GB1030600A - The liquefaction of gases with low boiling points - Google Patents

The liquefaction of gases with low boiling points

Info

Publication number
GB1030600A
GB1030600A GB17294/65A GB1729465A GB1030600A GB 1030600 A GB1030600 A GB 1030600A GB 17294/65 A GB17294/65 A GB 17294/65A GB 1729465 A GB1729465 A GB 1729465A GB 1030600 A GB1030600 A GB 1030600A
Authority
GB
United Kingdom
Prior art keywords
feed gas
exchanger
compressor
gas
throttled
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB17294/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sulzer AG
Original Assignee
Sulzer AG
Gebrueder Sulzer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sulzer AG, Gebrueder Sulzer AG filed Critical Sulzer AG
Publication of GB1030600A publication Critical patent/GB1030600A/en
Expired legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/02—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process
    • F25J1/0221—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using the cold stored in an external cryogenic component in an open refrigeration loop
    • F25J1/0224—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using the cold stored in an external cryogenic component in an open refrigeration loop in combination with an internal quasi-closed refrigeration loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/0002—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the fluid to be liquefied
    • F25J1/0005—Light or noble gases
    • F25J1/0007—Helium
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration"
    • F25J1/0035—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by gas expansion with extraction of work
    • F25J1/0037—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by gas expansion with extraction of work of a return stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration"
    • F25J1/004—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by flash gas recovery
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration"
    • F25J1/0045—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by vaporising a liquid return stream
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/02—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process
    • F25J1/0201—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using only internal refrigeration means, i.e. without external refrigeration
    • F25J1/0202—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using only internal refrigeration means, i.e. without external refrigeration in a quasi-closed internal refrigeration loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00—Processes characterised by the type or other details of the feed stream
    • F25J2210/42—Nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F25J2270/06—Internal refrigeration with work-producing gas expansion loop with multiple gas expansion loops

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

1,030,600. Gas liquefaction process; refrigerating. SULZER BROS. Ltd. April 23, 1965 [April 29, 1964], No. 17294/65. Headings F4H and F4P. Liquefaction of an overperfect gas, e.g. helium, is effected by cooling compressed feed gas at about 18 atmospheres pressure in heat exchangers 4 to 7, 10 (Fig. 1, not shown), to below the inversion temperature, throttling at a valve 11 to an intermediate pressure of about 3 atmospheres without condensation, dividing the flow into a first portion which is warmed in exchanger 10 and is subsequently warmed to ambient temperature in exchangers 4 to 7 and fed to the inlet of a compressor 12; the second portion of throttled feed gas being further cooled in an exchanger 16 and throttled at a valve 17 into a liquid helium receiver 18 from which product liquid helium is withdrawn and vapour is returned through the exchangers to the compressor 12. Gas leaving the compressor 12 is cooled in exchanger 4, expanded in a turbine 14 and after being cooled in exchanger 6 is joined by said first portion of throttled feed gas and expanded in a turbine 15 and added to vapour from receiver 18 and warmed in exchangers 4 to 7 before being returned to the compressor 12. Make-up helium is introduced through a duct 3 and condensable impurities are absorbed at 8, 9. In a modification the turbines are dispensed with and cold requirements are met by cooling the feed gas using an external source of liquid nitrogen. In a further modification, a portion of feed gas is expanded in turbines 48, 49, (Fig. 5, not shown), and added to said first portion of throttled feed gas.
GB17294/65A 1964-04-29 1965-04-23 The liquefaction of gases with low boiling points Expired GB1030600A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH562864A CH411957A (en) 1964-04-29 1964-04-29 Process for liquefying a low-boiling gas, in particular helium

Publications (1)

Publication Number Publication Date
GB1030600A true GB1030600A (en) 1966-05-25

Family

ID=4296774

Family Applications (1)

Application Number Title Priority Date Filing Date
GB17294/65A Expired GB1030600A (en) 1964-04-29 1965-04-23 The liquefaction of gases with low boiling points

Country Status (6)

Country Link
US (1) US3389565A (en)
CH (1) CH411957A (en)
DE (1) DE1259914B (en)
FR (1) FR1428851A (en)
GB (1) GB1030600A (en)
NL (2) NL6406768A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6141973A (en) * 1998-09-15 2000-11-07 Yukon Pacific Corporation Apparatus and process for cooling gas flow in a pressurized pipeline

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3677019A (en) * 1969-08-01 1972-07-18 Union Carbide Corp Gas liquefaction process and apparatus
DE2009401A1 (en) * 1970-02-27 1971-09-09 Linde Ag, 6200 Wiesbaden Process for liquefying low-boiling gases
GB1358169A (en) * 1970-10-19 1974-06-26 Cryogenic Technology Inc Method and apparatus for liquefying helium by isentropic expansion
NL7311471A (en) * 1973-08-21 1975-02-25 Philips Nv DEVICE FOR LIQUIDIZATION OF VERY LOW TEMPERATURE CONDENSING GASES.
US3992167A (en) * 1975-04-02 1976-11-16 Union Carbide Corporation Low temperature refrigeration process for helium or hydrogen mixtures using mixed refrigerant
US4195979A (en) * 1978-05-12 1980-04-01 Phillips Petroleum Company Liquefaction of high pressure gas
US4192661A (en) * 1978-06-01 1980-03-11 Helix Technology Corporation Adsorbing impurities from cryogenic fluid make-up prior to admixing with feed
US4701200A (en) * 1986-09-24 1987-10-20 Union Carbide Corporation Process to produce helium gas
US4701201A (en) * 1986-09-24 1987-10-20 Union Carbide Corporation Process to produce cold helium gas for liquefaction
US5836173A (en) * 1997-05-01 1998-11-17 Praxair Technology, Inc. System for producing cryogenic liquid
FR2775518B1 (en) * 1998-03-02 2000-05-05 Air Liquide PROCESS AND INSTALLATION FOR REFRIGERATING PRODUCTION FROM A THERMAL CYCLE OF A FLUID WITH LOW BOILING POINT
ES2582941T3 (en) * 2004-11-15 2016-09-16 Mayekawa Mfg. Co., Ltd. Method and device for liquefaction and cryogenic refrigeration
US7278280B1 (en) * 2005-03-10 2007-10-09 Jefferson Science Associates, Llc Helium process cycle
US7409834B1 (en) * 2005-03-10 2008-08-12 Jefferson Science Associates Llc Helium process cycle
DE102007005098A1 (en) * 2007-02-01 2008-08-07 Linde Ag Method for operating a refrigeration cycle
DE102011013345A1 (en) * 2011-03-08 2012-09-13 Linde Aktiengesellschaft refrigeration plant
DE102011112911A1 (en) * 2011-09-08 2013-03-14 Linde Aktiengesellschaft refrigeration plant
FR3000541B1 (en) * 2013-01-03 2015-01-23 Air Liquide REFRIGERATION AND / OR LIQUEFACTION DEVICE AND CORRESPONDING METHOD
CN104792113B (en) * 2014-01-22 2018-09-28 北京中科富海低温科技有限公司 Helium liquefier and its control method
FR3057941B1 (en) * 2016-10-20 2020-02-28 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude DEVICE AND METHOD FOR REFRIGERATION AND / OR LIQUEFACTION OF A CRYOGENIC FLUID
CN109764637B (en) * 2018-12-28 2020-09-25 中国科学院理化技术研究所 Helium liquefier flow device

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2895303A (en) * 1956-05-17 1959-07-21 Little Inc A Purification of low-boiling gases
US2957318A (en) * 1956-06-13 1960-10-25 Liquefreeze Company Inc Control for refrigerating system
DE1036282B (en) * 1956-08-17 1958-08-14 Sulzer Ag Cooling system
US3095274A (en) * 1958-07-01 1963-06-25 Air Prod & Chem Hydrogen liquefaction and conversion systems
US3094390A (en) * 1958-07-09 1963-06-18 Air Prod & Chem Production and storage of converted hydrogen
US3182461A (en) * 1961-09-19 1965-05-11 Hydrocarbon Research Inc Natural gas liquefaction and separation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6141973A (en) * 1998-09-15 2000-11-07 Yukon Pacific Corporation Apparatus and process for cooling gas flow in a pressurized pipeline

Also Published As

Publication number Publication date
NL125897C (en)
NL6406768A (en) 1965-11-01
FR1428851A (en) 1966-02-18
DE1259914B (en) 1968-02-01
CH411957A (en) 1966-04-30
US3389565A (en) 1968-06-25

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