GB1040139A - A method of partially nitrating polyhydric alcohols - Google Patents
A method of partially nitrating polyhydric alcoholsInfo
- Publication number
- GB1040139A GB1040139A GB2152563A GB2152563A GB1040139A GB 1040139 A GB1040139 A GB 1040139A GB 2152563 A GB2152563 A GB 2152563A GB 2152563 A GB2152563 A GB 2152563A GB 1040139 A GB1040139 A GB 1040139A
- Authority
- GB
- United Kingdom
- Prior art keywords
- pentaerythritol
- dinitrate
- alcohol
- methylene chloride
- trimethylol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000000802 nitrating effect Effects 0.000 title abstract 2
- 150000005846 sugar alcohols Polymers 0.000 title 1
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 abstract 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 3
- 229910017604 nitric acid Inorganic materials 0.000 abstract 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 abstract 2
- 150000002148 esters Chemical class 0.000 abstract 2
- YHRUOJUYPBUZOS-UHFFFAOYSA-N 1,3-dichloropropane Chemical compound ClCCCCl YHRUOJUYPBUZOS-UHFFFAOYSA-N 0.000 abstract 1
- YXCDZXGJZDGMEP-UHFFFAOYSA-N 4-hydroxy-3,3-bis(hydroxymethyl)butan-2-one Chemical compound CC(=O)C(CO)(CO)CO YXCDZXGJZDGMEP-UHFFFAOYSA-N 0.000 abstract 1
- KHAIISDEIXPDCH-UHFFFAOYSA-N 4-hydroxy-3,3-bis(hydroxymethyl)butan-2-one nitric acid Chemical compound [N+](=O)(O)[O-].[N+](=O)(O)[O-].C(O)C(C(=O)C)(CO)CO KHAIISDEIXPDCH-UHFFFAOYSA-N 0.000 abstract 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical group CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 1
- 229930194542 Keto Natural products 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 abstract 1
- FZJWITMDCJLVSZ-UHFFFAOYSA-N [2-(hydroxymethyl)-3-nitrooxy-2-(nitrooxymethyl)propyl] acetate Chemical compound [N+](=O)([O-])OCC(COC(C)=O)(CO[N+](=O)[O-])CO FZJWITMDCJLVSZ-UHFFFAOYSA-N 0.000 abstract 1
- OORDEDRRTSWSRC-UHFFFAOYSA-N [3-hydroxy-2,2-bis(hydroxymethyl)propyl] acetate Chemical compound CC(=O)OCC(CO)(CO)CO OORDEDRRTSWSRC-UHFFFAOYSA-N 0.000 abstract 1
- NNZJRQUVPNCRHW-UHFFFAOYSA-N [N+](=O)(O)[O-].[N+](=O)(O)[O-].C(O)C(CC)(CO)CO Chemical compound [N+](=O)(O)[O-].[N+](=O)(O)[O-].C(O)C(CC)(CO)CO NNZJRQUVPNCRHW-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 125000000468 ketone group Chemical group 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 1
- BRBAEHHXGZRCBK-UHFFFAOYSA-N pentrinitrol Chemical compound [O-][N+](=O)OCC(CO)(CO[N+]([O-])=O)CO[N+]([O-])=O BRBAEHHXGZRCBK-UHFFFAOYSA-N 0.000 abstract 1
- 229950006286 pentrinitrol Drugs 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C203/00—Esters of nitric or nitrous acid
- C07C203/02—Esters of nitric acid
- C07C203/04—Esters of nitric acid having nitrate groups bound to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/02—Preparation of esters of nitric acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEN21677A DE1160427B (de) | 1962-06-07 | 1962-06-07 | Verfahren zur Herstellung von Salpetersaeureestern mehrwertiger Alkohole |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1040139A true GB1040139A (en) | 1966-08-24 |
Family
ID=7341824
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2152563A Expired GB1040139A (en) | 1962-06-07 | 1963-05-29 | A method of partially nitrating polyhydric alcohols |
Country Status (4)
| Country | Link |
|---|---|
| BE (1) | BE632627A (enrdf_load_stackoverflow) |
| CH (1) | CH420093A (enrdf_load_stackoverflow) |
| DE (1) | DE1160427B (enrdf_load_stackoverflow) |
| GB (1) | GB1040139A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999067430A3 (de) * | 1998-06-24 | 2000-05-04 | Isis Pharma Gmbh | Analytische substrate und antioxidative mittel |
| EP1136468A3 (en) * | 2000-03-23 | 2001-11-14 | Cordant Technologies, Inc. | Method of synthesizing diglycerol tetranitrate, and solid rocket motor propellant containing the same |
| WO2004043898A1 (en) * | 2002-11-14 | 2004-05-27 | Dipharma S.P.A. | A process for the mononitration of alkanediols |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH540878A (de) * | 1970-06-30 | 1973-10-15 | Council Scient Ind Res | Verfahren zur Herstellung von aliphatischen Nitraten |
| US4352699A (en) * | 1981-06-01 | 1982-10-05 | Hercules Incorporated | Co-nitrating trimetholethane and diethylene glycol |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2465984A (en) * | 1946-05-21 | 1949-03-29 | Union Oil Co | Production of cycloalkyl nitrites |
| US2545538A (en) * | 1947-12-11 | 1951-03-20 | Du Pont | Process for manufacture of nitric esters of normally solid primary alcohols |
| NL98269C (enrdf_load_stackoverflow) | 1956-02-24 |
-
0
- BE BE632627D patent/BE632627A/xx unknown
-
1962
- 1962-06-07 DE DEN21677A patent/DE1160427B/de active Pending
-
1963
- 1963-05-07 CH CH572963A patent/CH420093A/de unknown
- 1963-05-29 GB GB2152563A patent/GB1040139A/en not_active Expired
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999067430A3 (de) * | 1998-06-24 | 2000-05-04 | Isis Pharma Gmbh | Analytische substrate und antioxidative mittel |
| EP1136468A3 (en) * | 2000-03-23 | 2001-11-14 | Cordant Technologies, Inc. | Method of synthesizing diglycerol tetranitrate, and solid rocket motor propellant containing the same |
| WO2004043898A1 (en) * | 2002-11-14 | 2004-05-27 | Dipharma S.P.A. | A process for the mononitration of alkanediols |
| JP2006506418A (ja) * | 2002-11-14 | 2006-02-23 | ディファルマ・ソシエタ・ペル・アチオニ | アルカンジオールのモノニトロ化方法 |
| US7335789B2 (en) | 2002-11-14 | 2008-02-26 | Dipharma S.P.A. | Process for the mononitration of alkanediols |
| US7851649B2 (en) | 2002-11-14 | 2010-12-14 | Dipharma S.P.A. | Process for the mononitration of alkanediols |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1160427B (de) | 1964-01-02 |
| BE632627A (enrdf_load_stackoverflow) | |
| CH420093A (de) | 1966-09-15 |
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