FR3058166B1 - Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues - Google Patents

Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues Download PDF

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Publication number
FR3058166B1
FR3058166B1 FR1660540A FR1660540A FR3058166B1 FR 3058166 B1 FR3058166 B1 FR 3058166B1 FR 1660540 A FR1660540 A FR 1660540A FR 1660540 A FR1660540 A FR 1660540A FR 3058166 B1 FR3058166 B1 FR 3058166B1
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France
Prior art keywords
carbon fibers
biosource
precursors
producing
producing carbon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1660540A
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English (en)
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FR3058166A1 (fr
Inventor
Alexander Korzhenko
Tatiana KOLOMIETS
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1660540A priority Critical patent/FR3058166B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to JP2019521438A priority patent/JP7062006B2/ja
Priority to PCT/FR2017/052952 priority patent/WO2018078288A1/fr
Priority to RU2019116178A priority patent/RU2748442C2/ru
Priority to CN201780067074.9A priority patent/CN109891011A/zh
Priority to KR1020197014764A priority patent/KR20190070350A/ko
Priority to EP17794394.1A priority patent/EP3532661A1/fr
Priority to US16/344,956 priority patent/US10844521B2/en
Priority to CA3041014A priority patent/CA3041014A1/fr
Publication of FR3058166A1 publication Critical patent/FR3058166A1/fr
Application granted granted Critical
Publication of FR3058166B1 publication Critical patent/FR3058166B1/fr
Priority to IL266086A priority patent/IL266086A/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/16—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate
    • D01F9/17—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate from lignin
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/05—Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C04B35/522—Graphite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/71—Ceramic products containing macroscopic reinforcing agents
    • C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
    • C04B35/80—Fibres, filaments, whiskers, platelets, or the like
    • C04B35/83—Carbon fibres in a carbon matrix
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/04—Carbon
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C08K7/02—Fibres or whiskers
    • C08K7/04—Fibres or whiskers inorganic
    • C08K7/06—Elements
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/16—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/444—Halide containing anions, e.g. bromide, iodate, chlorite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/447—Phosphates or phosphites, e.g. orthophosphate, hypophosphite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/449—Organic acids, e.g. EDTA, citrate, acetate, oxalate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/48—Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins
    • C04B2235/483—Si-containing organic compounds, e.g. silicone resins, (poly)silanes, (poly)siloxanes or (poly)silazanes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5208—Fibers
    • C04B2235/5252—Fibers having a specific pre-form
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5208—Fibers
    • C04B2235/5264—Fibers characterised by the diameter of the fibers
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/52—Constituents or additives characterised by their shapes
    • C04B2235/5284—Hollow fibers, e.g. nanotubes
    • C04B2235/5288—Carbon nanotubes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/616—Liquid infiltration of green bodies or pre-forms
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567—Treatment time
    • C—CHEMISTRY; METALLURGY
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658—Atmosphere during thermal treatment
    • C04B2235/6583—Oxygen containing atmosphere, e.g. with changing oxygen pressures
    • C04B2235/6585—Oxygen containing atmosphere, e.g. with changing oxygen pressures at an oxygen percentage above that of air
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Textile Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Composite Materials (AREA)
  • Inorganic Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Reinforced Plastic Materials (AREA)
  • Nonwoven Fabrics (AREA)
FR1660540A 2016-10-28 2016-10-28 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues Expired - Fee Related FR3058166B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR1660540A FR3058166B1 (fr) 2016-10-28 2016-10-28 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues
CA3041014A CA3041014A1 (fr) 2016-10-28 2017-10-26 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues.
RU2019116178A RU2748442C2 (ru) 2016-10-28 2017-10-26 Способ изготовления углеродных волокон из биопрекурсоров и получаемые углеродные волокна
CN201780067074.9A CN109891011A (zh) 2016-10-28 2017-10-26 由生物来源的前体制备碳纤维的方法和所制备的碳纤维
KR1020197014764A KR20190070350A (ko) 2016-10-28 2017-10-26 바이오소스 전구체들로부터 탄소 섬유들을 제조하기 위한 방법 및 제조된 탄소 섬유들
EP17794394.1A EP3532661A1 (fr) 2016-10-28 2017-10-26 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues
JP2019521438A JP7062006B2 (ja) 2016-10-28 2017-10-26 生物由来の前駆体から炭素繊維を製造する方法及び得られた炭素繊維
PCT/FR2017/052952 WO2018078288A1 (fr) 2016-10-28 2017-10-26 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues
US16/344,956 US10844521B2 (en) 2016-10-28 2017-10-26 Process for producing carbon fibres from biosourced precursors and the carbon fibres obtained
IL266086A IL266086A (en) 2016-10-28 2019-04-17 Process for producing carbon fibres from biosourced precursors and the carbon fibres obtained

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1660540A FR3058166B1 (fr) 2016-10-28 2016-10-28 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues
FR1660540 2016-10-28

Publications (2)

Publication Number Publication Date
FR3058166A1 FR3058166A1 (fr) 2018-05-04
FR3058166B1 true FR3058166B1 (fr) 2018-11-23

Family

ID=57539537

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Application Number Title Priority Date Filing Date
FR1660540A Expired - Fee Related FR3058166B1 (fr) 2016-10-28 2016-10-28 Procede de fabrication de fibres de carbone a partir de precurseurs biosources et fibres de carbone obtenues

Country Status (10)

Country Link
US (1) US10844521B2 (fr)
EP (1) EP3532661A1 (fr)
JP (1) JP7062006B2 (fr)
KR (1) KR20190070350A (fr)
CN (1) CN109891011A (fr)
CA (1) CA3041014A1 (fr)
FR (1) FR3058166B1 (fr)
IL (1) IL266086A (fr)
RU (1) RU2748442C2 (fr)
WO (1) WO2018078288A1 (fr)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7021044B2 (ja) * 2018-10-09 2022-02-16 北越コーポレーション株式会社 カーボン成形体の製造方法
GB2579864A (en) * 2018-12-18 2020-07-08 Univ Limerick Improvements relating to thermoelectric materials
GB201907004D0 (en) * 2019-05-17 2019-07-03 Univ Limerick Improvements relating to carbon fibre processing
KR102075114B1 (ko) * 2019-06-21 2020-02-07 국방과학연구소 라이오셀계 탄소섬유 제조를 위한 탄소 나노 튜브 코팅 및 열처리

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JPS59144625A (ja) * 1982-12-25 1984-08-18 Oji Paper Co Ltd 炭素繊維シ−トの製造法
US6720057B1 (en) * 1997-08-07 2004-04-13 Achim Neumayr Method for producing a cellulose fibre from hydrocellulose
FR2826646B1 (fr) 2001-06-28 2004-05-21 Toulouse Inst Nat Polytech Procede de fabrication selective de nanotubes de carbone ordonne en lit fluidise
CN1255585C (zh) 2004-07-15 2006-05-10 东华大学 纤维素基碳纤维的前体纤维的制备方法
EP1669480B1 (fr) * 2004-12-07 2007-05-02 Snecma Propulsion Solide Méthode pour obtenir des fils ou des feuilles à base de fibre de carbon à partir d'un précurseur cellulosique
US20070087120A1 (en) * 2005-10-18 2007-04-19 Connors Donald F Jr Fluid diffusion layers
US7824651B2 (en) 2007-05-08 2010-11-02 Nanotek Instruments, Inc. Method of producing exfoliated graphite, flexible graphite, and nano-scaled graphene platelets
US20110285049A1 (en) 2010-05-19 2011-11-24 Baker Frederick S Carbon nanotube (cnt)-enhanced precursor for carbon fiber production and method of making a cnt-enhanced continuous lignin fiber
KR101264001B1 (ko) 2011-01-13 2013-05-13 경북대학교 산학협력단 라이오셀/그래핀 나노복합체를 포함하는 전구체 섬유와 이를 이용한 탄소섬유 및 그 제조방법
KR101242377B1 (ko) 2011-10-05 2013-03-15 전남대학교산학협력단 탄소-탄소 복합 섬유의 제조 방법 및 이를 이용하여 제조되는 탄소 발열체, 탄소 히터
TWI589741B (zh) * 2012-01-23 2017-07-01 茵芬提亞公司 穩定木質素纖維以進一步轉換成碳纖維之方法
KR101230532B1 (ko) 2012-09-03 2013-02-06 국방과학연구소 탄소 복합재료
FR2997097B1 (fr) * 2012-10-22 2015-04-10 Arkema France Procede de fabrication d'une fibre de carbone, materiau precurseur utilise par le procede et fibre de carbone obtenue.
CN103774286B (zh) * 2014-01-08 2015-05-20 北京梦狐宇通竹纤维研究开发中心 一种纤维素纳米碳纤维过滤材料的制备方法
US20160168363A1 (en) * 2014-06-27 2016-06-16 Api Intellectual Property Holdings, Llc Nanocellulose-polymer composites, and processes for producing them
US20160122515A1 (en) * 2014-10-31 2016-05-05 Api Intellectual Property Holdings, Llc Automotive tires containing hydrophobic nanocellulose
CN104593906B (zh) * 2015-02-15 2017-01-11 东华大学 一种木质素基碳纤维的制备方法
FR3058167B1 (fr) * 2016-10-28 2019-11-22 Arkema France Nouveau procede de fabrication de materiaux hautement carbones et materiau hautement carbone obtenu

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FR3058166A1 (fr) 2018-05-04
CN109891011A (zh) 2019-06-14
EP3532661A1 (fr) 2019-09-04
WO2018078288A1 (fr) 2018-05-03
RU2748442C2 (ru) 2021-05-25
IL266086A (en) 2019-06-30
RU2019116178A3 (fr) 2021-01-22
JP7062006B2 (ja) 2022-05-02
RU2019116178A (ru) 2020-11-30
US10844521B2 (en) 2020-11-24
US20190271101A1 (en) 2019-09-05
CA3041014A1 (fr) 2018-05-03
KR20190070350A (ko) 2019-06-20
JP2019534395A (ja) 2019-11-28

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