FR3032362B1 - Procede de depot de nanoparticules et de microparticules carbonees oxydees - Google Patents

Procede de depot de nanoparticules et de microparticules carbonees oxydees Download PDF

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Publication number
FR3032362B1
FR3032362B1 FR1500231A FR1500231A FR3032362B1 FR 3032362 B1 FR3032362 B1 FR 3032362B1 FR 1500231 A FR1500231 A FR 1500231A FR 1500231 A FR1500231 A FR 1500231A FR 3032362 B1 FR3032362 B1 FR 3032362B1
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FR
France
Prior art keywords
substrate
temperature
spraying
microparticles
deposition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1500231A
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English (en)
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FR3032362A1 (fr
Inventor
Paolo Bondavalli
Gregory Pognon
Christophe Galindo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Thales SA
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Thales SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1500231A priority Critical patent/FR3032362B1/fr
Application filed by Thales SA filed Critical Thales SA
Priority to PCT/EP2016/052541 priority patent/WO2016124756A1/fr
Priority to KR1020177024642A priority patent/KR20170116066A/ko
Priority to EP16706982.2A priority patent/EP3254292A1/fr
Priority to CN201680013301.5A priority patent/CN107408462B/zh
Priority to AU2016214292A priority patent/AU2016214292A1/en
Priority to US15/548,710 priority patent/US20180025853A1/en
Priority to JP2017541337A priority patent/JP2018508992A/ja
Publication of FR3032362A1 publication Critical patent/FR3032362A1/fr
Application granted granted Critical
Publication of FR3032362B1 publication Critical patent/FR3032362B1/fr
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/84Processes for the manufacture of hybrid or EDL capacitors, or components thereof
    • H01G11/86Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/02Processes for applying liquids or other fluent materials performed by spraying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/007After-treatment
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/20Graphite
    • C01B32/21After-treatment
    • C01B32/23Oxidation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/24Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/26Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
    • H01G11/28Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features arranged or disposed on a current collector; Layers or phases between electrodes and current collectors, e.g. adhesives
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01GCAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
    • H01G11/00Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
    • H01G11/22Electrodes
    • H01G11/30Electrodes characterised by their material
    • H01G11/32Carbon-based
    • H01G11/36Nanostructures, e.g. nanofibres, nanotubes or fullerenes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2204/00Structure or properties of graphene
    • C01B2204/20Graphene characterized by its properties
    • C01B2204/22Electronic properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/13Energy storage using capacitors

Abstract

La présente invention se situe dans le domaine des composants pour le stockage de l'énergie et concerne un procédé de dépôt de nano/ microparticules, dont au moins des feuilles de graphène, sur un support (8), comprenant les étapes consistant à: • oxyder au moins lesdites feuilles de graphène; • suspendre lesdites nano-/microparticules dans au moins une solution comprenant au moins de l'eau comme solvant; • pulvériser par instabilité hydrodynamique chaque suspension sur ledit substrat (15) ; • chauffer ledit substrat (15), pendant chaque pulvérisation, de manière à promouvoir l'évaporation complète dudit solvant de chaque partie de chaque dite suspension pulvérisée sur ledit substrat (15) à une température inférieure ou égale à une fois et demie la température d'ébullition de chaque dite solution et inférieure ou égale à 200 degrés Celsius ; • recuire ledit dépôt (1) après la ou lesdites pulvérisations à une température suffisante pour désoxyder au moins le graphène oxydé présent dans ledit dépôt (1) et supérieure à la température dudit substrat (15) pendant l'étape de dépôt.
FR1500231A 2015-02-06 2015-02-06 Procede de depot de nanoparticules et de microparticules carbonees oxydees Active FR3032362B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR1500231A FR3032362B1 (fr) 2015-02-06 2015-02-06 Procede de depot de nanoparticules et de microparticules carbonees oxydees
KR1020177024642A KR20170116066A (ko) 2015-02-06 2016-02-05 산화된 탄소 기반 마이크로입자들 및 나노입자들을 퇴적하는 방법
EP16706982.2A EP3254292A1 (fr) 2015-02-06 2016-02-05 Procede de depot de nanoparticules et de microparticules carbonees oxydees
CN201680013301.5A CN107408462B (zh) 2015-02-06 2016-02-05 沉积氧化的碳基微颗粒和纳米颗粒的方法
PCT/EP2016/052541 WO2016124756A1 (fr) 2015-02-06 2016-02-05 Procede de depot de nanoparticules et de microparticules carbonees oxydees
AU2016214292A AU2016214292A1 (en) 2015-02-06 2016-02-05 Method of depositing oxidized carbon-based microparticles and nanoparticles
US15/548,710 US20180025853A1 (en) 2015-02-06 2016-02-05 Method of depositing oxidized carbon-based microparticles and nanoparticles
JP2017541337A JP2018508992A (ja) 2015-02-06 2016-02-05 酸化させた炭素系マイクロ粒子およびナノ粒子の堆積方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1500231 2015-02-06
FR1500231A FR3032362B1 (fr) 2015-02-06 2015-02-06 Procede de depot de nanoparticules et de microparticules carbonees oxydees

Publications (2)

Publication Number Publication Date
FR3032362A1 FR3032362A1 (fr) 2016-08-12
FR3032362B1 true FR3032362B1 (fr) 2020-05-29

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
FR1500231A Active FR3032362B1 (fr) 2015-02-06 2015-02-06 Procede de depot de nanoparticules et de microparticules carbonees oxydees

Country Status (8)

Country Link
US (1) US20180025853A1 (fr)
EP (1) EP3254292A1 (fr)
JP (1) JP2018508992A (fr)
KR (1) KR20170116066A (fr)
CN (1) CN107408462B (fr)
AU (1) AU2016214292A1 (fr)
FR (1) FR3032362B1 (fr)
WO (1) WO2016124756A1 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2644579C1 (ru) * 2016-12-13 2018-02-13 Сергей Иванович Жебелев Способ сборки наноматериалов из графена
GB201707428D0 (en) * 2017-05-09 2017-06-21 Applied Graphene Mat Plc ] Composite moulding materials
KR102655394B1 (ko) * 2019-04-02 2024-04-09 삼성디스플레이 주식회사 표시 장치의 제조 장치 및 표시 장치의 제조 방법
CN113244931B (zh) * 2020-02-11 2022-05-03 中国石油化工股份有限公司 催化剂以及含不饱和烃气体的催化氧化脱氧方法
FR3110281B1 (fr) 2020-05-14 2022-08-19 Thales Sa Electrode nanostructurée pour supercondensateur
CN113649252B (zh) * 2021-08-18 2022-12-27 中国科学院重庆绿色智能技术研究院 喷涂制备微纳多级自补偿结构及其柔性压力传感器

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KR100895521B1 (ko) * 2007-10-12 2009-04-30 (주)탑나노시스 스프레이 코팅을 이용한 탄소나노튜브 투명도전막 및 그제조방법
JP6034621B2 (ja) * 2011-09-02 2016-11-30 株式会社半導体エネルギー研究所 蓄電装置の電極および蓄電装置
KR101388695B1 (ko) * 2011-10-24 2014-04-28 삼성전기주식회사 그래핀 투명전극 및 이의 제조방법
WO2013100382A1 (fr) * 2011-12-31 2013-07-04 제일모직주식회사 Procédé de préparation d'un composite graphène-nanotubes de carbone à l'aide de pyrolyse par pulvérisation et composite graphène-nanotubes de carbone préparé par ce procédé
US9530531B2 (en) * 2013-02-21 2016-12-27 Nanotek Instruments, Inc. Process for producing highly conducting and transparent films from graphene oxide-metal nanowire hybrid materials
US9017777B2 (en) * 2013-02-26 2015-04-28 Quantumscape Corporation Inorganic films using a cascaded source for battery devices
US8871296B2 (en) * 2013-03-14 2014-10-28 Nanotek Instruments, Inc. Method for producing conducting and transparent films from combined graphene and conductive nano filaments
US20140272199A1 (en) * 2013-03-14 2014-09-18 Yi-Jun Lin Ultrasonic spray coating of conducting and transparent films from combined graphene and conductive nano filaments
TW201504363A (zh) * 2013-07-16 2015-02-01 Enerage Inc 石墨烯油墨及石墨烯線路的製作方法
CN103400632B (zh) * 2013-07-17 2016-05-11 常州二维碳素科技股份有限公司 一种石墨烯掺杂材料及其应用
CN103396573B (zh) * 2013-08-22 2015-07-22 电子科技大学 一种复合纳米薄膜的制备方法

Also Published As

Publication number Publication date
KR20170116066A (ko) 2017-10-18
WO2016124756A1 (fr) 2016-08-11
EP3254292A1 (fr) 2017-12-13
US20180025853A1 (en) 2018-01-25
FR3032362A1 (fr) 2016-08-12
JP2018508992A (ja) 2018-03-29
CN107408462B (zh) 2021-03-23
CN107408462A (zh) 2017-11-28
AU2016214292A1 (en) 2017-08-31

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