FR3032362B1 - Procede de depot de nanoparticules et de microparticules carbonees oxydees - Google Patents
Procede de depot de nanoparticules et de microparticules carbonees oxydees Download PDFInfo
- Publication number
- FR3032362B1 FR3032362B1 FR1500231A FR1500231A FR3032362B1 FR 3032362 B1 FR3032362 B1 FR 3032362B1 FR 1500231 A FR1500231 A FR 1500231A FR 1500231 A FR1500231 A FR 1500231A FR 3032362 B1 FR3032362 B1 FR 3032362B1
- Authority
- FR
- France
- Prior art keywords
- substrate
- temperature
- spraying
- microparticles
- deposition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 4
- 239000011859 microparticle Substances 0.000 title abstract 3
- 239000002105 nanoparticle Substances 0.000 title abstract 3
- 230000008021 deposition Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 229910052799 carbon Inorganic materials 0.000 title 1
- 239000000758 substrate Substances 0.000 abstract 4
- 229910021389 graphene Inorganic materials 0.000 abstract 3
- 238000005507 spraying Methods 0.000 abstract 3
- 238000000151 deposition Methods 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- 239000000725 suspension Substances 0.000 abstract 2
- 238000000137 annealing Methods 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000004146 energy storage Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D1/00—Processes for applying liquids or other fluent materials
- B05D1/02—Processes for applying liquids or other fluent materials performed by spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/007—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/20—Graphite
- C01B32/21—After-treatment
- C01B32/23—Oxidation
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/24—Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/26—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
- H01G11/28—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features arranged or disposed on a current collector; Layers or phases between electrodes and current collectors, e.g. adhesives
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/36—Nanostructures, e.g. nanofibres, nanotubes or fullerenes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/20—Graphene characterized by its properties
- C01B2204/22—Electronic properties
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Abstract
La présente invention se situe dans le domaine des composants pour le stockage de l'énergie et concerne un procédé de dépôt de nano/ microparticules, dont au moins des feuilles de graphène, sur un support (8), comprenant les étapes consistant à: • oxyder au moins lesdites feuilles de graphène; • suspendre lesdites nano-/microparticules dans au moins une solution comprenant au moins de l'eau comme solvant; • pulvériser par instabilité hydrodynamique chaque suspension sur ledit substrat (15) ; • chauffer ledit substrat (15), pendant chaque pulvérisation, de manière à promouvoir l'évaporation complète dudit solvant de chaque partie de chaque dite suspension pulvérisée sur ledit substrat (15) à une température inférieure ou égale à une fois et demie la température d'ébullition de chaque dite solution et inférieure ou égale à 200 degrés Celsius ; • recuire ledit dépôt (1) après la ou lesdites pulvérisations à une température suffisante pour désoxyder au moins le graphène oxydé présent dans ledit dépôt (1) et supérieure à la température dudit substrat (15) pendant l'étape de dépôt.
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1500231A FR3032362B1 (fr) | 2015-02-06 | 2015-02-06 | Procede de depot de nanoparticules et de microparticules carbonees oxydees |
KR1020177024642A KR20170116066A (ko) | 2015-02-06 | 2016-02-05 | 산화된 탄소 기반 마이크로입자들 및 나노입자들을 퇴적하는 방법 |
EP16706982.2A EP3254292A1 (fr) | 2015-02-06 | 2016-02-05 | Procede de depot de nanoparticules et de microparticules carbonees oxydees |
CN201680013301.5A CN107408462B (zh) | 2015-02-06 | 2016-02-05 | 沉积氧化的碳基微颗粒和纳米颗粒的方法 |
PCT/EP2016/052541 WO2016124756A1 (fr) | 2015-02-06 | 2016-02-05 | Procede de depot de nanoparticules et de microparticules carbonees oxydees |
AU2016214292A AU2016214292A1 (en) | 2015-02-06 | 2016-02-05 | Method of depositing oxidized carbon-based microparticles and nanoparticles |
US15/548,710 US20180025853A1 (en) | 2015-02-06 | 2016-02-05 | Method of depositing oxidized carbon-based microparticles and nanoparticles |
JP2017541337A JP2018508992A (ja) | 2015-02-06 | 2016-02-05 | 酸化させた炭素系マイクロ粒子およびナノ粒子の堆積方法 |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1500231 | 2015-02-06 | ||
FR1500231A FR3032362B1 (fr) | 2015-02-06 | 2015-02-06 | Procede de depot de nanoparticules et de microparticules carbonees oxydees |
Publications (2)
Publication Number | Publication Date |
---|---|
FR3032362A1 FR3032362A1 (fr) | 2016-08-12 |
FR3032362B1 true FR3032362B1 (fr) | 2020-05-29 |
Family
ID=53673980
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR1500231A Active FR3032362B1 (fr) | 2015-02-06 | 2015-02-06 | Procede de depot de nanoparticules et de microparticules carbonees oxydees |
Country Status (8)
Country | Link |
---|---|
US (1) | US20180025853A1 (fr) |
EP (1) | EP3254292A1 (fr) |
JP (1) | JP2018508992A (fr) |
KR (1) | KR20170116066A (fr) |
CN (1) | CN107408462B (fr) |
AU (1) | AU2016214292A1 (fr) |
FR (1) | FR3032362B1 (fr) |
WO (1) | WO2016124756A1 (fr) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2644579C1 (ru) * | 2016-12-13 | 2018-02-13 | Сергей Иванович Жебелев | Способ сборки наноматериалов из графена |
GB201707428D0 (en) * | 2017-05-09 | 2017-06-21 | Applied Graphene Mat Plc ] | Composite moulding materials |
KR102655394B1 (ko) * | 2019-04-02 | 2024-04-09 | 삼성디스플레이 주식회사 | 표시 장치의 제조 장치 및 표시 장치의 제조 방법 |
CN113244931B (zh) * | 2020-02-11 | 2022-05-03 | 中国石油化工股份有限公司 | 催化剂以及含不饱和烃气体的催化氧化脱氧方法 |
FR3110281B1 (fr) | 2020-05-14 | 2022-08-19 | Thales Sa | Electrode nanostructurée pour supercondensateur |
CN113649252B (zh) * | 2021-08-18 | 2022-12-27 | 中国科学院重庆绿色智能技术研究院 | 喷涂制备微纳多级自补偿结构及其柔性压力传感器 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100895521B1 (ko) * | 2007-10-12 | 2009-04-30 | (주)탑나노시스 | 스프레이 코팅을 이용한 탄소나노튜브 투명도전막 및 그제조방법 |
JP6034621B2 (ja) * | 2011-09-02 | 2016-11-30 | 株式会社半導体エネルギー研究所 | 蓄電装置の電極および蓄電装置 |
KR101388695B1 (ko) * | 2011-10-24 | 2014-04-28 | 삼성전기주식회사 | 그래핀 투명전극 및 이의 제조방법 |
WO2013100382A1 (fr) * | 2011-12-31 | 2013-07-04 | 제일모직주식회사 | Procédé de préparation d'un composite graphène-nanotubes de carbone à l'aide de pyrolyse par pulvérisation et composite graphène-nanotubes de carbone préparé par ce procédé |
US9530531B2 (en) * | 2013-02-21 | 2016-12-27 | Nanotek Instruments, Inc. | Process for producing highly conducting and transparent films from graphene oxide-metal nanowire hybrid materials |
US9017777B2 (en) * | 2013-02-26 | 2015-04-28 | Quantumscape Corporation | Inorganic films using a cascaded source for battery devices |
US8871296B2 (en) * | 2013-03-14 | 2014-10-28 | Nanotek Instruments, Inc. | Method for producing conducting and transparent films from combined graphene and conductive nano filaments |
US20140272199A1 (en) * | 2013-03-14 | 2014-09-18 | Yi-Jun Lin | Ultrasonic spray coating of conducting and transparent films from combined graphene and conductive nano filaments |
TW201504363A (zh) * | 2013-07-16 | 2015-02-01 | Enerage Inc | 石墨烯油墨及石墨烯線路的製作方法 |
CN103400632B (zh) * | 2013-07-17 | 2016-05-11 | 常州二维碳素科技股份有限公司 | 一种石墨烯掺杂材料及其应用 |
CN103396573B (zh) * | 2013-08-22 | 2015-07-22 | 电子科技大学 | 一种复合纳米薄膜的制备方法 |
-
2015
- 2015-02-06 FR FR1500231A patent/FR3032362B1/fr active Active
-
2016
- 2016-02-05 CN CN201680013301.5A patent/CN107408462B/zh active Active
- 2016-02-05 US US15/548,710 patent/US20180025853A1/en not_active Abandoned
- 2016-02-05 WO PCT/EP2016/052541 patent/WO2016124756A1/fr active Application Filing
- 2016-02-05 EP EP16706982.2A patent/EP3254292A1/fr not_active Withdrawn
- 2016-02-05 KR KR1020177024642A patent/KR20170116066A/ko not_active Application Discontinuation
- 2016-02-05 JP JP2017541337A patent/JP2018508992A/ja active Pending
- 2016-02-05 AU AU2016214292A patent/AU2016214292A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
KR20170116066A (ko) | 2017-10-18 |
WO2016124756A1 (fr) | 2016-08-11 |
EP3254292A1 (fr) | 2017-12-13 |
US20180025853A1 (en) | 2018-01-25 |
FR3032362A1 (fr) | 2016-08-12 |
JP2018508992A (ja) | 2018-03-29 |
CN107408462B (zh) | 2021-03-23 |
CN107408462A (zh) | 2017-11-28 |
AU2016214292A1 (en) | 2017-08-31 |
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