GB1007973A - Process for obtaining hydroxycobalamin from natural materials - Google Patents
Process for obtaining hydroxycobalamin from natural materialsInfo
- Publication number
- GB1007973A GB1007973A GB2115161A GB2115161A GB1007973A GB 1007973 A GB1007973 A GB 1007973A GB 2115161 A GB2115161 A GB 2115161A GB 2115161 A GB2115161 A GB 2115161A GB 1007973 A GB1007973 A GB 1007973A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydroxycobalamin
- obtaining
- anions
- natural materials
- dissociable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- DQOCFCZRZOAIBN-WZHZPDAFSA-L hydroxycobalamin Chemical compound O.[Co+2].[N-]([C@@H]1[C@H](CC(N)=O)[C@@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)\C2=C(C)/C([C@H](C\2(C)C)CCC(N)=O)=N/C/2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O DQOCFCZRZOAIBN-WZHZPDAFSA-L 0.000 title abstract 2
- 150000001450 anions Chemical class 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- RMRCNWBMXRMIRW-BYFNXCQMSA-M cyanocobalamin Chemical compound N#C[Co+]N([C@]1([H])[C@H](CC(N)=O)[C@]\2(CCC(=O)NC[C@H](C)OP(O)(=O)OC3[C@H]([C@H](O[C@@H]3CO)N3C4=CC(C)=C(C)C=C4N=C3)O)C)C/2=C(C)\C([C@H](C/2(C)C)CCC(N)=O)=N\C\2=C\C([C@H]([C@@]/2(CC(N)=O)C)CCC(N)=O)=N\C\2=C(C)/C2=N[C@]1(C)[C@@](C)(CC(N)=O)[C@@H]2CCC(N)=O RMRCNWBMXRMIRW-BYFNXCQMSA-M 0.000 abstract 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- 229910002651 NO3 Inorganic materials 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 229960002104 cyanocobalamin Drugs 0.000 abstract 1
- 235000000639 cyanocobalamin Nutrition 0.000 abstract 1
- 239000011666 cyanocobalamin Substances 0.000 abstract 1
- 239000003456 ion exchange resin Substances 0.000 abstract 1
- 229920003303 ion-exchange polymer Polymers 0.000 abstract 1
- -1 nitrate ions Chemical class 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 229910021653 sulphate ion Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon or a metal, e.g. chelates or vitamin B12
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL279534D NL279534A (https=) | 1961-06-12 | ||
| GB2115161A GB1007973A (en) | 1961-06-12 | 1961-06-12 | Process for obtaining hydroxycobalamin from natural materials |
| AT103362A AT251204B (de) | 1961-06-12 | 1962-02-08 | Verfahren zur Herstellung von Hydroxycobalamin |
| ES0274708A ES274708A1 (es) | 1961-06-12 | 1962-02-17 | Procedimiento para la extracciën, purificaciën y cristalizaciën de hidroxicobalamina |
| DK626162A DK107373C (da) | 1961-06-12 | 1962-04-30 | Fremgangsmåde til udvinding af hydroksykobalamin i form af den frie base. |
| DEP29470A DE1200827B (de) | 1961-06-12 | 1962-05-24 | Verfahren zur Herstellung von Aquocobalamin |
| CH690162A CH413234A (de) | 1961-06-12 | 1962-06-07 | Verfahren zur Herstellung von Hydroxycobalamin aus Naturprodukten |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2115161A GB1007973A (en) | 1961-06-12 | 1961-06-12 | Process for obtaining hydroxycobalamin from natural materials |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1007973A true GB1007973A (en) | 1965-10-22 |
Family
ID=10158055
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2115161A Expired GB1007973A (en) | 1961-06-12 | 1961-06-12 | Process for obtaining hydroxycobalamin from natural materials |
Country Status (7)
| Country | Link |
|---|---|
| AT (1) | AT251204B (https=) |
| CH (1) | CH413234A (https=) |
| DE (1) | DE1200827B (https=) |
| DK (1) | DK107373C (https=) |
| ES (1) | ES274708A1 (https=) |
| GB (1) | GB1007973A (https=) |
| NL (1) | NL279534A (https=) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2709669A (en) * | 1951-06-13 | 1955-05-31 | Merck & Co Inc | Process for separating vitamin b12 active substances from contaminants |
-
0
- NL NL279534D patent/NL279534A/ unknown
-
1961
- 1961-06-12 GB GB2115161A patent/GB1007973A/en not_active Expired
-
1962
- 1962-02-08 AT AT103362A patent/AT251204B/de active
- 1962-02-17 ES ES0274708A patent/ES274708A1/es not_active Expired
- 1962-04-30 DK DK626162A patent/DK107373C/da active
- 1962-05-24 DE DEP29470A patent/DE1200827B/de active Pending
- 1962-06-07 CH CH690162A patent/CH413234A/de unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES274708A1 (es) | 1962-05-16 |
| CH413234A (de) | 1966-05-15 |
| DE1200827B (de) | 1965-09-16 |
| NL279534A (https=) | |
| AT251204B (de) | 1966-12-27 |
| DK107373C (da) | 1967-05-22 |
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