FR2816609B1 - Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants - Google Patents

Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants

Info

Publication number
FR2816609B1
FR2816609B1 FR0014595A FR0014595A FR2816609B1 FR 2816609 B1 FR2816609 B1 FR 2816609B1 FR 0014595 A FR0014595 A FR 0014595A FR 0014595 A FR0014595 A FR 0014595A FR 2816609 B1 FR2816609 B1 FR 2816609B1
Authority
FR
France
Prior art keywords
mesoporeous
absorbents
catalysts
preparation process
inorganic solids
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR0014595A
Other languages
English (en)
Other versions
FR2816609A1 (fr
Inventor
Dominique Plee
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Carbonisation et Charbons Actifs CECA SA
Original Assignee
Carbonisation et Charbons Actifs CECA SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR0014595A priority Critical patent/FR2816609B1/fr
Application filed by Carbonisation et Charbons Actifs CECA SA filed Critical Carbonisation et Charbons Actifs CECA SA
Priority to CA002428734A priority patent/CA2428734A1/fr
Priority to PCT/FR2001/003496 priority patent/WO2002040402A1/fr
Priority to AU2002218356A priority patent/AU2002218356A1/en
Priority to JP2002542736A priority patent/JP2004525846A/ja
Priority to EP01996513A priority patent/EP1334066A1/fr
Priority to KR10-2003-7006547A priority patent/KR20030067685A/ko
Publication of FR2816609A1 publication Critical patent/FR2816609A1/fr
Application granted granted Critical
Publication of FR2816609B1 publication Critical patent/FR2816609B1/fr
Priority to US10/437,456 priority patent/US20040035751A1/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/181Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
    • C01B33/185Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process of crystalline silica-polymorphs having molecular sieve properties, e.g. silicalites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004Sorbent size or size distribution, e.g. particle size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016Particle form
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/2803Sorbents comprising a binder, e.g. for forming aggregated, agglomerated or granulated products
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28069Pore volume, e.g. total pore volume, mesopore volume, micropore volume
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078Pore diameter
    • B01J20/28083Pore diameter being in the range 2-50 nm, i.e. mesopores
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282Porous sorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/3433Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/3483Regenerating or reactivating by thermal treatment not covered by groups B01J20/3441 - B01J20/3475, e.g. by heating or cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/3491Regenerating or reactivating by pressure treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/03Catalysts comprising molecular sieves not having base-exchange properties
    • B01J29/0308Mesoporous materials not having base exchange properties, e.g. Si-MCM-41
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/041Mesoporous materials having base exchange properties, e.g. Si/Al-MCM-41
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/40Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/50Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54Sorbents specially adapted for analytical or investigative chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Nanotechnology (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
FR0014595A 2000-11-14 2000-11-14 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants Expired - Fee Related FR2816609B1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR0014595A FR2816609B1 (fr) 2000-11-14 2000-11-14 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants
PCT/FR2001/003496 WO2002040402A1 (fr) 2000-11-14 2001-11-09 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et adsorbants
AU2002218356A AU2002218356A1 (en) 2000-11-14 2001-11-09 Mesoporous inorganic solids, method for preparing same and uses thereof in particular as catalysts and adsorbents
JP2002542736A JP2004525846A (ja) 2000-11-14 2001-11-09 メソ細孔無機固体と、その製造方法と、その触媒および吸着剤としての使用
CA002428734A CA2428734A1 (fr) 2000-11-14 2001-11-09 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et adsorbants
EP01996513A EP1334066A1 (fr) 2000-11-14 2001-11-09 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et adsorbants
KR10-2003-7006547A KR20030067685A (ko) 2000-11-14 2001-11-09 메소다공성 무기 고형물, 이의 제조 방법 및 특히 촉매 및흡착제로서의 이의 용도
US10/437,456 US20040035751A1 (en) 2000-11-14 2003-05-14 Inorganic mesoporous solids, a process for their preparation and their use, notably as catalysts and adsorbents

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0014595A FR2816609B1 (fr) 2000-11-14 2000-11-14 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants

Publications (2)

Publication Number Publication Date
FR2816609A1 FR2816609A1 (fr) 2002-05-17
FR2816609B1 true FR2816609B1 (fr) 2003-01-10

Family

ID=8856397

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0014595A Expired - Fee Related FR2816609B1 (fr) 2000-11-14 2000-11-14 Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et absorbants

Country Status (8)

Country Link
US (1) US20040035751A1 (fr)
EP (1) EP1334066A1 (fr)
JP (1) JP2004525846A (fr)
KR (1) KR20030067685A (fr)
AU (1) AU2002218356A1 (fr)
CA (1) CA2428734A1 (fr)
FR (1) FR2816609B1 (fr)
WO (1) WO2002040402A1 (fr)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6906208B2 (en) 1999-09-07 2005-06-14 Abb Lummus Global Inc. Mesoporous material and use thereof for the selective oxidation of organic compounds
US7608747B2 (en) 1999-09-07 2009-10-27 Lummus Technology Inc. Aromatics hydrogenolysis using novel mesoporous catalyst system
CA2404830C (fr) * 2002-10-17 2011-03-22 University Of Windsor Tamis moleculaires mesaporeux metalliques pour oxyde metallique de transition utilises pour la production d'ammoniac par activation du diazote a la temperature ambiante
FR2891539B1 (fr) * 2005-09-30 2007-11-30 Rhodia Recherches & Tech Silice de cohesion elevee, procede de preparation et utilisations
JP4512060B2 (ja) * 2006-04-18 2010-07-28 独立行政法人科学技術振興機構 3次元構造メソポーラスシリカとその製造方法
CN100529754C (zh) * 2006-11-10 2009-08-19 中国科学院山西煤炭化学研究所 一种分离苯及其同系物的方法
US7824641B2 (en) * 2007-05-25 2010-11-02 Lehigh University Periodic mesoporous phosphorus-nitrogen compounds
US8088277B2 (en) * 2008-06-11 2012-01-03 General Electric Company Methods and system for removing impurities from heavy fuel
US8986836B2 (en) * 2009-03-19 2015-03-24 Ohio University Microspheres and their methods of preparation
EP3000785B1 (fr) * 2013-05-22 2019-03-06 Mitsui Chemicals, Inc. Particules d'oxyde métallique poreuses, leur procédé de fabrication, et leur utilisation
JP7320405B2 (ja) * 2018-09-28 2023-08-03 住友化学株式会社 高分子化合物の製造方法
JP7484650B2 (ja) 2020-10-15 2024-05-16 トヨタ自動車株式会社 多孔質カーボン、触媒担体、及び多孔質カーボンの製造方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3556725A (en) * 1969-02-26 1971-01-19 Sylvania Electric Prod Process for producing low-bulk density silica
US5057296A (en) * 1990-12-10 1991-10-15 Mobil Oil Corp. Method for synthesizing mesoporous crystalline material
US5622684A (en) * 1995-06-06 1997-04-22 Board Of Trustees Operating Michigan State University Porous inorganic oxide materials prepared by non-ionic surfactant templating route
DE19530031A1 (de) * 1995-08-16 1997-02-20 Merck Patent Gmbh Poröse monodisperse SiO¶2¶-Partikel
US5863515A (en) * 1996-02-20 1999-01-26 California Institute Of Technology Mesoporous alumina and process for its preparation
US5718878A (en) * 1996-07-12 1998-02-17 Akzo Nobel N.V. Mesoporous titania and process for its preparation
JP3410634B2 (ja) * 1997-05-30 2003-05-26 株式会社豊田中央研究所 球状メソ多孔体及びその製造方法
FR2764213B1 (fr) * 1997-06-10 1999-07-16 Inst Francais Du Petrole Catalyseur d'hydrotraitement de charges hydrocarbonees dans un reacteur a lit fixe
DE19730125A1 (de) * 1997-07-14 1999-01-21 Basf Ag Aluminiumoxid enthaltender Feststoff mit großer Oberfläche
DE19730126A1 (de) * 1997-07-14 1999-01-21 Basf Ag Aluminiumoxid enthaltender Feststoff mit großer Oberfläche
US6139814A (en) * 1997-11-10 2000-10-31 Ford Global Technologies, Inc. Thermally stable, high-surface-area metal oxides made by organic templating
US6027706A (en) * 1998-05-05 2000-02-22 Board Of Trustees Operating Michigan State University Porous aluminum oxide materials prepared by non-ionic surfactant assembly route
DE19841142A1 (de) * 1998-09-09 2000-03-23 Degussa Kieselsäuren und Metallsilikate mit regelmäßiger Mesoporenstruktur

Also Published As

Publication number Publication date
US20040035751A1 (en) 2004-02-26
JP2004525846A (ja) 2004-08-26
KR20030067685A (ko) 2003-08-14
CA2428734A1 (fr) 2002-05-23
AU2002218356A1 (en) 2002-05-27
EP1334066A1 (fr) 2003-08-13
WO2002040402A1 (fr) 2002-05-23
FR2816609A1 (fr) 2002-05-17

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Effective date: 20070731