GB1008467A - Production of fluorubin - Google Patents
Production of fluorubinInfo
- Publication number
- GB1008467A GB1008467A GB45580/61A GB4558061A GB1008467A GB 1008467 A GB1008467 A GB 1008467A GB 45580/61 A GB45580/61 A GB 45580/61A GB 4558061 A GB4558061 A GB 4558061A GB 1008467 A GB1008467 A GB 1008467A
- Authority
- GB
- United Kingdom
- Prior art keywords
- quinoxaline
- amino
- diaminoquinoxaline
- chloro
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KJCRNHQXMXUTEB-UHFFFAOYSA-N 69637-93-0 Chemical compound C1=CC=C2N=C(N=C3NC=4C(=CC=CC=4)NC3=N3)C3=NC2=C1 KJCRNHQXMXUTEB-UHFFFAOYSA-N 0.000 title abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 4
- NOFJFBHOKPHILH-UHFFFAOYSA-N 3-chloroquinoxalin-2-amine Chemical compound C1=CC=C2N=C(Cl)C(N)=NC2=C1 NOFJFBHOKPHILH-UHFFFAOYSA-N 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- IQCTWJDIPCKELJ-UHFFFAOYSA-N 3-N-(3-aminoquinoxalin-2-yl)quinoxaline-2,3-diamine Chemical compound NC=1C(=NC2=CC=CC=C2N1)NC1=NC2=CC=CC=C2N=C1N IQCTWJDIPCKELJ-UHFFFAOYSA-N 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000000020 Nitrocellulose Substances 0.000 abstract 2
- 125000003118 aryl group Chemical group 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 229920001220 nitrocellulos Polymers 0.000 abstract 2
- -1 2 - aminoquinoxalin - 3 - yl Chemical group 0.000 abstract 1
- ZNQVEEAIQZEUHB-UHFFFAOYSA-N 2-ethoxyethanol Chemical compound CCOCCO ZNQVEEAIQZEUHB-UHFFFAOYSA-N 0.000 abstract 1
- BPRUUXRKBDUYJY-UHFFFAOYSA-N 3-chloro-7-methylquinoxalin-2-amine Chemical compound N1=C(Cl)C(N)=NC2=CC(C)=CC=C21 BPRUUXRKBDUYJY-UHFFFAOYSA-N 0.000 abstract 1
- 239000001640 5-methylquinoxaline Substances 0.000 abstract 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 abstract 1
- FJWGYAHXMCUOOM-QHOUIDNNSA-N [(2s,3r,4s,5r,6r)-2-[(2r,3r,4s,5r,6s)-4,5-dinitrooxy-2-(nitrooxymethyl)-6-[(2r,3r,4s,5r,6s)-4,5,6-trinitrooxy-2-(nitrooxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-3,5-dinitrooxy-6-(nitrooxymethyl)oxan-4-yl] nitrate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O)O[C@H]1[C@@H]([C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@@H](CO[N+]([O-])=O)O1)O[N+]([O-])=O)CO[N+](=O)[O-])[C@@H]1[C@@H](CO[N+]([O-])=O)O[C@@H](O[N+]([O-])=O)[C@H](O[N+]([O-])=O)[C@H]1O[N+]([O-])=O FJWGYAHXMCUOOM-QHOUIDNNSA-N 0.000 abstract 1
- 239000003377 acid catalyst Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 125000003545 alkoxy group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 125000003277 amino group Chemical group 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 150000001555 benzenes Chemical class 0.000 abstract 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
- 229910052794 bromium Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Chemical group 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 235000019441 ethanol Nutrition 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 239000004922 lacquer Substances 0.000 abstract 1
- 238000003801 milling Methods 0.000 abstract 1
- 239000000049 pigment Substances 0.000 abstract 1
- YOWAEZWWQFSEJD-UHFFFAOYSA-N quinoxalin-2-amine Chemical compound C1=CC=CC2=NC(N)=CN=C21 YOWAEZWWQFSEJD-UHFFFAOYSA-N 0.000 abstract 1
- LUDZVVVPVCUUBP-UHFFFAOYSA-N quinoxaline-2,3-diamine Chemical class C1=CC=C2N=C(N)C(N)=NC2=C1 LUDZVVVPVCUUBP-UHFFFAOYSA-N 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B17/00—Azine dyes
- C09B17/005—Dyes containing at least four ortho-condensed rings with at least two ring N-atoms in the system, e.g. fluoflavine, fluorubine, fluorindine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Artificial Filaments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEB60672A DE1149477B (de) | 1960-12-29 | 1960-12-29 | Verfahren zur Herstellung von Fluorubin oder dessen Substitutionsprodukten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1008467A true GB1008467A (en) | 1965-10-27 |
Family
ID=6972921
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB45580/61A Expired GB1008467A (en) | 1960-12-29 | 1961-12-20 | Production of fluorubin |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3419557A (enExample) |
| BE (1) | BE612092A (enExample) |
| CH (1) | CH431773A (enExample) |
| DE (1) | DE1149477B (enExample) |
| GB (1) | GB1008467A (enExample) |
| SE (1) | SE301973B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7338553B2 (en) | 2005-10-08 | 2008-03-04 | Fujifilm Imaging Colorants Limited | Process, compound, ink and use |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102007050673A1 (de) * | 2007-10-19 | 2009-04-23 | Friedrich-Schiller-Universität Jena | Neue Hexaaza-acene und Verfahren zu ihrer Herstellung |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT649881A (enExample) * | 1960-05-19 | |||
| US3326915A (en) * | 1965-05-06 | 1967-06-20 | Burdick & Jackson Lab Inc | Self-polymerizable benzopyrazine monomers and process for the preparation thereof |
-
1960
- 1960-12-29 DE DEB60672A patent/DE1149477B/de active Pending
-
1961
- 1961-11-29 CH CH1388761A patent/CH431773A/de unknown
- 1961-12-13 SE SE12462/61A patent/SE301973B/xx unknown
- 1961-12-20 GB GB45580/61A patent/GB1008467A/en not_active Expired
- 1961-12-20 US US160942A patent/US3419557A/en not_active Expired - Lifetime
- 1961-12-28 BE BE612092A patent/BE612092A/fr unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7338553B2 (en) | 2005-10-08 | 2008-03-04 | Fujifilm Imaging Colorants Limited | Process, compound, ink and use |
Also Published As
| Publication number | Publication date |
|---|---|
| BE612092A (fr) | 1962-06-28 |
| CH431773A (de) | 1967-03-15 |
| US3419557A (en) | 1968-12-31 |
| SE301973B (enExample) | 1968-07-01 |
| DE1149477B (de) | 1963-05-30 |
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