract 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 239000010953 base metal Substances 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 239000011651 chromium Substances 0.000 abstract 1
- 229910017052 cobalt Inorganic materials 0.000 abstract 1
- 239000010941 cobalt Substances 0.000 abstract 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- 229910052750 molybdenum Inorganic materials 0.000 abstract 1
- 239000011733 molybdenum Substances 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 abstract 1
- 229910052721 tungsten Inorganic materials 0.000 abstract 1
- 239000010937 tungsten Substances 0.000 abstract 1
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/14—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom condensed with carbocyclic rings or ring systems
- C07D223/18—Dibenzazepines; Hydrogenated dibenzazepines
- C07D223/22—Dibenz [b, f] azepines; Hydrogenated dibenz [b, f] azepines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DED0047262 | 1965-05-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1077648A true GB1077648A (en) | 1967-08-02 |
Family
ID=7050310
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB20939/66A Expired GB1077648A (en) | 1965-05-14 | 1966-05-11 | A process for the preparation of 5h-dibenzo-(b,f) azepine |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US3531466A (de) |
| CH (1) | CH461499A (de) |
| DE (1) | DE1545736A1 (de) |
| GB (1) | GB1077648A (de) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0570336A2 (de) * | 1992-05-13 | 1993-11-18 | Ciba-Geigy Ag | Neues Hochtemperatur-Dehydrierungsverfahren zur Herstellung von 5H-Dibene b,f Azepin |
| AT409628B (de) * | 2000-04-10 | 2002-09-25 | Dsm Fine Chem Austria Gmbh | Reinigungsverfahren zur herstellung von hochreinem 5h-dibenzo-(b,f)-azepin |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT401772B (de) * | 1994-12-27 | 1996-11-25 | Chemie Linz Gmbh | Verfahren zur reinigung von 5h-dibenzo-(b,f)-azepin |
| CN103275006B (zh) * | 2013-05-29 | 2014-12-03 | 陈建国 | 一种合成卡马西平中间体亚氨基芪的方法 |
| CN111217751B (zh) * | 2020-03-16 | 2021-06-08 | 浙江华洲药业有限公司 | 一种亚氨基芪的合成方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2257800A (en) * | 1940-04-12 | 1941-10-07 | Du Pont | Alloy-skeleton catalyst |
| US2341995A (en) * | 1941-01-06 | 1944-02-15 | Herman B Kipper | Process for the dehydrogenation of liquid and gaseous petroleum hydrocarbons |
| US2488560A (en) * | 1946-11-25 | 1949-11-22 | Reiltlinger Otto | Structure of contact masses |
| US2599978A (en) * | 1949-04-15 | 1952-06-10 | Ohio Commw Eng Co | Process of plating carrier particles with a catalytic metal |
| CH442319A (de) * | 1964-09-23 | 1967-08-31 | Geigy Ag J R | Verfahren zur technisch wirtschaftlichen Herstellung von 5H-Dibenz(b,f)azepinen |
-
1965
- 1965-05-14 DE DE19651545736 patent/DE1545736A1/de not_active Withdrawn
-
1966
- 1966-03-17 CH CH385966A patent/CH461499A/de unknown
- 1966-05-04 US US547424A patent/US3531466A/en not_active Expired - Lifetime
- 1966-05-11 GB GB20939/66A patent/GB1077648A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0570336A2 (de) * | 1992-05-13 | 1993-11-18 | Ciba-Geigy Ag | Neues Hochtemperatur-Dehydrierungsverfahren zur Herstellung von 5H-Dibene b,f Azepin |
| EP0570336A3 (de) * | 1992-05-13 | 1994-04-13 | Ciba Geigy Ag | |
| AU663580B2 (en) * | 1992-05-13 | 1995-10-12 | Novartis Ag | Preparation of iminostilbene by high-temperature dehydrogenation |
| AT409628B (de) * | 2000-04-10 | 2002-09-25 | Dsm Fine Chem Austria Gmbh | Reinigungsverfahren zur herstellung von hochreinem 5h-dibenzo-(b,f)-azepin |
Also Published As
| Publication number | Publication date |
|---|---|
| CH461499A (de) | 1968-08-31 |
| US3531466A (en) | 1970-09-29 |
| DE1545736A1 (de) | 1970-07-16 |
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