GB1040728A - Improvements in and relating to cellulosic textile materials - Google Patents

Improvements in and relating to cellulosic textile materials

Info

Publication number
GB1040728A
GB1040728A GB18511/63A GB1851163A GB1040728A GB 1040728 A GB1040728 A GB 1040728A GB 18511/63 A GB18511/63 A GB 18511/63A GB 1851163 A GB1851163 A GB 1851163A GB 1040728 A GB1040728 A GB 1040728A
Authority
GB
United Kingdom
Prior art keywords
liquid medium
dioxane
dimethylol
sodium
ethyl
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB18511/63A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Union Carbide Corp
Original Assignee
Union Carbide Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Union Carbide Corp filed Critical Union Carbide Corp
Publication of GB1040728A publication Critical patent/GB1040728A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D407/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen atoms as the only ring hetero atoms, not provided for by group C07D405/00
    • C07D407/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen atoms as the only ring hetero atoms, not provided for by group C07D405/00 containing two hetero rings
    • C07D407/10—Heterocyclic compounds containing two or more hetero rings, at least one ring having oxygen atoms as the only ring hetero atoms, not provided for by group C07D405/00 containing two hetero rings linked by a carbon chain containing aromatic rings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/11—Compounds containing epoxy groups or precursors thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/55—Epoxy resins
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S8/00—Bleaching and dyeing; fluid treatment and chemical modification of textiles and fibers
    • Y10S8/08—Oxirane

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

2,3 - Bis(2,3 - epoxypropoxy) - 1,4 - dioxane is produced by reacting together glyoxal, ethylene glycol and allyl alcohol in the presence of sulphuric acid and treating the 2,3-diallyloxy-1,4-dioxane thus produced with a solution of peracetic acid in ethyl acetate.ALSO:Cellulosic textile materials, e.g. cotton, linen and viscose rayon, are crease proofed and shrink proofed by impregnating them with a liquid medium containing a diepoxy-dioxane having the formula <FORM:1040728/D1-D2/1> in which R is a hydrocarbon radical containing 1-3 carbon atoms and R1 is a hydrogen atom or methyl radical and then drying and heating. The liquid medium is preferably an aqueous medium which may also contain emulsifying agents and water-miscible organic solvents, e.g. methyl, hydroxy ethyl or carboxymethyl cellulose, sodium alginate, polyvinyl alcohol, polyethylene oxide, toluene, xylene, ethyl, butyl or isopropyl alcohol, acetone or an ester. The liquid medium may contain a catalyst, e.g. phosphoric, hydrochloric, boric, alkane sulphonic, perchloric, persulphuric, p-toluene sulphonic, citric, acetic, butyric, caproic, phthalic, tartaric, oxalic, succinic, fumaric, glutaconic, malonic acetoacetic and naphthalicacids acetic, phthalic and succinic acid anhydrides, magnesium, tin, cadmium, sodium or zinc fluoborate, boron trifluoride etherate, stannic, aluminium or magnesium chloride, sodium, zinc or aluminium sulphate and the hydrochlorides of aniline, n-propyl-amine, di-n-butylamine, dibenzylamine, triethylamine, alpha-phenylethylamine, beta-amino anthraquinone, 1, 3-diaminoanthraquinone, piperidine, pyridine, quinoline, pyrrole, morpholine, guanidine, 2-amino-2-methylpropanol and isobutanolamine. Formaldehyde, melamine-formaldehyde resins, 1, 3-dimethylol-5-ethyltetra-hydro-s-triazin-2(1H)-one, mono-or dimethylol urea, mono- or dimethylol ethylene urea, methylated methylol ureas, plasticizers, natural resins or softening agents may also be included in the liquid medium. After impregnation the textile material may be dried at a temperature of 95 DEG -175 DEG F for 5-1 minutes and then cured by heating at a temperature of 240 DEG -400 DEG F for between 15 seconds and 5 minutes.
GB18511/63A 1962-05-21 1963-05-10 Improvements in and relating to cellulosic textile materials Expired GB1040728A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US196476A US3135579A (en) 1962-05-21 1962-05-21 Treatment of textile fabrics with diepoxydioxanes

Publications (1)

Publication Number Publication Date
GB1040728A true GB1040728A (en) 1966-09-01

Family

ID=22725564

Family Applications (1)

Application Number Title Priority Date Filing Date
GB18511/63A Expired GB1040728A (en) 1962-05-21 1963-05-10 Improvements in and relating to cellulosic textile materials

Country Status (7)

Country Link
US (1) US3135579A (en)
BE (1) BE632560A (en)
CH (1) CH390208A (en)
DE (1) DE1219438B (en)
FR (1) FR1357395A (en)
GB (1) GB1040728A (en)
NL (1) NL293047A (en)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE587322A (en) * 1959-02-06
AT218471B (en) * 1959-06-22 1961-12-11 Ciba Geigy Process for finishing, in particular for making crease-free and shrink-proof, hydroxylated fiber materials
US3054803A (en) * 1959-06-23 1962-09-18 Celanese Corp 2-alkenyl-5-lower alkyl-5-hydroxy-methyl-meta dioxanes
US3026216A (en) * 1959-10-05 1962-03-20 Union Carbide Corp Treatment of textile fabrics with methylglycidyl ethers
US3067175A (en) * 1960-03-07 1962-12-04 Shell Oil Co Polyglycidaldehyde

Also Published As

Publication number Publication date
CH633863A4 (en) 1964-12-31
BE632560A (en)
US3135579A (en) 1964-06-02
FR1357395A (en) 1964-04-03
DE1219438B (en) 1966-06-23
NL293047A (en)
CH390208A (en) 1965-07-30

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