GB1002767A - Method for the manufacture of polyacrylonitrile - Google Patents
Method for the manufacture of polyacrylonitrileInfo
- Publication number
- GB1002767A GB1002767A GB32637/61A GB3263761A GB1002767A GB 1002767 A GB1002767 A GB 1002767A GB 32637/61 A GB32637/61 A GB 32637/61A GB 3263761 A GB3263761 A GB 3263761A GB 1002767 A GB1002767 A GB 1002767A
- Authority
- GB
- United Kingdom
- Prior art keywords
- fibres
- water
- stretching
- bath
- rinsing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229920002239 polyacrylonitrile Polymers 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 7
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract 6
- 235000005074 zinc chloride Nutrition 0.000 abstract 3
- 239000011592 zinc chloride Substances 0.000 abstract 3
- 238000009835 boiling Methods 0.000 abstract 1
- 230000015271 coagulation Effects 0.000 abstract 1
- 238000005345 coagulation Methods 0.000 abstract 1
- 239000000835 fiber Substances 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 230000002040 relaxant effect Effects 0.000 abstract 1
- 238000009987 spinning Methods 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/02—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/18—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds from polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/28—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F6/38—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from copolymers obtained by reactions only involving carbon-to-carbon unsaturated bonds comprising unsaturated nitriles as the major constituent
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Artificial Filaments (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
Abstract
1,002,767. Polyacrylonitrile fibres. TOHO RAYON KABUSHIKI KAISHA. Sep. 12, 1961 [Sep. 24, 1960], No. 32637/61. Heading B5B. Polyacrylonitrile fibres are obtained by spinning a solution of the polymer in aqueous zinc chloride solution of above 50% by weight zinc chloride into an aqueous coagulation bath containing from 10 to 20% by weight zinc chloride, rinsing the coagulated fibres in water at up to 80 C., stretching the fibres in water at above 95 C., and before the fibres cool or the water content of the fibres changes, relaxing them in contact with water at above 95 C. Rinsing may be effected under sufficient tension to stretch the fibres, and after rinsing, the fibres may be dried and then passed through a water bath to readjust their water content prior to stretching. The stretching and relaxation operations may be effected in the same bath, e.g. a boiling water bath. Alternatively stretching and relaxation may be effected in separate baths, the fibre passing over heated rollers to maintain its temperature during transference from one bath to the other.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3974660 | 1960-09-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1002767A true GB1002767A (en) | 1965-08-25 |
Family
ID=12561514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB32637/61A Expired GB1002767A (en) | 1960-09-24 | 1961-09-12 | Method for the manufacture of polyacrylonitrile |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3112161A (en) |
| BE (1) | BE608205A (en) |
| DE (1) | DE1289615B (en) |
| FI (1) | FI42854B (en) |
| GB (1) | GB1002767A (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3330898A (en) * | 1963-08-07 | 1967-07-11 | Dow Chemical Co | Method for preparing highly shrinkable acrylonitrile polymer fibers |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1069819B (en) * | 1959-11-26 | |||
| US2445042A (en) * | 1943-07-28 | 1948-07-13 | Du Pont | Method of treating oriented acrylonitrile structures |
| NL138683B (en) * | 1947-02-13 | |||
| US2681265A (en) * | 1948-11-27 | 1954-06-15 | American Viscose Corp | Spinning artificial filaments |
| BE496324A (en) * | 1949-06-13 | |||
| DE850213C (en) * | 1949-11-01 | 1952-09-22 | Kunstseidefabrik Bobingen | Process for the production of shaped structures from polyvinyl or polyacrylic compounds |
| GB690553A (en) * | 1950-01-05 | 1953-04-22 | British Celanese | Improvements in or relating to the production and use of solutions of acrylic polymers |
| US2558793A (en) * | 1950-03-24 | 1951-07-03 | Eastman Kodak Co | Mixtures comprising polyacrylonitrile and polyvinyl formate |
| GB816841A (en) * | 1955-10-07 | 1959-07-22 | Dow Chemical Co | Method for preparing acrylonitrile containing fibres |
-
1961
- 1961-09-12 GB GB32637/61A patent/GB1002767A/en not_active Expired
- 1961-09-15 BE BE608205A patent/BE608205A/en unknown
- 1961-09-19 FI FI1639/61A patent/FI42854B/fi active
- 1961-09-20 US US139413A patent/US3112161A/en not_active Expired - Lifetime
- 1961-09-22 DE DET20816A patent/DE1289615B/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US3112161A (en) | 1963-11-26 |
| BE608205A (en) | 1962-01-02 |
| DE1289615B (en) | 1969-02-20 |
| FI42854B (en) | 1970-08-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB1002767A (en) | Method for the manufacture of polyacrylonitrile | |
| GB741847A (en) | Improved method for producing filaments, films and like shaped structures from polymers and/or copolymers of acrylonitrile | |
| GB771946A (en) | Process for treating cords of thermoplastic material for use in the manufacture of tyres and like rubber products | |
| ES420987A1 (en) | Process for dyeing undrawn acrylonitrile polymer filaments | |
| GB1318024A (en) | Process for obtaining crimped fibres of acrylonitrile copolymers and polymer mixtures | |
| GB675143A (en) | Acrylonitrile polymers | |
| GB816841A (en) | Method for preparing acrylonitrile containing fibres | |
| GB767810A (en) | Improved process for the treatment of cotton products to improve their tensile strength | |
| GB597497A (en) | Improvements in or relating to the production of insolubilised protein-artificial filamentary products | |
| FR1178680A (en) | Method for increasing the stretchability of freshly spun viscose filaments | |
| ES343346A3 (en) | A procedure for the production of very accessible acrilonitril fibers. (Machine-translation by Google Translate, not legally binding) | |
| GB809916A (en) | Improvements in processing heat-shrinkable synthetic textile elements | |
| GB991957A (en) | Method of dyeing acrylonitrile polymer fibers | |
| ES438046A1 (en) | Process for the production of continuously dyed high-shrinkage filaments and fibres of acid-modified acrylonitrile copolymers | |
| GB1086553A (en) | Process for the manufacture of filaments of poly-ª-methyl-ª-butyrolactam | |
| GB1374184A (en) | Treatment of synthetic fibres | |
| GB1113051A (en) | Textile fibres | |
| GB956803A (en) | Viscose spinning process and product | |
| SU144446A1 (en) | The method of processing fibers from polyvinyl alcohol | |
| ES236034A1 (en) | A procedure for elevating the aptitude of stretching of newly spined viscose threads (Machine-translation by Google Translate, not legally binding) | |
| GB817724A (en) | Process for the production of artificial fibres of regenerated zein | |
| GB780375A (en) | Production of polyacrylonitrile fibres having a scaly integument | |
| GB900911A (en) | Process for treating artificial fibres | |
| GB1096062A (en) | Method of manufacturing synthetic fibres of polyvinyl alcohol having high abrasion resistance | |
| GB904605A (en) | A method of producing filaments and fibres by spinning sulphuric acid solutions of acrylonitrile polymers |