FR2697620B1 - Procédé et installation de production d'azote gazeux à débit variable. - Google Patents

Procédé et installation de production d'azote gazeux à débit variable.

Info

Publication number
FR2697620B1
FR2697620B1 FR9213026A FR9213026A FR2697620B1 FR 2697620 B1 FR2697620 B1 FR 2697620B1 FR 9213026 A FR9213026 A FR 9213026A FR 9213026 A FR9213026 A FR 9213026A FR 2697620 B1 FR2697620 B1 FR 2697620B1
Authority
FR
France
Prior art keywords
installation
production
nitrogen gas
variable flow
variable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR9213026A
Other languages
English (en)
Other versions
FR2697620A1 (fr
Inventor
Bernard Darredeau
Maurice Grenier
Catherine Garnier
Francois Venet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
Original Assignee
Air Liquide SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA filed Critical Air Liquide SA
Priority to FR9213026A priority Critical patent/FR2697620B1/fr
Priority to DE69306361T priority patent/DE69306361T2/de
Priority to EP93402420A priority patent/EP0595672B1/fr
Priority to JP5254126A priority patent/JPH06201259A/ja
Priority to US08/136,276 priority patent/US5355680A/en
Priority to CA002109364A priority patent/CA2109364A1/fr
Publication of FR2697620A1 publication Critical patent/FR2697620A1/fr
Application granted granted Critical
Publication of FR2697620B1 publication Critical patent/FR2697620B1/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04254Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using the cold stored in external cryogenic fluids
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04472Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages
    • F25J3/04496Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages for compensating variable air feed or variable product demand by alternating between periods of liquid storage and liquid assist
    • F25J3/04503Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages for compensating variable air feed or variable product demand by alternating between periods of liquid storage and liquid assist by exchanging "cold" between at least two different cryogenic liquids, e.g. independently from the main heat exchange line of the air fractionation and/or by using external alternating storage systems
    • F25J3/04509Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using the cold from cryogenic liquids produced within the air fractionation unit and stored in internal or intermediate storages for compensating variable air feed or variable product demand by alternating between periods of liquid storage and liquid assist by exchanging "cold" between at least two different cryogenic liquids, e.g. independently from the main heat exchange line of the air fractionation and/or by using external alternating storage systems within the cold part of the air fractionation, i.e. exchanging "cold" within the fractionation and/or main heat exchange line
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00Processes characterised by the type or other details of the feed stream
    • F25J2210/42Nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00Processes or apparatus involving steps for expanding of process streams
    • F25J2240/40Expansion without extracting work, i.e. isenthalpic throttling, e.g. JT valve, regulating valve or venturi, or isentropic nozzle, e.g. Laval
    • F25J2240/44Expansion without extracting work, i.e. isenthalpic throttling, e.g. JT valve, regulating valve or venturi, or isentropic nozzle, e.g. Laval the fluid being nitrogen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/10Mathematical formulae, modeling, plot or curves; Design methods
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/62Details of storing a fluid in a tank
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00Refrigeration
    • Y10S62/912External refrigeration system
    • Y10S62/913Liquified gas
FR9213026A 1992-10-30 1992-10-30 Procédé et installation de production d'azote gazeux à débit variable. Expired - Fee Related FR2697620B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR9213026A FR2697620B1 (fr) 1992-10-30 1992-10-30 Procédé et installation de production d'azote gazeux à débit variable.
DE69306361T DE69306361T2 (de) 1992-10-30 1993-10-04 Verfahren und Anlage zur Herstellung von gasförmigem Stickstoff mit variabelen Mengen
EP93402420A EP0595672B1 (fr) 1992-10-30 1993-10-04 Procédé et installation de production d'azote gazeux à débit variable
JP5254126A JPH06201259A (ja) 1992-10-30 1993-10-12 可変流量のガス状窒素を製造する方法及び装置
US08/136,276 US5355680A (en) 1992-10-30 1993-10-15 Process and installation for producing gaseous nitrogen with variable flow rate
CA002109364A CA2109364A1 (fr) 1992-10-30 1993-10-27 Procede et installation de production d'azote gazeux a debit variable

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9213026A FR2697620B1 (fr) 1992-10-30 1992-10-30 Procédé et installation de production d'azote gazeux à débit variable.

Publications (2)

Publication Number Publication Date
FR2697620A1 FR2697620A1 (fr) 1994-05-06
FR2697620B1 true FR2697620B1 (fr) 1994-12-23

Family

ID=9435035

Family Applications (1)

Application Number Title Priority Date Filing Date
FR9213026A Expired - Fee Related FR2697620B1 (fr) 1992-10-30 1992-10-30 Procédé et installation de production d'azote gazeux à débit variable.

Country Status (6)

Country Link
US (1) US5355680A (fr)
EP (1) EP0595672B1 (fr)
JP (1) JPH06201259A (fr)
CA (1) CA2109364A1 (fr)
DE (1) DE69306361T2 (fr)
FR (1) FR2697620B1 (fr)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3447437B2 (ja) * 1995-07-26 2003-09-16 日本エア・リキード株式会社 高純度窒素ガス製造装置
US5678425A (en) * 1996-06-07 1997-10-21 Air Products And Chemicals, Inc. Method and apparatus for producing liquid products from air in various proportions
US5682763A (en) * 1996-10-25 1997-11-04 Air Products And Chemicals, Inc. Ultra high purity oxygen distillation unit integrated with ultra high purity nitrogen purifier
FR2757282B1 (fr) * 1996-12-12 2006-06-23 Air Liquide Procede et installation de fourniture d'un debit variable d'un gaz de l'air
US5778700A (en) * 1997-04-30 1998-07-14 The Boc Group, Inc. Method of producing gaseous oxygen at variable rate
EP0908689A3 (fr) * 1997-08-20 1999-06-23 AIR LIQUIDE Japan, Ltd. Procédé et dispositif de distillation d'air
US6006546A (en) * 1998-04-29 1999-12-28 Air Products And Chemicals, Inc. Nitrogen purity control in the air separation unit of an IGCC power generation system
US5983668A (en) * 1998-04-29 1999-11-16 Air Products And Chemicals, Inc. Air separation unit feed flow control in an IGCC power generation system
FR2903483B1 (fr) * 2006-07-04 2014-07-04 Air Liquide Procede et appareil de separation d'air par distillation cryogenique
FR2959297B1 (fr) 2010-04-22 2012-04-27 Air Liquide Procede et appareil de production d'azote par distillation cryogenique d'air
CN102829606B (zh) * 2012-09-08 2015-02-18 浙江海天气体有限公司 一种利用液氧倒罐制取高纯液氮的空分装置

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2605647A1 (de) * 1976-02-12 1977-08-18 Linde Ag Verfahren und vorrichtung zur erzeugung von gasfoermigem sauerstoff durch zweistufige tieftemperaturrektifikation von luft
GB2129115B (en) * 1982-10-27 1986-03-12 Air Prod & Chem Producing gaseous nitrogen
EP0144430B1 (fr) * 1983-03-08 1989-01-11 Daidousanso Co., Ltd. Appareil de production d'azote gazeux de purete elevee
JPS6124968A (ja) * 1984-07-13 1986-02-03 大同酸素株式会社 高純度窒素ガス製造装置
DE3913880A1 (de) * 1989-04-27 1990-10-31 Linde Ag Verfahren und vorrichtung zur tieftemperaturzerlegung von luft
FR2660741A1 (fr) * 1990-04-10 1991-10-11 Air Liquide Procede et installation de production d'azote gazeux, et systeme de fourniture d'azote correspondant.
FR2670278B1 (fr) * 1990-12-06 1993-01-22 Air Liquide Procede et installation de distillation d'air en regime variable de production d'oxygene gazeux.
US5224336A (en) * 1991-06-20 1993-07-06 Air Products And Chemicals, Inc. Process and system for controlling a cryogenic air separation unit during rapid changes in production
US5271231A (en) * 1992-08-10 1993-12-21 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Method and apparatus for gas liquefaction with plural work expansion of feed as refrigerant and air separation cycle embodying the same

Also Published As

Publication number Publication date
CA2109364A1 (fr) 1994-05-01
EP0595672B1 (fr) 1996-12-04
DE69306361D1 (de) 1997-01-16
DE69306361T2 (de) 1997-05-28
EP0595672A1 (fr) 1994-05-04
JPH06201259A (ja) 1994-07-19
FR2697620A1 (fr) 1994-05-06
US5355680A (en) 1994-10-18

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Legal Events

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ST Notification of lapse