FR2903483B1 - Procede et appareil de separation d'air par distillation cryogenique - Google Patents

Procede et appareil de separation d'air par distillation cryogenique

Info

Publication number
FR2903483B1
FR2903483B1 FR0652793A FR0652793A FR2903483B1 FR 2903483 B1 FR2903483 B1 FR 2903483B1 FR 0652793 A FR0652793 A FR 0652793A FR 0652793 A FR0652793 A FR 0652793A FR 2903483 B1 FR2903483 B1 FR 2903483B1
Authority
FR
France
Prior art keywords
air separation
cryogenic distillation
cryogenic
distillation
separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0652793A
Other languages
English (en)
Other versions
FR2903483A1 (fr
Inventor
Pierre Olivier Bodelin
Benoit Davidan
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to FR0652793A priority Critical patent/FR2903483B1/fr
Priority to PCT/EP2007/056085 priority patent/WO2008003585A2/fr
Priority to US12/305,490 priority patent/US8776546B2/en
Priority to EP07765496A priority patent/EP2047195A2/fr
Priority to CN200780025308XA priority patent/CN101484769B/zh
Priority to JP2009517115A priority patent/JP5599609B2/ja
Publication of FR2903483A1 publication Critical patent/FR2903483A1/fr
Application granted granted Critical
Publication of FR2903483B1 publication Critical patent/FR2903483B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04254Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using the cold stored in external cryogenic fluids
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04472Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages
    • F25J3/04496Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages for compensating variable air feed or variable product demand by alternating between periods of liquid storage and liquid assist
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04793Rectification, e.g. columns; Reboiler-condenser
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04812Different modes, i.e. "runs" of operation
    • F25J3/04836Variable air feed, i.e. "load" or product demand during specified periods, e.g. during periods with high respectively low power costs
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00Processes characterised by the type or other details of the feed stream
    • F25J2210/42Nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/30External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/42One fluid being nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/62Details of storing a fluid in a tank

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)
FR0652793A 2006-07-04 2006-07-04 Procede et appareil de separation d'air par distillation cryogenique Expired - Fee Related FR2903483B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR0652793A FR2903483B1 (fr) 2006-07-04 2006-07-04 Procede et appareil de separation d'air par distillation cryogenique
PCT/EP2007/056085 WO2008003585A2 (fr) 2006-07-04 2007-06-19 Procédé de séparation d'air et appareil utilisant la distillation cryogénique
US12/305,490 US8776546B2 (en) 2006-07-04 2007-06-19 Air separation process and apparatus using cryogenic distillation
EP07765496A EP2047195A2 (fr) 2006-07-04 2007-06-19 Procédé de séparation d'air et appareil utilisant la distillation cryogénique
CN200780025308XA CN101484769B (zh) 2006-07-04 2007-06-19 使用低温蒸馏的空气分离方法和设备
JP2009517115A JP5599609B2 (ja) 2006-07-04 2007-06-19 極低温蒸留を使用する空気分離方法及び装置

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0652793A FR2903483B1 (fr) 2006-07-04 2006-07-04 Procede et appareil de separation d'air par distillation cryogenique

Publications (2)

Publication Number Publication Date
FR2903483A1 FR2903483A1 (fr) 2008-01-11
FR2903483B1 true FR2903483B1 (fr) 2014-07-04

Family

ID=37907151

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0652793A Expired - Fee Related FR2903483B1 (fr) 2006-07-04 2006-07-04 Procede et appareil de separation d'air par distillation cryogenique

Country Status (6)

Country Link
US (1) US8776546B2 (fr)
EP (1) EP2047195A2 (fr)
JP (1) JP5599609B2 (fr)
CN (1) CN101484769B (fr)
FR (1) FR2903483B1 (fr)
WO (1) WO2008003585A2 (fr)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2959297B1 (fr) * 2010-04-22 2012-04-27 Air Liquide Procede et appareil de production d'azote par distillation cryogenique d'air
FR2973486B1 (fr) * 2011-03-31 2013-05-03 Air Liquide Procede de separation d'air par distillation cryogenique
US10281207B2 (en) * 2016-06-30 2019-05-07 L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method for the production of air gases by the cryogenic separation of air with variable liquid production and power usage
FR3084736B1 (fr) * 2018-08-01 2022-04-15 Air Liquide Procede et appareil de production d'argon par distillation cryogenique de l'air
JP7460974B1 (ja) 2023-08-14 2024-04-03 レール・リキード-ソシエテ・アノニム・プール・レテュード・エ・レクスプロワタシオン・デ・プロセデ・ジョルジュ・クロード 窒素発生装置および窒素発生方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5242158B2 (fr) * 1973-01-26 1977-10-22
JPS6124968A (ja) * 1984-07-13 1986-02-03 大同酸素株式会社 高純度窒素ガス製造装置
FR2660741A1 (fr) * 1990-04-10 1991-10-11 Air Liquide Procede et installation de production d'azote gazeux, et systeme de fourniture d'azote correspondant.
US5224336A (en) * 1991-06-20 1993-07-06 Air Products And Chemicals, Inc. Process and system for controlling a cryogenic air separation unit during rapid changes in production
DE4135302A1 (de) * 1991-10-25 1993-04-29 Linde Ag Anlage zur tieftemperaturzerlegung von luft
FR2697620B1 (fr) * 1992-10-30 1994-12-23 Air Liquide Procédé et installation de production d'azote gazeux à débit variable.
US5335680A (en) * 1993-04-26 1994-08-09 Moore Pamela K Hair clip
JP2672251B2 (ja) * 1993-08-10 1997-11-05 大同ほくさん 株式会社 窒素ガス製造装置
JP3676531B2 (ja) * 1997-01-28 2005-07-27 大陽日酸株式会社 窒素ガス製造方法
JP3021389B2 (ja) * 1997-05-01 2000-03-15 大同ほくさん株式会社 高純度窒素ガス製造装置
JP3065976B2 (ja) * 1997-12-04 2000-07-17 日本エア・リキード株式会社 窒素製造装置
EP0908689A3 (fr) * 1997-08-20 1999-06-23 AIR LIQUIDE Japan, Ltd. Procédé et dispositif de distillation d'air
US5996373A (en) * 1998-02-04 1999-12-07 L'air Liquide, Societe Ananyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Cryogenic air separation process and apparatus
FR2784308B1 (fr) * 1998-10-09 2001-11-09 Air Liquide Procede et installation de separation de gaz avec production d'un debit gazeux variable
US6357259B1 (en) * 2000-09-29 2002-03-19 The Boc Group, Inc. Air separation method to produce gaseous product
JP3644918B2 (ja) * 2001-10-01 2005-05-11 日本エア・リキード株式会社 空気分離装置及び空気分離方法

Also Published As

Publication number Publication date
WO2008003585A9 (fr) 2009-03-05
JP2009541709A (ja) 2009-11-26
CN101484769A (zh) 2009-07-15
US20090314031A1 (en) 2009-12-24
CN101484769B (zh) 2013-01-02
US8776546B2 (en) 2014-07-15
JP5599609B2 (ja) 2014-10-01
FR2903483A1 (fr) 2008-01-11
EP2047195A2 (fr) 2009-04-15
WO2008003585A2 (fr) 2008-01-10
WO2008003585A3 (fr) 2009-01-15

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Effective date: 20200306